Aspen plus gettingstartedfreecourse

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Aspen Plus - Getting Started Prepared by Chemical Engineering Guy
Presentation · February 2019
DOI: 10.13140/RG.2.2.36814.72005
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Emmanuel Ortega
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Chemical Engineering Guy
www.ChemicalEngineeringGuy.com

Change:
• All T of Reactors
• Feed Composition
• No. of Plates in Distl. Col
• T of Heat Ex
• Gas Sep. T
• Compressor P
• Utility Costs

▪ Makes us easier/faster work
▪ Multiple and Simultaneous Simulations
▪ Different Real-Life Scenarios
▪ Change on raw/feed materials scenario
▪ Pricing and Costs calculation
▪ Raw Materials
▪ Plant Cost
▪ Utilities
▪ How it would behave under different conditions
▪ High/Low Pressure
▪ Humidity Changes
▪ Temperature change (cool/warm days/seasons)

▪ Mainly:
▪ Petrochemical
▪ Pharmaceutical
▪ Fine chemicals
▪ Other commodities such as:
▪ Sulfuric acids
▪ Chlorine/Caustic industry
▪ Solvents
▪ Coatings
▪ Many more…

▪ Excelent for your curriculum as an engineer
▪ Perfect for analytical/numerical minds
▪ Good for debuging and fixing “what if” scenarios

1. Introduction
2. Our Chemical Process!
3. Setting up the Physical Property Environment
4. Simulation Environment I – The Flowsheet
5. Simulation Environment II – Unit Operations
6. Running, Results & Analysis
7. Case Studies (A,B,C,D)
8. Conclusion

▪ Introductory Knowledge of Processes Modeling
▪ Setting the adequate Physical Properties
▪ General Flowsheet Concepts
▪ Basic Flowsheet “manipulation”
▪ Common Unit Operations
▪ Minimum Requirements to set up & run a Simulation
▪ Analyze several changes in process conditions
▪ Create an interest in Process Modeling

▪ Please contact me if required (doubts, questions, comments, suggestions)
▪ Contact@ChemicalEngineeringGuy.com
▪ More courses…

▪ Unit Operations
▪ Heat Exchange
▪ Heat Exchanger
▪ Reaction Kinetics
▪ Combustion Chamber / Reactor
▪ Momentum
▪ Pump
▪ Compressor
▪ Separation Process
▪ Flash Drum
▪ Distillation Columns

▪ A hydrocarbon feed rich in aromatics is to be separated via a series of
separation processes.
▪ It is sent from a previous plant at ambient temperature (15°C) and
pressurized to 10 bar.
▪ A total of 100 kmol/h must be treated
▪ Most of the hydrocarbons msut be recovered and the leftovers will be burnt in
a combustion chamber.
▪ The combustion chamber will burn all hydrocarbons to form carbon dioxide.
Assume 100% combustion. The air for combustion was previously adjusted to
50°C, 10bar. There is no pression loss in the combustion chamber.
▪ The liquified section must be de-pressurized in order to continue treatment. It
drops to 2 bar via a valve.

▪ This stream is then fed to a Distillation Column.
▪ It currently has a total of 15 trays.
▪ Feed tray must be between 7 and 8.
▪ Recommended operation is partial vapor in order to avoid an extra stage. Reflux
▪ Ratio is set to 5 (molar) and the approx.
▪ Pressure drop is unknown, but can be assumed to be low or negligible.
▪ At least 20% of the feed must be recovered for further treatment
▪ The Distillate is to be treated in a following process. It must be compressed to
5 bar. We use a compressor with approx. 88% efficiency. It can be modeled as
an isentropic compression.

▪ The bottoms of this column are not pure enough. Further distillation is
required.
▪ The following column requires a total of:
▪ 20 trays feeding in 50% approx.
▪ It uses a total condenser since the distillate is required as a liquid
▪ Recommended Distillate recovery is 60%
▪ Reflux is set to 4 molar
▪ The pressure drop is unkown, but current process has:
▪ Condenser working ate 1.90 bar
▪ Reboiler working at 2.10 bar
▪ The distillate can be sent for storage
▪ The bottom must be further pressurized +0.5 bar in order to allow for
pressure drop due to frictions. Efficiency of pump is 66.7%

▪ Requirements:
▪ Model the plant using Aspen Plus in Steady State
▪ Verify Material/Energy Balances of the unit operations & processes
▪ Verify purity and composition of streams
▪ Verify conditions such as T, P and Flow rates.
▪ For specific unit operations, verify their relevant results
▪ Heater → Heat duty
▪ Combustion Chamber → T-max, Heat released by reaction
▪ Compressor/Pump → Required Work
▪ For the Columns → Reboiler & Condenser Duties

▪ Pipes

▪ Flash Tank:

▪ Combustion Chamber / Reactor

▪ Distillation Columns

▪ Compressor & Pump

▪ PDF of Process diagram
▪ Spreadsheet with Unit Operations & Process conditions
▪ Spreadsheet with Component list & database

▪ Landing Page

▪ Min. Requirements:
▪ Adding Components to the Component List
▪ Selecting a Physical Property Method (Thermodynamic pack)
▪ If you want to further explore this environment →
▪ Aspen Plus - Physical Properties
▪ Different Types of Components
▪ Methods (EOS, Activity, Mixed)
▪ Modeling new/inexistent components
▪ Physical & Chemical Property Analysis
▪ Thermodynamic & Transport Properties

▪ Add the following compounds to the “Component List”
▪ Methane
▪ Ethane
▪ Propane
▪ N-Butane
▪ Cyclohexane
▪ Benzene
▪ Toluene
▪ Oxygen
▪ Nitrogen

▪ Select Peng Robinson, as it is mostly non-polar system
▪ Most models will be “set-up”
▪ Pure substances Properties will be loaded
▪ Binary Interactions are calculated
▪ Tip: Use the Method Assistant

▪ Get to know what is a flowsheet and how to manipulate it.
▪ Menus, Tool, Areas, etc…
▪ Important:
▪ General Setup
▪ Blocks: Unit Operations, Others
▪ Streams (Material, Heat, Work)
▪ Analysis tools

▪ Manipulation of the Flowsheet:
▪ Adding Unit Operations
▪ Adding Material and Energy streams
▪ Moving
▪ Labeling
▪ Rotating
▪ Deleting
▪ Copy and Pasting

▪ Typical Unit Operations
▪ Adding UO
▪ Setting up
▪ Connecting streams
▪ Inlet/outlet

▪ Feed
▪ F = 100 kmol/h
▪ T = 15°C
▪ P = 10 bar
▪ Comp:
▪ Toluene 0.190
▪ Benzene 0.200
▪ Cyclohex 0.120
▪ Butane 0.110
▪ Propane 0.075
▪ Methane 0.150
▪ Ethane 0.155
▪ Air
▪ F = 1200 kmol/h
▪ T = 50°C
▪ P = 10 bar
▪ Comp:
▪ 0.79 N2
▪ 0.21 O2

▪ Heater
▪ T = 40°C
▪ dP = 0 bar
▪ P = 10 bar

▪ Flash2
▪ Q = 0
▪ T = 40°C
▪ P = 10 bar
▪ dP = 0 bar

▪ Valve
▪ P = 2 bar

▪ RadFrac
▪ Stages = 15
▪ Feed = 8
▪ Cond = Partial
▪ D-Rate = 20 kmol/h
▪ Reflux = 5 molar
▪ P-reboiler = 1.95 bar

▪ Distil
▪ Stages = 20
▪ Feed = 10
▪ Cond = Total
▪ D:F Ratio = 0.60
▪ Reflux = 4 molar
▪ P-cond = 1.90 bar
▪ P-reboiler = 2.10 bar

▪ Compr
▪ Type = Isentropic
▪ Eff = 88%
▪ P-final = 5 bar

▪ Pump
▪ Type = Isentropic
▪ Eff = 66.7%
▪ P-increse = 0.5 bar

▪ RSTOIC
▪ Type = Stoichiometry
▪ Q = 0
▪ P = 10 bar
▪ dP = 0 bar

▪ RXN
▪ CH4 + 2O2 = CO2 + 2H2O
▪ C2H6 + 7O2 = 4CO2 + 6H2O
▪ C3H8 + 5O2 = 3CO2 + 4H2O
▪ 2C4H10 + 13O2 = 8CO2 + 10H2O
▪ C6H12 + 6O2 = 3CO2 + 6H2O
▪ 2C6H6 + 15O2 = 12CO2 + 6H2O
▪ C7H8 + 9O2 = 7CO2 + 4H2O

▪ Running the simulation
▪ Errors & Debugging
▪ Getting Results
▪ Stream Results
▪ Block Results
▪ Analysis
▪ What if Scenarios

▪ Error Messages

▪ Manual “what if” cases
▪ Change several inputs to get new outputs
▪ Change of T Heat
▪ Change of P valve
▪ Change of P Reactor
▪ Changer of Reflux Dist1
▪ Change of Stages Dist2

▪ Compare your results with mine:

▪ Change T = 40°C to T = 30°C of Heater

▪ Change Pressure of Valve
▪ P = 1 bar
▪ P = 5 bar
No Drastic
Change

▪ Change Pressure of Reactor
▪ P = -5bar
▪ P = 1bar

▪ Change Reflux Ratio from 4 to 2 and/or 6 and/or 15

1. Introduction
2. Our Chemical Process!
3. Setting up the Physical Property Environment
4. Simulation Environment I – The Flowsheet
5. Simulation Environment II – Unit Operations
6. Running, Results & Analysis
7. Case Studies
8. Conclusion

▪ Introductory Knowledge of Processes Modeling
▪ General Flowsheet Concepts
▪ Setting the adequate Physical Properties
▪ Basic Flowsheet “manipulation”
▪ Minimum Requirements to set up & run a Simulation
▪ Common Unit Operations
▪ Create an interest in Process Modeling

▪ Typically, you will follow your training with
▪ Basic Course
▪ What do you learn there:
▪ More on Aspen Plus
▪ More on Physical Property Environment
▪ Flowsheet techniques
▪ More Unit Operations
▪ Analysis Tools
▪ Plenty Workshops
▪ Process & Industry Case Studies

▪ Aspen Plus – Basic Course!
▪ 1 Month Free Trial then $8.00 USD/month

▪ Aspen Plus – Training Bundle includes:
▪ Aspen Plus – Getting Started
▪ Aspen Plus – Basic Course
▪ Aspen Plus – Physical Properties
▪ Aspen Plus – Intermediate Course
▪ Aspen Plus – Boot camp: 12 Case studies
▪ All other new upcoming Aspen Plus courses
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