This document presents a thesis on characterizing Brillouin effects in optical microfibers. The thesis was conducted by Kazi Tasneem Farhan for their M. Eng. Sc. program under the supervision of Assoc. Prof. Dr. Zulfadzli Yusoff. The research objectives were to fabricate uniform microfibers of different lengths and diameters and characterize Brillouin scattering, lasing, and spatial effects. Various microfibers were fabricated and their profiles, insertion losses, and Brillouin responses were measured and analyzed. Spatial characterization showed Brillouin gain shifts along the microfiber length. The experimental results agreed with previous numerical simulations. Future work could focus on optimizing Ge-doped microfibers for