This document compares two scintillation detectors, NaI(Tl), of different sizes (2"x2" and 1"x1.5") using a cobalt-60 radioactive source. It finds that the larger crystal size (2"x2") leads to a lower probability of photons escaping and being recorded, increasing energy analysis capability. However, it also increases Compton scattering probability, reducing the net peak area relative to increased scattering. The study examines the effects of varying voltage and amplification on the energy spectra of both detectors. It finds that higher voltage and amplification increase total and scattering areas for both detectors, but reduce energy resolution. The larger detector requires higher voltage for clear spectra emergence and maintains better energy resolution at higher settings