Grease Compatibility Studies – Can Your
Next Grease Change Cause Issues
Today’s Topics
 Why mixing greases is a bad idea
 Why using Compatibility Charts is an EVEN WORSE idea
 What should I do if I can't avoid the mixing
 What is REALLY in ASTM D6185? Why is it being changed?
 How can I work greases like the REAL WORLD?
 Demonstration of the Grease Thief Test Stand
 How to interpret Grease Compatibility results
Mixing greases
 Grease gets runny
 Grease gets hard
 Leaks out
 Failure to lubricate
 Hard as a rock
 Unable to pump
 Machine failure
Compatibility Charts – BAD IDEA
Compatibility Charts – BAD IDEA
Compatibility Charts – BAD IDEA
 Charts do not agree
 Do not reference testing
that was used to create
them
 Do not account for base oil
differences
 Do not account for additive
differences
Why run a Compatibility Study?
 When grease mixing cannot be avoided
 When its too late, the mixing has already occurred
 When getting all the old grease out is impossible or impractical
 Even if greases are made with the same base oil and thickener type
they may be incompatible
 Evaluating grease mixtures can prevent issues when supply or
formulation changes have happened
 If the greases are incompatible, mixing them during use could lead to
significant changes in grease flow characteristics and shear behavior
which would result in inadequate lubrication
Advantages of a Compatibility Study
 Allows for evaluation of mixtures without risk to equipment
or affecting uptime
 Can provide data to support the ability to mix greases
slowly or if maintenance needs to be scheduled to change
out greases
 Assess risks and costs of available alternatives
Compatibility Study– per D6185
 Primary testing using three standards to evaluate grease
mixtures (10:90, 50:50 and 90:10)
– Dropping point by D566/D2265
– Shear stability by D217
– Storage stability by D217
 If all mixtures pass primary testing or if an application requires
specific evaluation secondary compatibility tests can be used
for further evaluation
Working the mixtures
ASTM D6185 Proposed Change: Test Stand Mix & Work
10,000 Double Strokes in Grease Worker 72 Hours in Bearing Simulator
9 balls rotating at 1795 rpm
3.6x Ball Pass frequency
Equivalent to 93 seconds of working in a typical
electric motor bearing
Total mixing/working events: 28,000,000
MRG Compatibility Study– added steps
 The baselines and 10:90, 50:50 and 90:10 mixtures and mixed and
verified using FTIR and RDE
 The baselines and mixtures and packed and worked on test stand
simulator for 72 hours
 Using D7718 samples are pulled, and rheological properties are
evaluated for changes
 Formulations are compared for additive dilution, function
 Baseline formulations are compared
Prep for Compatibility Study
Interpreting Results
 To pass the mixtures need to have responses that are
between the two baseline greases
 Changes outside of this can cause the grease mixture to
perform differently than expected
Interpreting Results
Interpreting Results

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Grease Mixing and Compatibility Studies

  • 1. Grease Compatibility Studies – Can Your Next Grease Change Cause Issues
  • 2. Today’s Topics  Why mixing greases is a bad idea  Why using Compatibility Charts is an EVEN WORSE idea  What should I do if I can't avoid the mixing  What is REALLY in ASTM D6185? Why is it being changed?  How can I work greases like the REAL WORLD?  Demonstration of the Grease Thief Test Stand  How to interpret Grease Compatibility results
  • 3. Mixing greases  Grease gets runny  Grease gets hard  Leaks out  Failure to lubricate  Hard as a rock  Unable to pump  Machine failure
  • 6. Compatibility Charts – BAD IDEA  Charts do not agree  Do not reference testing that was used to create them  Do not account for base oil differences  Do not account for additive differences
  • 7. Why run a Compatibility Study?  When grease mixing cannot be avoided  When its too late, the mixing has already occurred  When getting all the old grease out is impossible or impractical  Even if greases are made with the same base oil and thickener type they may be incompatible  Evaluating grease mixtures can prevent issues when supply or formulation changes have happened  If the greases are incompatible, mixing them during use could lead to significant changes in grease flow characteristics and shear behavior which would result in inadequate lubrication
  • 8. Advantages of a Compatibility Study  Allows for evaluation of mixtures without risk to equipment or affecting uptime  Can provide data to support the ability to mix greases slowly or if maintenance needs to be scheduled to change out greases  Assess risks and costs of available alternatives
  • 9. Compatibility Study– per D6185  Primary testing using three standards to evaluate grease mixtures (10:90, 50:50 and 90:10) – Dropping point by D566/D2265 – Shear stability by D217 – Storage stability by D217  If all mixtures pass primary testing or if an application requires specific evaluation secondary compatibility tests can be used for further evaluation
  • 10. Working the mixtures ASTM D6185 Proposed Change: Test Stand Mix & Work 10,000 Double Strokes in Grease Worker 72 Hours in Bearing Simulator 9 balls rotating at 1795 rpm 3.6x Ball Pass frequency Equivalent to 93 seconds of working in a typical electric motor bearing Total mixing/working events: 28,000,000
  • 11. MRG Compatibility Study– added steps  The baselines and 10:90, 50:50 and 90:10 mixtures and mixed and verified using FTIR and RDE  The baselines and mixtures and packed and worked on test stand simulator for 72 hours  Using D7718 samples are pulled, and rheological properties are evaluated for changes  Formulations are compared for additive dilution, function  Baseline formulations are compared
  • 13. Interpreting Results  To pass the mixtures need to have responses that are between the two baseline greases  Changes outside of this can cause the grease mixture to perform differently than expected