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Wet Chemistry Lab
2014
Feras Mfarrej
 General Safety Rules
 Glassware Safety
 Chemical Safety
 Electrical Safety
 Heating Safety
 First Aid
• Think before you start a piece of work.
• Never work alone.
• Wear the proper protective equipment.
• Keep your workplace tidy
• Never put anything into your mouth
• NO eating, drinking, smoking, or applying cosmetics in
labs
• Tie back long hair.
• Roll up loose sleeves
• During lab work, keep your hands away from your face.
• Never “horse around” or play practical jokes in the
laboratory.
• After handling chemicals, always wash your hands with
soap and water.
• Never do unauthorized experiments
• Do not leave an on-going experiment unattended
• Listen to or read instructions carefully before attempting
to do anything.
 Know the location of the fire extinguisher, fire blanket, eyewash
station, and first aid kit
 Clean up your lab area at the conclusion of the laboratory period.
 Report all accidents, no matter how minor, to the supervisor
 In case of an emergency where we have to evacuate, proceed out
the nearest exit.
 No vendors
 No visitors
 Chipped or cracked glassware should not be used. Show it to the
supervisor
 Broken glassware should not be disposed of in a classroom trashcan.
There is a special glass disposal container for it
 When pouring liquids into glassware, make sure the container you are
pouring into is resting on a table at least a hand-breadth from the edge.
 Pour down a glass stirring rod to prevent liquids from splattering
 When inserting glass tubing into a rubber stopper, apply a lubricant to
the glass and use a twisting motion
 Do not place hot glassware in water. Rapid cooling may make it shatter
 Wear protective goggles and a lab apron
whenever heating or pouring hazardous
chemicals
 Never mix chemicals together unless you are
told to do so (and then only in the manner
specified).
• If you need to smell the odor of a chemical,
waft the fumes toward your nose with one
hand. Do not put your nose over the container
and inhale the fumes.
 Never pour water into a concentrated acid. Acid should be poured
slowly into water.
 Follow the instructions of your supervisor when disposing of all
chemicals
• When working with hazardous materials, have a second person nearby
• Check labels on containers twice to make sure you use the right
chemical and of the correct concentration.
• The most dangerous substance is the one that has no label.
• Never return chemicals to reagent bottles. (Try for the correct amount
and share any excess.)
• Never taste any chemicals (you should never taste anything in the lab).
 Wash hands frequently (Wash your hands after handling hazardous
chemicals.)
 Label everything
 Read labels and SDSs
 Corrosives - Nitric Acid
 Oxidizers - Silver Nitrate
 General Organic Compounds -
Aniline
 Caustics - Calcium Oxide
 Reactive Metals - Sodium
 Explosive Anhydrides and
Anhydrous Compounds -
Sodium Peroxide
 Ketones - Acetone
• Poisons - Potassium Cyanide
• General Inorganic Compounds -
Calcium Carbide
• Flammable Metals - Magnesium
• Flammables - Ethanol, Butanol,
Ethyl Ether
• Carcinogens - Formaldehyde
 When using the fume hood you first need to make sure the exhaust
blower is operating and air is entering the hood.
 Remember, do not put your face inside the hood!
 Minimize storage of chemicals in the hood
 Clean spills immediately
 Work with the sash at the proper operating level
Hazardous Waste- This is a waste which contains the characteristics of
being any of the following:
 Toxic
 Corrosive
 Ignitable
 Flammable
 Oxidizer
 Clean all spills immediately.
 Dispose of chemicals in proper receptacle.
 Ensure that no trash is left behind
 No trash in the sinks
 Dispose of waste and broken glassware in proper containers
 Be sure your hands and your lab area are dry before using electrical
equipment
 Lay electrical cords where no one can trip on them or get caught in
them
 Never poke anything into electrical outlets.
• If water or a chemical is spilled onto equipment, shut off power at the
main switch and unplug the equipment
• If it is safe to do so, work with only one hand, keeping the other hand
at your side or in your pocket, away from all conductive material
Lab Saftey
 Let burners and hotplates cool down before touching them. Test to see
if they are cool enough by bringing the back of your hand close to them
 Use tongs and/or protective gloves to handle hot objects
 Never reach across an open flame or burner
 Use only the type of glassware that may safely be heated
 Always point the top ends of glassware , that are being heated away
from people
 When heating a glassware , move it around slowly over the flame to
distribute the heat evenly
 Only glassware that is thoroughly dry should be heated
 Heat glassware by placing it on a wire gauze platform on a ring-stand.
Do not hold it in your hand
 When lighting a burner, wait until a match is struck or the striker is in
place before you turn on the gas
 The amount of air can be adjusted by the air supply valve below the
tube of the burner. This regulates the flame temperature and color
• Never leave a burner or hotplate unattended.
• Beware of hot glass -it looks exactly like cold glass
Lab Saftey
 Injury: Burns ‫الحروق‬
 To do: Immediately flush with cold water until
burning sensation is lessened.
 Injury: Cuts, bruises ‫جروح‬‫وكدمات‬
 To do: Do not touch an open wound without safety
gloves. Pressing directly on minor cuts will stop
bleeding in a few minutes. Apply cold compress to
bruises to reduce swelling.
 Injury: Fainting ‫إغماء‬
 To do: Provide fresh air and have the person recline so
that their head is lower than the rest of their body.
 Injury: The eyes ‫العين‬ ‫اصابات‬
 To do: Flush eyes immediately with plenty of water for
several minutes. If a foreign object is lodged in the
eye, do not allow the eye to be rubbed.
 Injury: Poisoning ‫تسمم‬
 To do: Find out what substance was responsible for
the poisoning and alert the supervisor immediately.
 Injury: Spills on the skin ‫على‬ ‫انسكاب‬‫الجلد‬
 To do: Flush with large quantities of water. For acid
spills apply baking soda solution. For base spills apply
vinegar or boric acid.
 Injury: Electrical shock ‫الكهربائية‬ ‫الصدمة‬
 To do: Shut off the current at the source. Remove wire
with rubber gloves. Alert the supervisor immediately.
 Flush contaminated area
with water
 Remove contaminated
clothing
 Rinse with water for 15
minutes
 Seek medical attention if
irritation persists
 Prevent Ingestion
 NO eating, drinking, smoking, or applying cosmetics
in labs
 Wash hands frequently
 Label everything
 Read labels and SDSs
Lab Saftey
DO NOT GUESS!!!!
Who is responsible for safety in the lab?
http://www.cdc.gov/
http://www.unece.org/trans/danger/publi/ghs/ghs_welcome_e.html
Globally Harmonized System of Classification and Labeling of Chemicals (GHS)
Thank You
Firas Mfarrej 12/2014

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Lab Saftey

  • 2.  General Safety Rules  Glassware Safety  Chemical Safety  Electrical Safety  Heating Safety  First Aid
  • 3. • Think before you start a piece of work. • Never work alone. • Wear the proper protective equipment. • Keep your workplace tidy
  • 4. • Never put anything into your mouth • NO eating, drinking, smoking, or applying cosmetics in labs • Tie back long hair. • Roll up loose sleeves • During lab work, keep your hands away from your face. • Never “horse around” or play practical jokes in the laboratory.
  • 5. • After handling chemicals, always wash your hands with soap and water. • Never do unauthorized experiments • Do not leave an on-going experiment unattended • Listen to or read instructions carefully before attempting to do anything.
  • 6.  Know the location of the fire extinguisher, fire blanket, eyewash station, and first aid kit  Clean up your lab area at the conclusion of the laboratory period.  Report all accidents, no matter how minor, to the supervisor  In case of an emergency where we have to evacuate, proceed out the nearest exit.  No vendors  No visitors
  • 7.  Chipped or cracked glassware should not be used. Show it to the supervisor  Broken glassware should not be disposed of in a classroom trashcan. There is a special glass disposal container for it  When pouring liquids into glassware, make sure the container you are pouring into is resting on a table at least a hand-breadth from the edge.
  • 8.  Pour down a glass stirring rod to prevent liquids from splattering  When inserting glass tubing into a rubber stopper, apply a lubricant to the glass and use a twisting motion  Do not place hot glassware in water. Rapid cooling may make it shatter
  • 9.  Wear protective goggles and a lab apron whenever heating or pouring hazardous chemicals  Never mix chemicals together unless you are told to do so (and then only in the manner specified). • If you need to smell the odor of a chemical, waft the fumes toward your nose with one hand. Do not put your nose over the container and inhale the fumes.
  • 10.  Never pour water into a concentrated acid. Acid should be poured slowly into water.  Follow the instructions of your supervisor when disposing of all chemicals • When working with hazardous materials, have a second person nearby • Check labels on containers twice to make sure you use the right chemical and of the correct concentration.
  • 11. • The most dangerous substance is the one that has no label. • Never return chemicals to reagent bottles. (Try for the correct amount and share any excess.) • Never taste any chemicals (you should never taste anything in the lab).  Wash hands frequently (Wash your hands after handling hazardous chemicals.)  Label everything  Read labels and SDSs
  • 12.  Corrosives - Nitric Acid  Oxidizers - Silver Nitrate  General Organic Compounds - Aniline  Caustics - Calcium Oxide  Reactive Metals - Sodium  Explosive Anhydrides and Anhydrous Compounds - Sodium Peroxide  Ketones - Acetone • Poisons - Potassium Cyanide • General Inorganic Compounds - Calcium Carbide • Flammable Metals - Magnesium • Flammables - Ethanol, Butanol, Ethyl Ether • Carcinogens - Formaldehyde
  • 13.  When using the fume hood you first need to make sure the exhaust blower is operating and air is entering the hood.  Remember, do not put your face inside the hood!  Minimize storage of chemicals in the hood  Clean spills immediately  Work with the sash at the proper operating level
  • 14. Hazardous Waste- This is a waste which contains the characteristics of being any of the following:  Toxic  Corrosive  Ignitable  Flammable  Oxidizer
  • 15.  Clean all spills immediately.  Dispose of chemicals in proper receptacle.  Ensure that no trash is left behind  No trash in the sinks  Dispose of waste and broken glassware in proper containers
  • 16.  Be sure your hands and your lab area are dry before using electrical equipment  Lay electrical cords where no one can trip on them or get caught in them  Never poke anything into electrical outlets.
  • 17. • If water or a chemical is spilled onto equipment, shut off power at the main switch and unplug the equipment • If it is safe to do so, work with only one hand, keeping the other hand at your side or in your pocket, away from all conductive material
  • 19.  Let burners and hotplates cool down before touching them. Test to see if they are cool enough by bringing the back of your hand close to them  Use tongs and/or protective gloves to handle hot objects  Never reach across an open flame or burner
  • 20.  Use only the type of glassware that may safely be heated  Always point the top ends of glassware , that are being heated away from people  When heating a glassware , move it around slowly over the flame to distribute the heat evenly  Only glassware that is thoroughly dry should be heated
  • 21.  Heat glassware by placing it on a wire gauze platform on a ring-stand. Do not hold it in your hand  When lighting a burner, wait until a match is struck or the striker is in place before you turn on the gas  The amount of air can be adjusted by the air supply valve below the tube of the burner. This regulates the flame temperature and color • Never leave a burner or hotplate unattended. • Beware of hot glass -it looks exactly like cold glass
  • 23.  Injury: Burns ‫الحروق‬  To do: Immediately flush with cold water until burning sensation is lessened.
  • 24.  Injury: Cuts, bruises ‫جروح‬‫وكدمات‬  To do: Do not touch an open wound without safety gloves. Pressing directly on minor cuts will stop bleeding in a few minutes. Apply cold compress to bruises to reduce swelling.
  • 25.  Injury: Fainting ‫إغماء‬  To do: Provide fresh air and have the person recline so that their head is lower than the rest of their body.
  • 26.  Injury: The eyes ‫العين‬ ‫اصابات‬  To do: Flush eyes immediately with plenty of water for several minutes. If a foreign object is lodged in the eye, do not allow the eye to be rubbed.
  • 27.  Injury: Poisoning ‫تسمم‬  To do: Find out what substance was responsible for the poisoning and alert the supervisor immediately.
  • 28.  Injury: Spills on the skin ‫على‬ ‫انسكاب‬‫الجلد‬  To do: Flush with large quantities of water. For acid spills apply baking soda solution. For base spills apply vinegar or boric acid.
  • 29.  Injury: Electrical shock ‫الكهربائية‬ ‫الصدمة‬  To do: Shut off the current at the source. Remove wire with rubber gloves. Alert the supervisor immediately.
  • 30.  Flush contaminated area with water  Remove contaminated clothing  Rinse with water for 15 minutes  Seek medical attention if irritation persists
  • 31.  Prevent Ingestion  NO eating, drinking, smoking, or applying cosmetics in labs  Wash hands frequently  Label everything  Read labels and SDSs
  • 33. DO NOT GUESS!!!! Who is responsible for safety in the lab?