This document provides details about the study areas, sampling methods, and statistical analysis used in a study of forest soils in South Africa. It describes the climate, geology, soils, and vegetation of the Rhenosterhoek, Mauchsberg, and Klipkraal forest areas from which soil samples were taken. A total of 22 sampling sites were selected across plantations of different ages to represent similar geological and geographical properties. Soil sampling involved taking composite samples from the top 20 cm of soil at each site.