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Preface
This manual describes the procedures for laboratory testing of road construction and
building materials carried out at Central Materials Laboratory and at construction site
Laboratory. The test procedures are in essence based on AASHTO, ASTM and British
Standard methods of Sampling and Testing.
To enhance the understanding of the testing principles and procedures, illustrative
examples, standard test data sheets, diagrams, figures, and test result reports are
included. The user is supposed to strictly follow the routine testing procedures described
in the relevant sections of the manual. Besides, it is essential to use this manual in
conjunction with the reference standards; i.e. AASHTO, ASTM and BS Standards.
Manual part I presents details of the methods for Atterberg limits, Particle size analysis,
AASHTO and unified soil classification, Moisture – Density Relationship (compaction),
the California Bearing Ratio (CBR) , Specific Gravity and In-place Density of soil-
aggregates.
This testing manual has been prepared and compiled by SABA Engineering Plc, as part
of the assignment for Consultancy Services for The Establishment of Regional
Construction Materials Testing Laboratories for 11 towns in Ethiopia. Preparation of this
soils and materials manual has been a component under the Contract Agreement signed
between the MoWUD, the implementing body on behalf of the Ministry of Capacity
Building, Public Sector Capacity Building (PSCAP) Support Project and SABA
Engineering Plc. The project is financed by the World Bank.
TABLE OF CONTENT
Page
Introduction --------------------------------------------------------------------------------------------1
Moisture Content --------------------------------------------------------------------------------------13
Atterberg Limits
Casagrande - Liquid Limit Method ----------------------------------------------------------------15
Plastic Limit -------------------------------------------------------------------------- 25
Plasticity Index ---------------------------------------------------------------------- 28
Cone Penetrometer Liquid Limit ------------------------------------------------------------------28
Soil Classification
AASHTO Soil Classification ----------------------------------------------------------------35
Unified Soil Classification ------------------------------------------------------------------44
Shrinkage Limits
Volume Metric -------------------------------------------------------------------------------- 48
Linear ------------------------------------------------------------------------------------------ 54
Amount of Material Finer than No. 200 sieve ---------------------------------------------------- 59
Standard Method of Mechanical Analysis of Soil ------------------------------------------------ 62
Hydrometer Analysis --------------------------------------------------------------------------------- 65
Specific Gravity of Soil ------------------------------------------------------------------------------- 84
Moisture Density Relationship --------------------------------------------------------------------- 91
California Bearing Ratio (CBR) -------------------------------------------------------------------- 107
In-place Density ------------------------------------------------------------------------------------- 129
1
INTRODUCTION
SOIL
1. Soil is derived from the Latin word solium. The upper layer of the earth that may be dug or
plowed specifically, the loose surface material of the earth in which plants grow. The soil is
used in the field of agronomy where the main concern is in the use of soil for raising crops.
The term soil is used for the upper layer of mantle which can support plant. The material
which is called soil by the agronomist or the geologist is known as top soil in geotechnical
engineering or soil engineering. The top soil contains a large quantity of organic matter and
is not suitable as a construction material or a foundation for structures. The top soil is
removed from the earth's surface before the construction of structures.
In soil engineering is defined as an unconsolidated material, composed of solid particles,
produced by the disintegration of rocks. The void space between the particles may contain
air, water or both. The solid particles may contain organic matter. The soil particles can be
separated by such mechanical means as agitation in water.
A natural aggregate of mineral particles bonded by strong and permanent cohesive forces is
called rock.
Soil is composed of loosely bound mineral grains of various size and shapes, organic
material, water and gases.
The bonds holding solid particles together in most soil are relatively weak in comparison to
most sound rocks. In fact and air-dried sample of soil will crumble and break down within a
relatively short period when placed in water and gently agitated.
The solid particles of which soils are composed are usually the products of both physical
and chemical action on weathering. Deposits of these weathered solid constituent may be
found near or directly above the bed rock (residual soils) or organic deposits from which they
were formed. Many soil deposits, however, have been transported from their point of origin
to new locations by such agents as water, wind, ice or volcanic action water-transported
soils are classed as alluvial (deposited by moving water on flood plains, deltos, and bars.
2
The Origin of Soil
Soils are formed by weathering of rocks due to mechanical disintegration or chemical
decomposition. when surface of a rock is exposed to atmosphere for an appreciable
time, it disintegrates or decomposes into small particles and thus the soils are formed.
Soil may be considered as an incidental material obtained from the geologic cycle
which goes on continuously in nature. The geologic cycle consist of erosion,
transportation, deposition and upheaval of soil. Exposed rocks are eroded and
degraded by various physical and chemical processes. The products of erosion are
picked p by agencies of transportation, such as water and wind and are carried to new
locations where they are deposited.
Based on the mode of origin, rocks can be divided into three basic types: igneous,
sedimentary, and metamorphic.
Igneous Rock:- are formed by solidification of molten magma ejected from the deeper
part of the earth's mantle. Molten magma on the surface of the earth cools after being
ejected by either fissure or volcanic eruption.
Sedimentary Rock:- the deposits of gravel, sand, silt and clay formed by weathering
may be come compacted by overburden pressure.
Metamorphic Rock:- is the process of changing the composition and texture of rock
(without melting) by heat and pressure.
Marble:- is formed calcite and dolomite by re-crystallization. The mineral grains in
marble are larger than those in the original rock. Quartzite a metamorphic rock formed
from quartz-rich sand stones.
Soil Structure
Soil particles may vary over a wide range. Soils are generally called gravel, sand, silt, or
clay, depending on the predominant silt of soil particles. To describe soils by their
particle size, several organizations have developed soil-separate-size limits. For the
coarse grained soils, primary structure can frequently be observed with the unaided
3
eye or a hand lens. Methods for observing the structure of fine grained soil (silts and
clays) have been slower in developing.
Water, Solids, and Air Relationships
In the case of primary structures, however, visual observations usually are insufficient,
and indirect means are employed to evaluate this factor roughly. To do this it has been
found convenient to think of any soil as being composed of three states of matter solid,
water and gas or air. Although it is impossible to make this separation into three
separate states in the laboratory, it is convenient to represent soil as shown in figure 1.
Va O
Vv
V Vw Ww W
Vs Ws
Fig. 1
2. Soil Type
A geotechnical engineer should be well versed with the nomenclature and terminology of
different types of soils. The following list gives the names and salient characteristics of
different types of soils, arranged in alphabetical order.
Black cotton Soil
Brown clay
Red clay
Gray clay
Pinkish clay
Bentonite clay
Boulders
Tuff
Desert soils
Cobbles
Gravel
Lateritic
Peat
Sand
Silt
Top soil
Expansive clays
Organic clay
Blue clay
Yellow clay
Green clay
White clay
etc.
Air
Water
Solids
2
1. Desert Soil :- Loose fine deposit sand and silt and dust particles size of the particles is
uniform in gradation.
2. Lateritic Soils :- formed by decomposition of rock, removal of base and silica, and
accumulation of iron oxide and aluminum oxide. The presence of iron oxide gives these
soils the characteristic red or pink color. These are residual soils formed from basalt.
3. Black Cotton soil :- is clay of high plasticity. Its contain essentially the clay mineral
montmorillonite. The soil has high shrinkage and swelling characteristics. The shrinkage
strength of the soil is extremely low. The soil is highly compressible and has very low
bearing capacity. It is extremely difficult to work with such soil.
4. Betonite:- it is a type of clay with a very high percentage of clay mineral montmorillnite.
It is highly plastic clay, resulting from the decomposition of volcanic ash. It is highly
plastic clay, resulting from the decomposition of volcanic ash. It is highly water
absorbent and has highly shrinkage and swelling characteristics.
5. Expansive Clay:- a large volume changes as the water content is changed. This soil
contain the montmorillonite.
6. Clay:- it consists of microscopic and sub-microscopic particles derived from the chemical
decomposition of rock. It contains a large quantity of clay minerals. It can be made
plastic by adjusting the water content. It exhibits considerable strength when dry. Clay
is a fine grained soil. It is a cohesive soil the particle size is less than 0.002mm.
7. Gravel:- gravel is a type of coarse-grained soil. The particles size ranges from 4.75mm to
75mm.
8. Cobbles:- cobbles are large size particles in the range of 75mm to 300mm.
9. Boulders:- boulders are rock fragments of large size, more than 300mm in size.
10. Peat:- it is an organic soil having fibrous aggregates of macroscopic and microscopic
particles. It is formed from vegetal matter and different plants, animals wast water under
conditions of excess moisture, such as in swamps. It is highly compressible and not
suitable of foundation.
3
11. Sand:- it is a coarse-grained soil, having 0.075 to 4.75mm size. The particles are visible
to naked eye. The sand is most of product from river.
12. Silt:- it is a fine grained soil, with particle size between 0.002 to 0.075mm the particle
size is not visible to naked eye. It has non or little plasticity and no more swelling and
cohesion less.
13. Tuff:- it is a fine-grained soil composed of very small particles ejected from volcanoes
during its explosion and deposited by wind or water.
14. Top Soil:- top soil are surface souls that support and grow plants, they contain a large
quantity of organic matter and are not suitable for foundation.
3. Soil Mechanics
Soil mechanics is the application of the laws of mechanics and hydraulics to engineering
problems dealing with sediments and other unconsolidated occultation of solid particles
produced by the mechanical and chemical disintegration of rock regardless of whether or
not they contain on admixture of organic constituents; soil mechanics is therefore, a branch
of mechanics which deals with the action of forces on soil and with the flow of water in soil.
4. Geotechnical Engineering Soil
In an applied science dealing with the applications of principles of soil mechanics to
practical problems. It has a much wider scope than soil mechanics, as it deals with all
engineering problems related with soils. It includes soil investigations, design and
construction of foundations, earth-retaining structures and earth structures.
5. Soil Engineering
Foundation:- every civil engineering structure, whether it is a building, a bridge, or a
dam, is founded on or below the surface of the earth. Foundations are required to
transmit the load of the structure to soil safely and efficiently.
4
a) Foundation is termed shallow foundation (light load) when it transmits the load to
upper strata of earth.
(A) Shallow Foundation (Footing)
Load
Column
Natural Ground Level
Soil
5
6
7
Purpose of Soil Testing
The chemical and physical properties of materials are determined by carrying out different
tests on samples of soil in a laboratory.
Tests for the assessment of engineering properties, such as moisture content, Atterberg
limits, gradation and hydrometer analysis, density, CBR, in-situ density etc.
The parameters determined from laboratory tests, taken together with descriptive data
relating to the soil, area required by soil engineers for many purposes. The more usual
applications are follows.
a) The findings of a site investigation can be supplemented by farther testing as
construction proceed
b) Criteria for the acceptance of a material used in construction
c) Data acquired from classification tests are applied to the identification of soil
of soil strata.
d) Laboratory tests are needed as part of the control measures which are applied
during construction of earth works on for ensuring that the design criteria are
met.
The advantages of laboratory testing are in a field investigation for different construction
projects, the field operations, which includes of the geology and history of the site
subsurface exploration and in place testing, are of prime importance. The determination of
the ground characteristics by in place testing can take into account large scale effects.
However the measurement of soil properties by mans of laboratory tests offers a number of
advantages, as follows:
1. A test can be run under conditions which are similar to, or which different from those
prevailing in situ, as may appropriate.
2. Test can be carried out on material (soils) which have been broken down and
reconstituted.
3. Control of the test conditions, including boundary conditions can be exercised.
4. Control can be exercised over the choice of material which is too be tested.
5. Laboratory testing generally permits a greater degree of accuracy of measurements
that does field tests.
8
The evaluation of soil properties from reliable test procedures has led to a closen
understanding of the nature and probable behavior of soils as engineering materials. Some
of the resulting advantages in the realm of civil engineering construction have been:
a) Increasing economy in the use of soils as construction materials
b) Reduction of uncertainties in the analysis of foundations and earthworks
c) Exploitation of difficult sites
d) Economies in design due to the use of lower factors of safety
e) Erection of structures, and below-ground construction, which would not have been
feasible without this knowledge.
Scope of Manual
This manual is concerned only with soil testing.
Soil Laboratory Testing
Test:- derived from Latin, testum treating or trying gold, metals and silver alloys.
Examination or trial by which the quality of anything may be determined. The process or
action of examining a substance under known conditions in order to determine its identify
or that of one of its constituents. The physical properties of materials are tested in order to
determine their ability to satisfy particular requirements.
Laboratory:- experiments in natural science.
Sample:- a relatively small quantity of material from which the quality of the mass which it
represents may be inferred.
Specimen:- a part of as representative of the whole sample.
This manual deals with standard laboratory.
- Moisture content
- Atterberg limits (LL, PL, PI, SL, LS)
- Compaction
- Classification
- California Bearing Ratio
- In-place Density
- Sieve analysis and hydrometer
9
Method of test for soil (for civil engineering purposes.)
The procedure (tests) described here are based on Standard Practice Specified in the
AASHTO, ASTM and BS (Standard). The main emphasis of the manual, however, is on the
detailed procedures to be followed in preparing samples for and carrying out different tests
in the laboratory. Appropriate to this test, details of the apparatus required, a procedural
stages, and step by step detailed procedures are included. The typical examples, calculation
and plotting of graphs and presentation of results are described.
Finally:- it is essential material testing technician requires a knowledge of good testing
techniques and an understanding of the correct procedures for the soil sample preparation
and for testing. Terminology and units are used metric (SI).
10
Soil Survey (Investigation) and Sampling
Purpose of the Soil Investigation (survey) is an essential part of a preliminary engineering
soil survey for location and design purposes. Information on the distribution of soil material
and ground-water table and conditions must be obtained before a reasonable and economic
design can detailed soil survey (investigation) provides pertinent information on the following
subject.
1. The selection of the type of surface and its design.
2. The design of the roadway section
3. The location of the road, both vertically and horizontally
4. The design and location of culvert ditches and drains.
5. The need for subgrade treatment and the type of treatment required.
6. The location and selection of borrow material for files and subgrade treatment.
7. The selection of local sources of construction materials for subbase, base course and
surfacing or wearing course.
The soil survey consists of the following:
- The exploration of the site of the road location by test pit or auger borings and the
preparation of soil profiles the significant soil layers. The critical depths to bed rock
and water table and the extent of adverse ground conditions such as swaps or peat
bogs.
- The study of all existing information on soil, and ground-water conditions occurring
in the vicinity of the proposed road location.
- The identification of the various soil types from soil profile characteristics occurring
on the proposed road project.
- The taking of representative samples of soil and local construction materials
(subbase, base course and surfacing materials) for laboratory testing.
Road site Exploration:- the field work for this phase of the soil survey consists of making
examinations of the soils by means of borings, test pits or road cuttings. Borings for
foundation should be deep enough to determine if bed rock, adverse ground (peat) or water
conditions are apt to be encountered during the construction of the proposed road. After the
boundaries of each soil type are established, sampling sites are selected so that
representative samples can be obtained for laboratory test purposes.
11
Equipment for Soil Survey
The type of equipment required for making a soil survey.
1. Ouger
2. Rod
3. Tape
4. Sample bags
5. Shovel
6. Pick
Soil sampling or selection:- sample of soil or gravel should be obtained from each soil layer
(depth) and limited distance with pick and shovel from the proposed test pit selected on the
basis of a study auger boring or test pit records. Each sample should be placed in a canvas
bag, marked with adequate identification, tied securely and shipped to the laboratory. A
sufficient amount and number of samples should be taken to establish the range in test
results for what appears to be the same soil layer.
Or soils survey should be conducted along the proposed route in order to asses the existing
pavement condition including soil extension. Construction materials subbase material
(select material source, base course material, surfacing and water should be sampled for
laboratory test determination.
12
SECTION I
1. MOISTURE CONTENT AND INDEX TESTS
1.1 Moisture Content (BS1377: Part 2: 1990 and ASTM D2216)
1. Definition
The mass of water which can be removed from the soil and aggregate by heating (oven
drying) at 105 - 1100c expressed as a percentage of the dry mass.
2. Apparatus
- Moisture can (container)
- Balance
- Oven
- Spatula
- Pan
3. Procedure
Clean and dry the moisture can (container). Make sure that all are marked the same
reference no. or letter.
a. Weigh each container and record.
b. Place the wet sample in the container, the mass of sample to be used as follows:
Mass of soil sample 50-300 gm
Mass of aggregate sample 300-500 gm
c. Weigh wet of sample + container and record
d. Place the wet sample + container in the over. Maintain the required temperature
normally 105-1100c for 12 - 24 hours.
e. Remove the sample from the oven and allow in the air to cool at least 10-15min.
f. Weigh the dried sample + container and record.
13
14
4. Calculation:-
The moisture content of a soil or aggregate is expressed as a percentage of its dry mass.
Moisture content = A - B
B - C
Where A. Weight of wet sample + Container
B. Weight of dry sample + Container
C. Weight of Container
1.2 Atterberg Limits
1.2.1 Determining the Liquid Limit of Soil (AASHTO Designation T89-90)
1. Definition:
The liquid limit of a soil is the moisture (water) content at which soil passes from the
plastic to liquid state as determined by the liquid limit test.
2. Apparatus:
a. Mixing (Evaporating dish) about 114mm diameter
b. Spatula or peel knife having blade about 76 mm length and 19 mm width
c. Motorized liquid limit device
d. Grooving tool
e. Moisture can (container)
f. Balance sensitive to 0.01gm
g. Pan (small)
h. Drying oven
i. Graduated measuring cylinder 10-50ml
3. Sample preparation
The soil sample as received sufficient from field - A sample shall be taken from the
thoroughly mixed portion of the material passing the No 40(0.425mm) sieve which
has been obtained in accordance with the standard method of preparing disturbed
soil sample or the standard method of wet preparation of disturbed soil sample for
test.
Dry preparation - Allow the sample in air to dry at room temperature or in an oven at
a temperature not exceeding 600c. Break down aggregations of particles in a mortar
15
using a rubber pestle but avoid crushing individual particles. Place in the cup or dish
a sample weighing about more than 100gm.
4. Procedure
4.1 Adjustment of Mechanical Device:-
The liquid limit device shall be inspected to determine that the device is in good
working order, that the pin connecting the cup is not worn sufficiently to permit
side play that the screws connecting the cup to the hanger arm are tight and
that a groove has not been worn in the cup through long usage. The grooving
tool shall be inspected to determine that the critical dimensions are as shown
Fig. 1.1.
By means of the gauge on the handle of the grooving tool and the adjustment
plat H, Fig 1.1, the height to which the cup is lifted shall be adjusted so that the
point on the cup which comes in contact with the base is exactly 1cm (0.3937")
above base.
The adjustment plate H shall than be well secured by tightening the screws 1.
With the gage still in place revolving the crank rapidly several times shall check
the adjustment. If the adjustment is correct, a slight ringing sound will be heard
when the cam strikes the cam follower. If the cup is raised off the gauge or no
sound is heard further adjustment shall be made. The apparatus must be clean
and the bowl must be dry and oil free. Check that the grooving tool is clean and
dry, and conforms to the correct profile.
The machine should be placed on a firm solid part of the bench so that it will
not wobble. The position should also be convenient for turning the handle
steadily and at the correct speed (two turns per second). Practice against a
second's timer with the cup empty to get accustomed to the correct rhythm.
4.2 Mixing:-
The soil sample shall be placed in the evaporating (mixing) dish and add
sufficient distilled water and mix the soil sample in the mixing dish with the
spatula for at least 10min. some soils especially heavy clay may need a longer
mixing time up to 45min. When sufficient water has been thoroughly mixed
with the soil to form a uniform mass of stiff consistency, a sufficient quantity of
16
this mixture shall be placed in the cap above the spot where the cap rests on
the base and shall then be squeezed and spread into the position shown in Fig.
1.2 with as few strokes of the spatula as possible, care being taken to prevent
the entrapping of air bubbles within the mass. With spatula the soil shall be
leveled and at the same time trimmed to a depth of 10mm at the point of
maximum thickness. The excess sample shall be returned to the mixing dish.
The sample in the cup of the mechanical device shall be divided by a firm stroke
of the grooving tool along the diameter through the centerline of the cum
follower so that a clean sharp groove of the proper dimensions will be formed. To
avoid tearing of the sides of the groove or slipping of the soil cake in the cup,
upto six strokes from front to back or from back to front counting as one stroke
shall be permitted. The depth of the groove should be increased with each
stroke and only the last stroke should scrape the bottom of the cup.
4.3 Turn the crank handle of the machine at a steady rate of two revolutions per
second, so that the bowl is lifted and dropped. Use a second's time if necessary
to obtain the correct speed. If a revolution counter is not fitted, count the
number of bumps counting aloud if necessary. Continue turning until the
groove is closed along a distance of 13mm. The back end of the standard
grooving tool serves as a length gauge. The groove is closed when the two parts
of the soil come into contact at the bottom of the groove. Record the number of
blows required to reach this condition. If there is a gap between two
17
18
19
20
Points of contact continue until there is a length of continuous contact of
13mm, and record the number of blows.
4.4 Remove a slice of soil approximately the width of the spatula extending from
edge of the soil. Followed together shall be removed and placed in two suitable
containers. The containers and samples shall be weighed and the weight
recorded.
4.5 The soil remaining in the cup shall be transferred to the evaporating dish. The
cup and grooving tool shall then be washed, clean and dried in preparation for
the next trials.
4.6 The foregoing operation shall be repeated for at least two additional portions of
the samples to which sufficient water has been added to bring the soil to a more
fluid condition. The object of this procedure is to obtain samples of such
consistency that at least one determination will be made in each of the following
ranges of blows; 1st 25-35, 2nd 20-30, 3rd 15-25.
4.7 Place all the weighed and recorded sample and container in the oven to dry [see
Section 1.1 (d-f)].
4.8 Calculation:-
The water content of the soil shall be expressed as the moisture content in
percentage of the weight the oven dried mass and shall be calculated as follows.
% Moisture content = (A-B) x 100
B-C
Where A = weight of wet sample + container
B = weight of dry sample + container
C = weight of container
4.9 Preparation of flow curve
Using a semi-logarithmic chart, plot the moisture content as ordinate (linear
scale) against the corresponding number of blows as abscissa (logarithmic scale)
and the number of blows as ordinates on the logarithmic scale. The flow curve
shall be a straight line drown as. It may be used to determine the liquid limit for
a soil with only one test; this procedure is generally called the "one point
21
method" this method has been adopted by ASTM under the designation D423-
66, Liquid limit = WN (N/25) n
Where N = number of blows in liquid limit device for 0.5in, groove closure
WN = corresponding moisture content
n = 0.121 for all soils.
The reason for obtaining fairly good results by the one point method is due to
the small range of moisture involved for N between 20 and 30.
The following table gives the values of (N)/25)0.121 for N=20 to N=30
N (N/25) 0.121
20 0.973
21 0.979
22 0.985
23 0.990
24 0.995
25 1.000
26 1.005
27 1.009
28 1.014
29 1.018
30 1.022
22
23
nearly as possible through the three or more plotted points. This is called the
flow curve.
4.10 Liquid Limit Determination:-
Draw the ordinate representing 25 blows and where it intersects the flow carve
draw the horizontal line to the moisture content axis. Read off this value of
moisture content and record it on the horizontal line to the nearest 0.1%.
Fig. 1.2 Liquid limit (Casagrande test) Result and Graph
1.2.2 Determining the Plastic Limit and Plasticity Index of Soil
(AASHTO Designation T 90-90)
Definition:-
The moisture content at which a mixture of soil passes from a liquid state to that of a
semi-solid state.
24
1. Sample Preparation
If the plastic limit analysis required take a quantity of soil weighing about 30-
50gm from the thoroughly mixed portion of the material passing the No 40
(0.425mm) sieve [see section 1.2.1 (3)].
2. Apparatus
1. Glass plate reserved for rolling of threads. This should be smooth and free
from scratches, soil and grease and about 300mm square and 10mm thick.
2. Palette knife or spatula
3. A short length 100mm length 3mm diameter of metal rod
4. Standard moisture content apparatus [section 1.2.1 (2)]
3. Procedure
- Prepare chilled or a small portion of thoroughly or mixed sample from the first
trial of LL test.
- Roll into ball
- Roll into thread until crumbling occurs.
a. Rolling into a Ball
Mould the ball between the fingers and roll between the palms of the hands so
that the warmth of the hands slowly dries it. Squeeze an ellipsoidal shape
mass. Roll this mass between the fingers and the ground glass plate with just
sufficient pressure to roll the mass into a thread of uniform diameter through
out its length. Equalize the distribution of moisture, and then form into a
thread about 6mm diameter, using the first finger and thumb of each hand.
The thread must be intact and homogenous. The pressure should reduce the
diameter of the thread from 6mm to about 1/8in or 3mm after between five
and ten back and front movements of the hand. Some heavy expansive clays
may need more than this because this type of soil tends to become harder
near the plastic limit. It is important to maintain a uniform rolling pressure
throughout: do not reduce pressure as the thread approaches 3mm diameter.
When the diameter of the thread becomes 1/8in (3mm) break the thread into
six or eight pieces. Squeeze the pieces together between the thumbs and
fingers of both hands into a uniform mass roughly ellipsoidal in shape and re-
roll. Continue this alternate rolling to a thread 1/8in. (3mm) in diameter
gathering together kneading and re-rolling, until the thread crumbles and
25
occurs surface cracks, under the pressure required for rolling and the soil can
no longer be rolled into thread. The crumbling may occur when the thread has
a diameter greater than 1/8in. (3mm). This shall be considered a satisfactory
end point provided the soil has been previously rolled into a thread 1/8in.
(3mm) in diameter. The crumbling will manifest itself differently with the
various types of soil. Some soils such as dulotancy tuff, ash etc fall apart in
numerous small aggregations of particles. Others may form an outside tubular
layer that starts splitting at both ends. The splitting progress toward the
middle and finally the thread falls apart in many small ploty particles. This
type of samples should no longer be rolled.
26
27
a. Gather the pieces together after crumbling stage is reached. Divide into two
parts and place in a suitable moisture can (container), weigh the container
and wet soil, record the weight.
Place the moisture can and wet sample in the over. Maintain the required
temperature normally 105-1100c for 12-24 hours. Remove the sample from
oven and allow in the air for about 5-10min. Weigh the dried sample and
moisture can and record.
b. Calculation
Moisture content (A-B) x 100 (plastic limit)
B-C
Refer section 1.2.1 (4.8)
1.2.3 Plasticity Index
The difference between the liquid limit and plastic limit is calculated to give the
plasticity index (PI).
Eg. Plasticity Index (PI) = Liquid Limit (LL, PL) Plastic Limit (PI).
(If LL=40 and PL=21, then PI=40-21=19)
28
1.3 Liquid Limit - With Cone Penetrometer
1.3.1 General
This method is used for determining the liquid limit of soil. It is based on the
measurement of penetration into the soil of a standardized cone of specified mass. At
the liquid limit the cone penetration is 20mm, it requires the same apparatus as is
used for bituminous material testing but fitted with a special cone.
1.3.2 Apparatus
1. A flat glass plate, of convenient size, 10mm thick and about 500mm square.
2. Spatulas or palette knives.
3. Cone for the penetrometer, stainless steel or duralumin with smooth polished
surface, length approximately 35mm, cone angle 300, sharp point mass of cone
and sliding shaft 80g±0.1g.
4. Sharpness gauge for cone, consisting of a small steel plate 1.75mm ±0.1mm thick
with a 1.5mm±0.02mm diameter hole accurately drilled and reamed.
5. Metal cups of brass or aluminum alloy 55mm thick and 40mm deep.
6. Metal straight edge about 100mm long.
7. Moisture content apparatus.
8. An evaporating dish (mixing dish), about 150mm diameter.
9. Wash bottle or beaker, containing distilled water.
1.3.3 Sample preparation
a. Use of Natural Soil:-
When the soil consists of clay and silt with little or no material retained on a
No.40 (0.425mm) sieve, it can be prepared for testing from its natural state.
Take a representative sample of about 500g of soil and chop into small pieces or
shred with cheese grater. Mix with distilled water on a glass plate, using two
palette knives. During this process remove any coarse particles by hand or with
tweezers. Mix the water thoroughly into the soil until a thick homogeneous paste
is formed and the paste has absorbed all the water with no surplus water visible.
The mixing time should be at least 10min. with vigorous working of the palette
knives. A longer mixing time period up to 45min may be needed for some soils,
which do not readily absorb water.
29
Place the mixed soil in an airtight container, such as a sealed polythene bag, and
leave to mature for 24 hours. A shorter maturing time may be acceptable for low
plasticity clays, and very silty soils could be tested immediately after mixing. If in
doubt, comparative trial tests should be performed. In a laboratory with a
continuous workload it is good practice to be consistent and allow 24 hours
maturing for all soils.
The mixed and matured materials is then ready for the tests.
b. Wet preparation :-
Take a representative sample of the soil at its natural moisture content to give at
least 350gm of material passing the No.40 (0.425mm) sieve. This quantity allows
for a liquid limit and a plastic limit test. Chop into small pieces or shred with a
cheese grater, and place in a weighed beaker, weigh and determine the mass of
soil m(g) by difference.
Take a similar representative sample and determine its moisture content w(%).
The dry mass of soil in the test sample mD(g) can then be calculated from the
equation:.
mD = 100m
100+w
Add enough distilled water to the beaker to just submerge the soil. Break down
the soil pieces and stir until the mixture forms slurry. Nest a No. 40 (0.425mm)
sieve on a receiver, under a guard sieve eg. No 10 (2mm) sieve if appropriate. Pour
the slurry through the sieve or sieves, and wash with distilled water, collecting all
the washings in the receiver. Use the minimum amount of water necessary, but
continue washing until the water passing the No. 40 (0.425) sieve runs virtually
clear. Transfer all the washings passing the sieve to a suitable beaker with out
losing any soil particles.
Collect the washed material retained on the sieves. Dry in the oven and determine
the dry mass mR(g).
Allow the soil particles in the beaker to settle for several hour, or overnight. If
there is a layer of clear water above the suspension, this may be carefully poured
or siphoned off, without losing any soil particles. However if the soil contains
30
water-soluble salts which might influence its properties, do not remove any water
accept by evaporation.
Stand the container in a warm place or in a current of warm air, so that it can
partially dry. Protect from dust. Stir the soil water mixture frequently to prevent
local over-drying. Alternatively, excess water may be removed by filtration. When
the mixture forms a stiff paste such that the penetration of the cone penetrometr
would not exceed 15mm the soil is ready for mixing on the glass plate as
described above. No additional curing time is required and the material is ready
for the tests.
Calculate the percentage by dry mass of soil in the original sample passing the
0.425mm sieve (Pa) from the equation
Pa = mD - mR x 100
mD
c. Dry preparation:-
Allow the soil sample to air dry at room temperature, or in one oven a
temperature not exceeding 500c [see section 1.2.1(3)].
1.3.4 Procedure
a. Take a sample of about 300gms-soil paste and place the prepared soil paste on
the glass plate.
b. Mix the soil paste on the glass with the spatulas for at least 10-min. Some soil
especially heavy clays may need a longer mixing time. If necessary add more
distilled water so that the first cone penetration reading is about 15mm.
c. Press the mixed soil paste into the cup with a palette knife (spatula) taking care
not to trap air. Strike off excess soil with the straight edge to give a smooth level
surface.
d. Lock the cone shaft unit near the upper end of its travel and lower the supporting
assembly carefully so that the tip of the cone is within a few mms of the surface of
the soil in the cup. When the cone is in the correct position, a slight movement of
the cup will just make the soil surface. Lower the stem of the dial gauge to
contact the cone shaft and record the reading of the dial gauge to the nearest
0.1mm.
31
32
e. Release (Allow) the cone by pressing the button for a period of 5±1 second timed
with a seconds timer or watch. If the apparatus is not fitted with an automatic
release and locking device, take care not to jerk the apparatus during this
operation. After 5 seconds release the button so as to lock the cone in place.
Lower the dial gauge stem to make contact with the top of the core shaft without
allowing the pointer sleeve to rotate relative to the stem adjustment knob. Record
the reading of the dial gauge to the nearest 0.1mm Record the difference between
the beginning and end of the drop as the cone penetration. See Fig. 1.3.
f. Lift out the cone and clean it carefully to avoid scratching.
g. Add a little distilled water and remix and add a little more wet soil to the cup,
taking care not to trap air, make the surface smooth. Repeat section 1.3.3(d). If
the second cone penetration differs from the first by less than 0.5mm, the average
value is recorded, and proceed to the next h.
h. If the second penetration is between 0.5 and 1mm different from the first, a third
test is carried out provided that the overall range does not exceed 1mm, the
average of the three penetrations is recorded and the content is measured stage
(1).
i. If the overall range exceeds 1mm, the soil is removed from the cup and re-mixed
and the test is repeated from stage C.
j. Take a moisture content sample of about not less than 10g, the area penetrated
by the cone, using the tip of a small spatula. Place it in a suitable container and
determine its moisture content.
k. The soil remaining in the cup is re-mixed with the rest of the sample on the glass
plate together with a little more distilled water, until a uniform softer consistency
is obtained. The cup is scraped out with the square-ended spatula wiped clean
and dried, and stages (C-J) are repeated at least three more times, with further
increments of distilled water.
33
34
A range of penetration values from about 15mm to 25mm should be covered,
fairly uniformly distributed.
1. Calculation
The moisture content of the soil from each penetration reading is calculated
from the wet and dry weightings as in the moisture content [see section 1.2.1
(4.8)].
Moisture content (%) = (A-B) x 100
B-C
Where A = weight of wet sample + container
B = weight of dry sample + container
C = weight of container
Test Results
From the graph the moisture content corresponding to a standard cone penetration
of 20mm is read off to the nearest 0% reported to the nearest whole number as the
liquid limit. See Fig. 1.3
1.4 Choice I General Soil classification
1.4.1 General:-
The American Association of State Highway and Transportation Official (AASHTO)
system of soil classification is based upon the observed field performance of soil
under highway pavements and is widely known and used among highway engineers.
1.4.2 Definition:-
Soil classification is systematically grouping or categorizing of soil. It provides a
common language to express briefly the general characteristics of soils.
1.4.3 Procedure:-
The AASHTO soil classification system is classified into seven (7) major groups A-1
through A-7. Soils classified under groups A-1, A-3 and A-2 are granular (gravels,
sand and gravelly clay). Materials with 35% or less passing through a No.200
(0.075mm) sieve. The silt and silty clay materials with more than 35% passing the
No.200 (0.075mm) sieve are classified under groups A-4, A-5, A-6 and A-7. After the
necessary laboratory tests have been preformed the proper classification for a given
material can normally be made without great difficulty. The classification of a specific
35
soil is based upon the results of tests made in accordance with standard methods of
soil testing. To classify a soil by Table 1.1 one must proceed form left to right with the
required test data available by the process elimination. The first group from the left
into which the test data will fit gives the correct classification. To evaluate the
performance quality of a soil as a highway subgrade material under this system, a
number called the group index is included with the groups and sub-groups of the
soil. The group index of a soil may range from 0-20 and is expressed as a whole
number. The approximate subgrade and base performance quality of a given soil is
inversely proportional to its group index, and it can be expressed by the following
empirical relation.
Group index (GI) = (F-35%) [0.2+0.005 (LL-40)]+0.01(F-15)(PI-10)
Where GI = group index
F = percentage of soil passing a No 200 (0.075mm) sieve
LL = liquid limit
PI = plasticity index
The group index is rounded off to the nearest whole number. The group index may
also be evaluated with Fig. 1.4 by adding the vertical reading, the vertical reading is
obtained from the two charts:
 Chart one LL with No. 200 (0.075mm)passing sieve and
 Chart two PI with a No. 200 (0.075mm) passing sieve.
Add the two values.
1.4.4 Classification
Parameters
1. Liquid Limit
2. Plasticity Index
3. Grain Size Analysis
Note:- Detail Soil Classification
General
A-1, A-3, A-2, A-4, A-5, A6 and A-7
1. Granular Materials and Sand: 35% or less passing a No.200
(0.075mm) sieve are A-1, A-3 and A-2.
36
Soil Group A-1 material
divided into two subgroups
Sieve
size
%
passing
LL PI
A-1
A-1-a
No. 10
No. 40
No. 200
50max
30max
15max
- 6 max
A-1-b
No. 40
No. 200
50max
25max
- 6 max
2. Soil Group A-3 Material
Sieve Size % Passing LL PI
A-3
No. 40 51 min
NP NP
No. 200 10 max
3. Soil Group A-2 Material
Soil Group A-2
material divided into
four subgroups
Sieve
size
%
passing
LL PI
A-2
A-2-4 No.200 35 or less 40 max 10max
A-2-5 No.200 35 or less 41 min 10max
A-2-6 No.200 35 or less 40 max 11 min
A-2-7 No.200 35 or less 41 min 11 min
2. Silt and Silty Clay or Heavy Clay Materials: 35% or more passing No.
200 (0.075mm) sieve are A-4, A-5, A-6, and A-7.
4. Soil Group A-4 Material
Sieve
Size
%
Passing
LL PI
A-4 No.200 36 min 40 max 10 min
5. Soil Group A-5 Material
Sieve
Size
%
Passing
LL PI
Soil Group A-5 No.200 36 min 41 max 10 min
37
6. Soil Group A-6 Material
Sieve
Size
%
Passing
LL PI
A-6 No.200 36 min 40 max 11 min
7. Soil Group A-7 Material
Sieve
Size
%
Passing
LL PI
A-7 A-7-5 No.200 36 min 41 min 11 min
A-7-6 No.200 36 min 41 min 11 min
Group of soil A-7-5 is plasticity Index result less or equal Liquid Limit – 30 (PI less or
equal to LL-30)
Group of soil A-7-6 is plasticity Index result greater than Liquid Limit result -30 (PI less
than LL-30)
38
39
Example:- 1
Liquid Limit = 42
Plasticity Index = 12
Passing No 200 (0.075mm) sieve = 35
Soil classification is A-2-7 (1).
Example:- 2
Liquid Limit = 60
Plasticity Index = 30
Passing No 200 (0.075mm) sieve = 36
Soil classification is A-7-5 (5).
Example:- 3
Liquid Limit = 49
Plasticity Index = 22
Passing sieve No 200 (0.075mm) = 38
Soil classification is A-7-6 (4).
Example:- 4
Liquid Limit or Plasticity Index is NP.
Passing sieve No 200 (0.075mm) = 36
Soil classification is A-4 (0).
1.4.5 Soil Fractions
1. Over size (Boulders) - Material retained on 3 inch (75mm) sieve. They should be
excluded from the portion of a sample to which the classification is applied but
the percentage of such material should be recorded.
2. Gravel - Material passing sieve with 3inch (75mm) and retained on the No 10
(2mm) sieve.
3. Coarse Sand - Material passing the No. 10 (2mm) sieve and retained on No. 40
(0.425mm) sieve.
4. Fine Sand - Material passing the No. 40 (0.425mm) sieve and retained on the No
200 (0.075mm) sieve.
40
5. Silty Clay - Material passing the No. 200 (0.075mm) sieve. The word silt is applied
to a fine material having a PI of 10 or less and the term clay is applied to fine
material having a PI of more than 10.
1.4.6 Description of Classification Groups
A. Granular Materials
- Group A-1 - Well graded mixtures of stone fragments or gravel ranging from
course to fine with non-plastic or slightly plastic silt binder.
- Subgroup A-1-a - Stone fragments and sandy gravel some times with silt.
- Subgroup A-1-b - Stone fragments and gravel with some times clayey silt.
- Group A-3 - fine sands and non-plastic silt.
- Group A-2 - sandy gravel with silt and gravelly clay.
- Subgroup A-2-4- and A-2-5- include various granular materials and sandy
clayey silt.
- Subgroup A-2-6 and A-2-7 include materials similar to those described
under subgroups A-2-4 and A-2-5 except that the fine portion contains
plastic clay having a higher PI.
41
3. choice II-Soil Classification
Definition:- soil classification is systematically grouping or categorizing of soil. It provides a
common language to express briefly the general characteristics of soils
A. AASHTO Soil Classification System: is classified into 7 major groups A-1 through A-7
classified and under groups A-1, A-3, A-2, A-4, A-5, A-6, A-7 soils. Under groups A-1, A-
2 and A-3 are granular or gravelly clay and sand materials with 35% or less passing
through a No. 200 (075mm) sieve.
The silt and clay materials with more than 35% passing the No 200 (075mm) sieve are
classified under groups A-4, A-5, A-6 and A-7.
AASHTO Classification Parameters
1. Liquid Limit
2. Plasticity index
3. Grain size analysis
Group A-1 A-2 and A-7 material divided into 4 and 2 sub groups.
A-1
A-1-a
A-1-b
A-2 materials are divided into 4 sub groups.
A-2
A-2-4
A-2-5
A-2-6
A-2-7
 A-1 material can be used for surfacing, base course and subbase.
 A-2 material for subbase and subgrade.
 A-4,5,6 and 7 subgrade only.
A-7 material is divided into two sub groups
A-7
A-7-5
A-7-6
42
A-7-5 Group of Soil Material:- PI is equal to or less than LL-30
A-7-6Group of Material:- PI is greater than LL-30
Examples
LL PI
Passing Sieve (mm)
Soil Classification
2 0.425 0.075
1 42 12 - - 36 A-7-5 (1)
2 70 30 - - 39 A-7-5 (5)
3 30 10 - - 10 A-2-4 (0)
4 41 20 - - 45 A-7-6 (5)
5 NP 20 15 3 A-1-a (1)
A-1 Material:- Stone fragments, gravelly and coarse sand with binder of low plasticity
or NP.
A-2 Materials:- gravelly silt, clay and sand with low and little high plastic material
A-3 Material:- Sand
A-4,5,6 & 7 Materials:- Silty clay and Same fines with few gravel
B. Silty Clay Soil Materials
- Group A-4 - The typical material of this group is fine sandy and silty clay sometimes
non-plastic material, liquid limit not exceeding 40 and PI not exceeding 10.
- Group A-5 - The typical material of this group is similar to that described under
group A-4, except that it is usually of diatomaceous or micaceous character and may
be highly elastic as indicated by the high liquid limit.
- Group A-6 - This typical material is a plastic clay soil. The group includes also
mixture of fine clayey soil and the Plasticity Index may be high.
- Group A-7 - The typical materials and problems of this group are similar to those
described under group A-6 except that they have the liquid limit and the range of
group index values is 1 to 20 with increasing values indicating the combined effect of
increasing liquid limits and plasticity indexes and decreasing percentages of coarse
material.
- Subgroup of A-7-5 - includes those materials with moderate plasticity index in
relation to liquid limit and which may be highly elastic as well as subject to
considerable volume change.
43
- Subgroup of A-7-6 - includes those materials with high plasticity indexes in relation
to liquid limit and which are subject to extremely high volume change.
 Highly organic soils such as peat and muck are not included in this classification.
1.5 Unified Soil Classification System
General
Unified classification system is widely used. This system is an out growth of the Airfield
classification developed by casagrande and is utilized by the corps of engineers. In this
system, soils fall within one of three major categories: curse grained, fine grained and
highly organic soils. These categories are further subdivided into 15 basic soil groups.
The following group symbols are used in the unified system.
G - gravel O - organic
S - sand W - well graded
M - silt P - poorly graded
C - clay U - uniformly graded
Pt - peat L - low liquid limit
H - high liquid limit
Combinations of above letters are used to identify the soils. For expamle, SP is a sand
that is poorly graded and CL and CH indicate clays with low and high liquid limits
respectively.
The essentials of unified classification system are given in Table 1.5.1 and
characteristics pertinent of roads and air fields are sown in Table 1.5.2.
A. Soil components in the unified classification system are as follows:
- Cobbles - above 75mm (3 inch)
- Gravel - 75mm to 4.75mm (3inch - No.4) sieve
- Coarse sand - 4.75mm to 2mm (No 4 - No. 10) sieve
- Medium sand -2mm to 0.425 mm (No 10 to No 40) sieve
- Fine sand - 0.425 mm to 0.075mm (No 40 to No 200) sieve
- Fine silt and clay - passing 0.075mm (0.075) sieve.
44
B. Laboratory test specified for silts and clays are the determination of the liquid limit
and the plastic limit and plasticity index.
C. Laboratory test for coarse-grained soils is based on the grain size analysis. Coarse-
grained materials are those containing 50% or less passing 0.075 mm (No.200) sieve.
Fine grained are those with more than 50% passing 0.075mm (No.200) sieve.
After determining its grain size distribution, liquid limit and plasticity index, the soil
can be classified using table 1.2 and Fig 1.4.
The minus 0.075mm (No. 200) sieve material is "silt" if non-plastic and the liquid
limit and plasticity index plot below the "A" line on the plasticity chart (Fig. 1.4) and
"clay" if plastic and the liquid limit and plasticity index plot above the "A" line. This
holds true for inorganic silts and clays and organic silts, but not for organic clays
since they plot below the "A" line. The "A" line is an arbitrarily drawn line on the
plasticity chart of Fig. 1.4.
The letters in parentheses stand for symbols by which each group is known.
A. Coarse Grained Symbols
GW-GM, GP-GM,_GW-GC, GP-GC, SW-SM, SW-SC, SP-SM
B. Fine Grained Soil Classification with Symbols
ML, MI, MH, MV, ME, CL, CI, CH, CV, CE
In Ethiopian practice this chart is divided into five zones, giving the following
categories for clays and silts.
1. Clays of low plasticity (CL) less than 35, liquid limit or silts of low plasticity (ML)
less than 35 liquid limit.
2. Clays or silts of medium plasticity (CI) or (MI), liquid limit from 35 to 50.
3. Clays or silts of high plasticity (CH) or (MH), liquid limit from 50 to 70
4. Clays or silts of very high plasticity (CV) or (MV), liquid limit from 70 to 90
5. Clays or silts or extremely high plasticity (CE) or (ME), liquid limit exceeding 90.
45
Example
Liquid Limit = 72
Plasticity Index = 36
Passing No. 200 sieve = 98
Classification is according to the chart (Fig. 1.5.2) = MV. The soil is MV group.
46
47
48
1.6 Determining the Shrinkage Factors and Limit of Soils
1. Scope
This procedure furnishes data from which the following soil characteristics may by
calculated:
(a) Shrinkage Limit
(b) Shrinkage Ratio
(c) Volumetric change
(d) Linear shrinkage
A. Determination of Volumetric Shrinkage
2. Apparatus
2.1 Evaporating (mixing) dish about 150mm diameter.
2.2 Spatula or peel knife having a blade above 76mm long and 20mm wide.
2.3 Glass cup about 57mm diameter and 38mm deep with rim ground flat.
2.4 Prong plate, glass or clear acrylic, fitted with three non-corrodible prongs.
2.5 Glass plate, large enough to cover the shrinkage dish.
2.6 Measuring cylinder 25 to 100ml.
2.7 Mercury, rather more than that will fill the glass cup.
2.8 Straight edge, spatula, small tools.
49
2.9 Balance 3000g capacity reading to 0.01g.
2.10 Moisture content can (container).
2.11 Large tray containing a small amount of water to retain any spilled mercury.
2.12 Vaseline
3. Sample preparation
Receive sufficient sample from field prepare. About 50g of soil sample passing the
0.425 (No. 40) sieve from natural soil and place the prepared sample in the mixing
dish or cup.
50
51
4. Procedure
4.1 Place the prepared soil sample in an evaporating dish and thoroughly mix with
distilled water to make into a readily workable plate. Air bubbles must not be
included. The moisture content should be somewhat greater than the liquid
limit. The consistency should be such as to require about 10 blows of the
Casagrande liquid limit apparatus to close the groove or to give about 25-28mm
penetration of the cone penetrometer.
Add the mixed soil paste to the shrinkage dish so as to fill it about one-third.
Avoid trapping of air. Tap the dish on the smooth surface bench surface to
cause the soil to flow to the edges of the dish. This should also release any small
air bubbles present. The bench should be padded with a few layers of blotting
paper or similar material.
Add a second amount of soil, about the same as the first and repeat the tapping
operation until all entrapped air has been released. Add more soil and continue
tapping, so that the dish is completely filled with excess standing out. Strike off
the excess with a straight edge and clean off adhering soil from the outside.
Immediately after the above, weigh the sample (soil) and dish to 0.01g. Record
as m1.
4.2 Drying
Allow the sample in the dish to dry in the air for at least 12 hours or 24 hours
until its color changes from dark to light. Place it in oven at 600c for 6 hours
and continue at 105 - 1100c and dry to constant mass.
If the shrinkage curve during drying is required, make a series of volume
measurement at suitable intervals before drying in the oven. Leave the soil in
the shrinkage dish exposed to warm air, and when it has shrunk away from the
dish and can be safely handled, determine its volume and mass. Place the soil-
pat on a flat surface to dry further and repeat the measurements until the color
changes from dark to light. Then dry in the oven.
52
4.3 Weighing Dry Mass
Cool in a dessicatoor or in air and weigh the dry soil and dish or container to
0.01g. Record ad md.
4.4 Measurement of Volume
Remove the dried soil-pat carefully from the shrinkage dish. It should be intact
and be kept long enough to dry in air before transferring to the oven.
Place the glass cup in a clean evaporating dish standing on the large tray. Fill
the cup to overflowing with mercury, and remove the excess by pressing the
glass prong plate firmly on top of the cup. Avoid trapping air under the glass
plate. Carefully remove the prong plate, and brush off any mercury drops
adhering to the glass cup. Place the cup into another lean evaporating dish
without spilling any mercury. Place the soil-pat on the surface of the mercury
press the three prongs of the prong plate carefully on the sample so as to force
it under the mercury Fig… Avoid trapping any air; press the plate firmly on to
the dish. Displaced mercury will be filled in the evaporating dish. Brush off any
droplets of mercury adhering to the cup into the dish. Transfer all the displaced
mercury to the measuring cylinder and record its volume (Vd). This is equal to
the volume of the dry soil-pat.
4.5 Measure the dish volume and weight. Clean and dry the shrinkage dish and
weigh it to 0.01g (m2). Its internal volume is determined by measuring the
volume of mercury held. Place the dish in on evaporating dish and fill it to
overflowing with mercury. The evaporating dish will catch the overflow. Place
the small glass plate firmly over the top of the shrinkage dish so that excess
mercury is displaced, but avoid trapping any air. Remove the glass plat carefully
and transfer the mercury to the 25ml-measuring cylinder. Record the volume of
mercury in ml, which is the volume of the shrinkage dish (V1).
53
4.6 Calculations
Calculate the moisture content of the initial wet soil-pat, w1 from the equation.
Moisture content (w1) = (M1-Md) x 100
Md
Dish No. A B C
Wt of dish + wet soil (m1)
Wt of dish + dry soil (m2)
Wt of dish (m1)
Wt of water (m1-m2) (m4)
Wt of wet soil (m1-m3) (m6)
Volume of dish (V1)
Volume of dry soil (V2)
Volume Change (V1-V2) (V3)
Shrinkage limit (Ws) can then be calculated from the equation,
Moisture content (Wo) = (m1-m2) x 100
m5(m2-m3)
Where V1 = volume of wet soil (dish)
V2 = volume of dry soil-pat
m5 = mass (wt) of dry soil
The shrinkage ratio, Rs, can be calculated from
Rs = ms
V2
SABA Engineering Plc.
P.O.Box 62668 Addis Ababa, Ethiopia. Tel. 34 10 65/34 16 17/34 30 04 Fax.. 34 12 30/34 16 17
E-mail sava.eng@telecom.net.et
54
SHRINKAGE LIMIT TEST (VOLUMETRIC)
Lab No.
Dish No. A B C
A. Wt. of dish and wet soil 48 47.5 48.2
B. Wt. of dish and dry soil 36 35.8 36
C. Wt. of dish 10 9 10
D. Wt. of water (A-B) 12 11.7 12.2
E. Wt. of dry soil (B-C) 26 25 26
F. Volume of dish 13 10.8 13
G. Volume of displaced mercury 8 6.4 8
H. Volume of change cc (F-G) 5 5 5
I. D – H 7 6.7 7.2
Shrinkage Limit (I/E) x 100 26.9 26.8 27.7
Shrinkage Ration (E/G) 3.25 3.91 3.25
55
b. Linear Shrinkage
Definition:-
This test gives the percentage linear shrinkage of a soil. It can be used for soils of low
plasticity, including silts, as well as for clays.
1. Apparatus
1.1 Non-corrodible metal mould (Brass), 140mm long and 25mm in diameter
1.2 Flat glass plate as for the liquid limit test
1.3 Palette knives
1.4 Petroleum jelly
1.5 Vernier calipers
1.6 Moisture content apparatus
2. Procedure
2.1 Preparation of mould:-
Clean and dry the mould. Apply a thin film of Vaseline or petroleum jelly to the
inner surfaces to prevent soil from sticking.
2.2 Preparation of sample
About 200g of soil sample passing 0.425mm (No.40) sieve is prepared from soil.
This proportion of the original sample passing the 0.425mm (No.40) sieve is
recorded.
Place the soil in the mixing dish and mix thoroughly with distilled water, as the
liquid limit test. Continue mixing until it becomes a smooth homogenous paste
at about the liquid limit. This is not critical, but it may be checked by using the
cone penetrometer, which should give a penetration of about 20mm.
56
2.3 Place the paste in the mould, avoiding the trapping of air as far as possible, so
that the mould is slightly over filled. Tap it gently on the bench to remove any air
pockets. Level (trim) off along the top edge of the mould with a spatula or
straight edge. Wipe off any soil adhering to the rim of the mould.
2.4 Leave the mould and soil exposed to the air but in a draught-free position so
that the soil can dry slowly.
When the soil has shrunk away from the walls of the mould, it can be
transferred to an oven set at 600c. When shrinkage has virtually ceased,
increase the drying temperature to 105 - 1100c to complete the drying.
2.5 Allow the mould and soil to cool in a dessicator, measure the length of the bar of
soil with the caliper, making two or three readings and taking the average (LD).
If the specimen is curved during drying, remove it carefully from the mould and
measure the lengths of the top and bottom surfaces. Take the mean of these two
lengths as the dry length as (LD).
57
If the specimen has fractured in one place, two portions can be fitted together
before measuring the length. If it has cracked badly, and the length is difficult to
measure, repeat the test using a very slower drying rate leaving the sample and
mould longer in air (about more than 24 hours) before transferring to the oven.
2.6 Calculation
Calculate the linear shrinkage (LS) as a percentage of the original length of the
specimen from the equation,
LS = (1-LD) x 100
LO
Where: LO = original length of the mould
LD = length of dry specimen
Linear Shrinkage Limit
Inician Length (Lo) - wet
Final Length (Ld) - dry
SL = Lo - Ld x 100
LD
Results
The Linear Shrinkage of the soil is reported to the nearest whole Number
58
. AMOUNT OF MATERIAL FINER THAN NO.200(0.075mm) SIEVE
IN AGGREGATE
AASHTO DESIGNATION T-11
1. Scope
This method of test covers a procedure for the determination of the quantity of aggregate
finer than a standard No. 200 (0.075mm) sieve by washing.
This procedure may not determine the total amount of material finer than the No. 200
(0.075mm) sieve. Such a determination may be made by combining washing and dry sieving
as required in the sieve analysis of fine and coarse aggregate.
2. Apparatus
1.1 Sieves - No. 16 and No. 200 (0.075) sieves. The sieves shall be of woven wire-cloth
construction, conforming to the requirements of AASHTO Designation M-92.
1.2 Container - a pan or vessel of a size sufficient to contain the sample, when covered
with water, and to permit vigorous agitation without an advertent loss of any art of the
sample or water.
1.3 Balance - A balance with a capacity of 2000gm and sensitive to 0.1gm.
1.4 Scale - A heavy duty scale with a capacity of at least 50 lb and sensitive to 0.1 lb.
1.5 Drying Oven - an oven capable of maintaining a uniform temperature of 230 ± 90F.
2. Test Sample
The test sample shall be selected from material which has been thoroughly mixed and which
contains sufficient moisture to prevent segregation. Representative samples shall weigh,
after drying, not less than the amount indicated in the following table.
59
Maximum Sieve Size Minimum Sample (Mass)Weight
No. 4 500gm
3/8 inch 1000gm
¾ inch 2500gm
1 ½ inch or over 5000gm
60
3. Test Procedures
Dry the test sample to constant weight (± 16 hours) at a temperature of 230±90F, and
weigh the sample to the nearest 0.1 percent.
Place the sample in a suitable container, and cover the sample with water. Agitate the
contents of the container by vigorous stirring with a large spoon or rod, and pour the
wash water over the nested sieves, arranged with the No. 200 sieve on the bottom. The
agitation should be sufficiently vigorous so that all particles finer than the No. 200 sieve
are brought into suspension and are subsequently washed through the nested sieve. Be
careful to avoid loss of the coarser particles. Repeat this washing operation until the
wash water is clear.
If the material consists of clay, it may be advantageous to let is soak 16 to 20 hours and
to add a detergent to assist deflocculation.
In the case of soil samples, it is often advantageous to separate the sample on the No. 4
sieve. The material passing the No.4 sieve may be washed as outlined above. The
material passing the No. 4 sieve may be washed as outlined above or by means of a
suitable mechanical washing device.
Return all material retained on the nested sieves to the washed sample. Dry the sample
to constant weight (± 16 hours) at a temperature of 230±90F, and weight the sample to
the nearest 0.1 percent.
Pan - drying shall be permissible when oven - drying is impracticable or impossible.
However, in no case shall a sample be heated in excess of 2390F.
4. Calculation
The percentage of material finer than the No. 200 sieve shall be calculated as follows:
F = W - W1 x 100
W
Where F = the percent of material finer than the No. 200 sieve.
W = the original dry weight of the sample
W1 = the dry weight of the sample after washing.
5. Precautions
The No. 200 (0.075) sieve is extremely delicate, and should be handled accordingly. In no
event should wire brushes be used on this sieve.
Take care to avoid loss of sample material during washing and during transfer of
material from the nested sieves to the washed sample.
61
Standard Method of Mechanical Analysis of Soils
AASHTO DESIGNATION T88 - 57
1. Scope
This method describes a procedure for the quantitative determination of the distribution
of particles size in soils.
2. Apparatus
The apparatus shall consist of the following:
Balance - A balance sensitive to 0.1gm for weighing small samples; for large samples, the
balance is to be sensitive to within 0.1 percent of the weight of the sample to be tested.
Stirring apparatus - a mechanically operated stirring apparatus consisting of an electric
motor suitability mounted to turn a vertical shaft at a speed not less than 10,000
revolutions per minute without load, a replaceable stirring paddle made of metal, plastic or
hard rubber similar to the design shown in Figure 1, and a dispersion scup conforming to
either of the designs shown in Figure 2.
(Alternate b) Dispersing Device - An air - jet type dispersing device similar to
either of the designs shown in Figure 3.
Hydrometer - A hydrometer of the exact size and shape shown in Figure 4, the body of
which has been blown in a mold to assure duplication of all dimensions, and equipped with
either scale a or scale B. Scale A shall be graduated form -5 to +60 gm of soil per liter, and
hydrometers equipped with this scale shall be identified as 152H. It shall be calibrated on
the assumption that distilled water has a specific gravity of 1.000 at 680F and that the soil
in suspension has a specific gravity of 2.65. Scale B shall be graduated from 0.995 to 1.038
specific gravity and calibrated to read 1.000 in distilled water at 680F (200c). Hydrometers
equipped with this scale shall be identified as 151H.
A glass graduate 18 inches in height, 2 ½ inches in diameter, and graduated for a
volume 1000ml.
Thermometer - A Fahrenheit thermometer accurate to 10F (0.50c).
Sieve - A series of sieves of square mesh woven wire cloth, conforming to the
requirements of standard specifications for sieves for Testing purposes (AASHTO
Designation: M92). The sieves required are as follows:
62
2 inch sieve (50mm)
1 ½ inch sieve (37.5mm)
1 inch sieve (25mm)
¾ inch sieve (20mm)
3/8 inch sieve (10mm)
No. 4 sieve (4.75)
No. 10 sieve (2mm)
No. 40 sieve (0.425)
No. 200 sieve (0.075mm)
Water Bath or Constant Temperature Room
A water bath or constant temperature room for maintaining the soil suspension at
a constant temperature during the hydrometer analysis. A satisfactory water bath
is an insulated than which maintains the suspension at a convenient constant
temperature as near 680F (20.00c) as the room and faucet water temperature will
permit. Such a device is illustrated in Figure 5. In cases where the work is
performed in a room at an automatically controlled constant temperature, the
water bath is not necessary and subsequent reference to a constant temperature
bat shall be interpreted as meaning either a water bath or a constant temperature
room.
Beaker - A beaker of 250 ml Capacity
3. Sample
The sample required for this test shall include all of the material on the No. 10 (2,000
micron) sieve, plus a 60 or 110gm representative portion of the fraction passing the No. 10
sieve, the larger quantity being required only when this fraction is very sandy. These
samples shall be obtained in accordance with the Standard method of Dry Preparation of
Disturbed Soil Samples Test (AASHTO DESIGNATION: T87), or the Standard Method of Wet
Preparation of Disturbed Soil Samples for test (AASHTO DESIGNATION: T146).
4. Sieve Analysis of Fraction Retained on No. 10 sieve
The portion of the sample retained on the No. 10 sieve shall be separated into a series of
sizes by the use of the 2 inch, 1 ½, 1 ½ - inch, 1 - inch, ¾ - inch, 3/8 - inch, and the
No. 4 sieve.
63
The sieving operation shall be conducted by means of a lateral and vertical, accompanied
by jarring action so as to keep the sample moving continuously over the surface of the
sieve. In no case shall fragments in the sample be turned or manipulated through the
sieve by hand. Sieving shall be continued until not more than 1 percent by weight of
the residue passes any sieve during 1 minute when sieving machines are used, their
thoroughness of sieving shall be tested by comparison with hand methods of sieving as
above described.
The portion of the sample retained on each sieve shall be weighed and the weight
recorded although it shall be permissible to record the accumulated weights as the
contents of each successive sieve is added to the fractions previously deposited on the
scales pan.
64
HYDROMETER AND SIEVE ANALYSIS OF FRACTION PASSING
THE NO.10 SIEVE
5. Hygroscopic Moisture
A 10gm portion of the fraction of the sample passing the No.10 sieve shall be used for the
determination of the hygroscopic moisture. The portion of the sample shall be weighed, dried
to constant weight in an oven at 1100c (2300F), weighed, and the results recorded.
6. Dispersion of Soil Sample
Approximately 50 grams of most soil or 100 grams of very sandy soils shall be taken from
the fraction passing the No. 10 sieve by use of a riffle sampler, weighed, placed in a 250ml,
breaker, covered wit 125ml of stock solution of the selected dispersing agent, stirred
thoroughly with a glass rod, and allowed to soak for a minimum of 12 hours. Any of the four
dispersing agents listed in Table 1 may be used.
The stock solution shall be prepared by dissolving the quantity of the salt given in the table
in sufficient distilled water to make a liter of solution. After soaking, the contents of the
beaker shall be washed into one of the dispersion cups shown in Figure 2, distilled water
added until the cup is more than half full, and the contents dispersed for a period of 1
minute in the mechanical stirring apparatus.
7. Alternate Method for Dispersion
The representative soil sample shall be weighed and placed in a 250ml beaker, covered
with 125ml of the stock solution of the selected dispersing agent specified in section 6,
and allowed to soak for a minimum of 12 hours.
The air jet dispersion apparatus shall be assembled as shown in fig 3 without the cover
cap in place. The needle value controlling the fine pressure shall be opened until the
pressure gauge indicates one pound per square inch air pressure. The initial air
pressure is required to prevent the soil water mixture from entering the air - jet
chamber when the mixture is transferred to the dispersion cup. After the apparatus is
adjusted, the soil water mixture shall be transferred from the beaker to the dispersion
cup, using a wash bottle to assist in the transfer operation.
65
The volume of the soil - water mixture in the dispersion cup shall not exceed 250ml. The
cover containing the baffle late shall be placed upon the dispersion cup and the needle
value opened until the pressure gauge reads 20 pounds per square inch. The soil -
water mixture shall be dispersed for 5, 10 or 15 minutes depending upon the plasticity
index of the soil. Soils with a PI of 5 or less shall be dispersed from 5 minutes; soils
with a PI between 6 and 20 for 10 minutes; and soils with a PI greater than 20 for 15
minutes. Soils containing large percentages of mica need be dispersed for 1 minute
only.
After the dispersion period is completed, the needle value shall be closed until the
pressures gauge indicates one pound per square inch. The cover shall be removed and
all adhering soil particles washed back into the dispersion cup. The soil-water
suspension shall then the washed into the 1000ml glass graduate and the needle value
closed.
66
8. Hydrometer Test
After dispersion, the mixture shall be transferred to the glass graduate and distilled
water having the same temperature as the constant temperature bath added until the
mixture attains a volume of 1000ml. The graduate containing the soil suspension shall
then be placed in the constant temperature bat. When the soil suspension attains the
temperature of the bath, the graduate shall be removed and its contents thoroughly
shaken for 1 minute, the palm of the hand being used as a stopper over the mouth of
the graduate.
At the conclusion of this shaking, the time shall be recorded, the graduate placed in the
bat, and readings taken with the hydrometer at the end of 2 minutes. The hydrometer
shall be read at the top of the meniscus formed by the suspension around its stem. If
hydrometer with scale A is used, it shall be read to the nearest 0.5gm/liter. Scale B
shall be read to the nearest 0.0005 specific gravity. Subsequent readings shall be
taken at intervals of 5, 15, 30, 60, 250, and 1440 minutes after the beginning of
sedimentation. Readings of the thermometer placed in the soil suspension shall be
made immediately following each hydrometer reading and recorded.
67
68
69
After each reading the hydrometer shall be very carefully removed from the soil
suspension and placed with a spinning motion in a graduate of clean water. About 25
or 30 seconds before the time for a reading, it shall be taken for a clean water, and
slowly immersed in the soil suspension to assure that it comes to rest before the
appointed reading time.
9. Sieve Analysis
At the conclusion of the final reading of the hydrometer, the suspension shall be washed on
a No.200 (74 micron) sieve. That fraction retained on the No.200 sieve shall be dried and a
sieve analysis made, using the following sieves: No.40, No.60 and No. 200.
CALCULATIONS
10.Percentage of Hygroscopic Moisture
The hygroscopic moisture shall be expressed as a percentage of the weight of the oven-dried
soil and shall be determined as follows:
Percentage of hygroscopic moisture = W - W1 x 100
W1
Where W = weight of air - dried soil, and
W1 = weight of oven - dried soil
To correct the weight of the air - dried sample for hygroscopic moisture, the given value shall
be multiplied by the expression.
100 __
100 + percentage of hygroscopic moisture
11.Coarse Material
The percentage of coarse material shall be calculated from the weight of the fractions
recorded during the sieving of the material retained on the No.10 sieve, in accordance
with section 4, and the total weights recorded during the preparation of the sample, in
accordance with the Standard Method of Dry Preparation of Disturbed Samples for
Tests (AASHTO DESIGNATION: 87).
The percentage of coarse material retained on the No.10 sieve shall be calculated as
follows: From the weight of the air - dried total sample, subtract the weight of the air -
70
dried total sample, subtract the weight of the oven - dried fraction retained on the
No.10 sieve. The difference is assumed to equal the weight of the air dried fraction
passing the No.10 sieve (Note 1).
NOTE 1: According to this assumption no hygroscopic moisture is contained in the air
- dried particles retained on the No.10 sieve, when as a matter of fact a small
percentage of moisture may be present in this fraction. This amount of
moisture, compared with that held in the pores of the fraction passing the
No.10 sieve is relatively small. Therefore, any error produced by the
assumption as stated may be considered negligible in amount.
The weight of the fraction passing the No.10 sieve shall be corrected for hygroscopic
moisture as indicated in section 10. To this value shall be added the weight of the oven -
dried fraction retained on the No.10 sieve to obtain the weight of the total test sample
corrected for hygroscopic moisture. The fractions retained on the No.10 and coarser sieves
shall be expressed as percentages of this corrected weight.
12.Percentage of Soil in Suspension
Hydrometer readings made at temperatures other than 680F shall be corrected by
applying the appropriate composite correction from one of the following tables. Tables
151H and 152H list composite correction for hydrometer 151H and 152H to account
for the different dispersing agents, temperature variations from 680F, (20.00c), and
height of meniscus on the stem of hydrometer.
The percentage of the dispersed soil is suspension represented by different corrected
hydrometer readings depends upon both the amount and the specific gravity of the soil
dispersed. The percentage of dispersed soil remaining in suspension shall be calculated
as follows:
For hydrometer 152H, P = Ra x 100
W
Where : p = Finer
R = Corrected hydrometer reading
W = Mass of dry soil
a = Constant depending on the density of the suspension
71
72
73
For hydrometer 151H, P = 1606 (R - 1)a x 100
W
Where, P = Percentage of originally dispersed soil remaining in suspension
R = Corrected hydrometer reading
W = Weight in grams of soil originally dispersed minus the hygroscopic
moisture and
a = Constant depending on the density of the suspension.
For an assumed value of G for the specific gravity of the soil, and water density of
1.000 at 680F (20.00c), the value "a" may be obtained by the formula.
A = 2.6500 - 1.000 x G
2.6500 G-1.0
The value of "a", given to two decimal places are shown in table 2.
TABLE 2 - Values of a, for different specific gravities
Specific Gravity, G Constant, a
2.95 0.94
2.85 0.96
2.75 0.98
2.65 1.00
2.55 1.02
2.45 1.05
2.35 1.08
Table 151H and 152H
It is sufficiently accurate for ordinary tests to select the constant for the specific gravity
nearest to that of the particular soil tested.
To convert the percentages of the soil in suspension to percentages of the total test
sample including the fraction retained on the No.10 sieve, the percentage of originally
dispersed soil remaining in suspension shall be multiplied by the expression.
100 - Percentage retained on No.10 sieve
100
74
13.Diameter of soil particles in suspension
The maximum diameter, d, of the particles in suspension, corresponding to the
percentage indicated by a given hydrometer reading, shall be calculated by the use of
stocks' law.
According to stocks law:
d = √ 30nL
980(G - G1)T
Where d = maximum grain diameter in millimeters
N = Coefficient of viscosity of the suspending medium (in the case water)
in poises varies with changes in temperature of the suspending
medium.
L = distance in cm through which soil particles settle in a given period of
time.
T = time in minutes, period of sedimentation
G = specific gravity of soil particles and
G1 = specific gravity of the suspending medium (approximately 1.0 for
water)
The maximum grain diameter in suspension for assumed conditions and corresponding
to the periods of sedimentation specified in this procedure are given in Table 3. These
grain diameters shall be corrected for the conditions of test applying the proper
correction factors as described and explained below.
Table 3: Maximum Grain Diameter in Suspension under Assumed Conditions
Time (Min.) Max Grain Diameter (Mm)
2 0.040
5 0.026
15 0.015
30 0.010
60 0.0074
250 0.0036
1440 100015
75
The grain diameters given in Table 3 are calculated according to the following
assumptions:
L, the distance through which the particles fall is constant and equal to 17.5cm
n, the coefficient of viscosity equals 0.01005 poise, that of water at 680F.
G, the specific gravity of the soil is constant and equal to 2.65.
Figure 6
The grain diameter corrected for other than the assumed conditions shall be obtained by
the formula.
D = d' X KL XDGXDa
Where in d = corrected grain diameter in mm
d' = grain diameter obtained from table 2
KL = correction factor obtained from figure 6. When the hydrometer
reading not adjusted for composite correction is used for the ordinate
reading
Kg = correction factor obtained from figure 7A.
Kn = correction factor obtained from figure 7B.
The coefficient Kg and Ka are independent of the shape and position of the hydrometer
and are as shown in Figures 7A and 7B.
Figure 7A and 7B
14.Fine Sieve Analysis
The percentage of the dispersed soil sample retained on each of the sieves in the sieve
analysis of the material washed on the No.200 shall be obtained by dividing the weight
of fraction retained on each sieve by the over-dry weight of the dispersed soil and
multiplying by 100.
The percentage of the total test sample, including the fraction retained on the No.10
(2000 microns) sieve, shall be obtained by multiplying these values by the expression.
76
100 minus the percentage retained on No.10 sieve
100
77
78
15. Plotting
The accumulated percentages of grains of different diameters shall be plotted on semi
logarithmic paper to obtain a "grain size accumulation curve," such as that shown in figure
8.
Figure 8
16. Report
16.1 The results, read from the accumulation curve, shall be reported as follows:
a) Particles larger than 2mm Percent
b) Coarse sand, 2.0 to 0.42mm Percent
c) Fine sand, 0.42 to 0.074mm Percent
d) Silt, 0.074 to 0.005mm Percent
e) Clay, smaller than 0.005mm Percent
f) Colloids, smaller than 0.001mm Percent
16.2 The results complete mechanical analysis furnished by the combined sieve and
hydrometer analysis shall be reported as follows.
SIEVE ANALYSIS
Sieve Size Percent Passing
2inch (50mm)
1 ½ inch (37.5mm)
1 inch (25mm)
¾ inch(20mm)
3/8 inch (10mm)
No.4 (4.75mm)
No.10 (2mm)
No.40 (0.425mm)
No.200 (0.075mm)
79
HYDROMETER ANALYSIS
Smaller than Percent
0.02mm
0.005mm
0.001mm
For materials examined for any particular type of work or purpose, only such fractions
shall be reported as are included in the specification or other requirements for the
work or purpose.
SABA Engineering Plc.
P.O.Box 62668 Addis Ababa, Ethiopia. Tel. 34 10 65/34 16 17/34 30 04 Fax.. 34 12 30/34 16 17
E-mail sava.eng@telecom.net.et
80
Mechanical Analysis
1. Sieve Analysis
Sieve Site
(mm)
Weight
retained gm
% Retained % Passing
75 -
63.5 -
50 -
37.5 -
25 600 23.83 76
20 480 19.06 57
12.5 360 14.3 43
9.5 278 11.04 32
4.7 260 10.33 21
2 60 2.38 19
Pan 480 19.06
Total 2518 100
2. Specific gravity = 2.67
3. Hygroscopic Moisture
a) Wt. of wet sample = 50
b) Wt. of dry sample = 48
c) % dry sample b/a x 100 = 96
Coputed dry Wt. cxa = 48gm
100
4. Sample Pass 2mm
Sieve Weight Retain % Retained % Passing
0.425 10 20.83 15.0
0.250 8 16.7 12
0.075 6 12.5 9.5
81
2. Hydrometer (152H)
Observed
time
Sedimentation
Min (Elapsed
time)
Hydrometer
Reading
Temp.
0F/0c
Diameter
mm
Corrected
Reading 680F
% finer
P=Ra/w*100
Diameter
mm
0 70
2 27 70 0.0395 20.5 42.52
5 25 70 0.0256 18.5 38.37 0.02
15 23 70 0.0148 16.5 34.22
30 20 71 0.0101 13.7 28.41
60 17 71 0.00692 10.7 22.19 0.005
250 15 71 0.00354 8.7 18.04 0.002
1440 12 70 0.00144 5.5 11.41 0.001
3. Report
A B
1. Particles larger than 4.75mm 76% b. Smaller than % passing
2. Coarse sand 4.75-0.425mm 10% 0.02mm 7.2
3. Fine sand 0.425-0.075mm 5% 0.005mm 4.2
4. Silt 0.075-0.002mm 6.50% 0.001mm 2.2
5. Clay smaller than 0.002mm 2.50%
82
83
SPECIFIC GRAVITY OF SOILS
AASHTO DESIGNATION: T 100 - 75 (1982)
(ASTEM DESIGNATION: d 854 - 58 (1972))
1. SCOPE
1.1This method of test is intended for determining the specific gravity of soils by means of a
pycnometer. When the soils is composed of particles larger than the 4.75mm (No.4)
sieve, the method outlined in the Standard Method of Test for Specific Gravity and
Absorption of Coarse Aggregate (AASHTO T 85) shall be followed. When the soil is
composed of particles both large and smaller than the 4.75mm sieve, the sample shall be
separated on the 4.75mm sieve and the appropriate method of test used on each portion.
The specific gravity value for the soil shall be the weighted average of the two values.
When the specific gravity value is to be used in calculations in connection with the
hydrometer portion of the Standard Method of Mechanical Analysis of Soils (AASHTO 88)
it is intended that the specific gravity test be made on that portion of the soil which
passes the 2.00mm (No.10) or 0.425mm (No.40) sieve, as appropriate.
2. DEFINITION
2.1Specific Gravity - Specific gravity is the ration of the mass in air of a given volume of a
material at a stated temperature to the mass in air of an equal volume of distilled water
at a stated temperature.
3. APPARATUS
The apparatus shall consist of the following:
Pycnometer - Either a volumetric flask having a capacity of at least 100ml or a
stoppered bottle having a capacity of at least 50ml (Note 1). The stopper shall be
of the same material as the bottle, and of such size and shape that it can be easily
inserted to a fixed depth in the neck of the bottle, and shall have a small hole
through its center to permit the emission of air and surplus water.
Note 1 - The use of either the volumetric flask or the stoppered bottle is a matter
of individual preference, but in general, the flask should be used when a larger
sample that can be used in the stoppered bottle is needed due to maximum grain
size of the sample.
84
Balance - Either a balance sensitive to 0.01g for use with the volumetric flask,
or a balance sensitive to 0.001g for use with the stoppered bottle.
Desiccator - A desiccator, about 8 in. (approximately 200mm) in diameter
containing anhydrous sillca gel or other suitable desiccant.
Oven - A thermostatically controlled drying over capable of maintaining a
temperature of 110±5c (230±90F).
Thermometer - A thermometer covering the range of 0-500c (32 - 1220F),
readable and accurate to 10c (20F).
4. GENERAL REQUIREMENTS FOR WEIGHING
4.1When the volumetric flask is used in the specific gravity determination all masses shall
be determined to the nearest 0.01g. When the stoppered bottle is used in the specific
gravity determination all masses shall be determined to the nearest 0.001g.
5. CALIBRATION OF PYCNOMETER
The pycnometer shall be cleaned, dried, weighed, and the mass recorded. The
pycnometer shall be filled with distilled water (Note 2) essentially at room temperature.
The mass of the pycnometer and water, Wa, shall be determined and recorded. A
thermometer shall be inserted in the water and its temperature Ti determined to the
nearest whole degree.
NOTE 2 - Kerosene is a better wetting agent than water for most soils and may be used
in place of distilled water for oven - dried samples.
From the mass W1 determined at the observed temperature Ti a table of vales of masses
Wa shall be prepared for a series of temperatures that are likely to prevail when
masses Wb are determined later (Note 3). These values of Wa shall be calculated as
follows:
Wa (at Tx) = density of water at Tx X (Wa (at Ti) - Wf) + Wf
Density of water at Ti
Wa = mass of the pycnometer and water, in grams
Wf = mass of pycnometer, in grams
Ti = observed temperature of water, in degrees Celsius, and
Tx = any other desired temperature, in degrees Celsius.
85
NOTE 3 - The method provides a procedure that is most convenient for laboratories
making many determinations with the same pycnometer. If no equally applicable to a
single determination, bringing the pycnometer and contents to some designated
temperature when masses Wa and Wb are taken, requires considerable time. It is
much more convenient to prepare a table of masses Wa for various temperatures likely
to prevail when masses Wb are taken. It is important that masses Wa and Wb be based
on water at the same temperature. Values for the relative density of water at
temperatures form 18 to 300c are given in table 1.
6. SAMPLE
The soil to be used in the specific gravity test may contain its natural moisture or be
oven - dried. The mass of the test sample on an oven - dry basis shall be at least 25g
when the volumetric flask is to be used, and at least 10g when the stoppered bottle is
to be used.
Samples containing natural moisture - When the sample contains its natural moisture,
the mass of the soil, Wo, on an oven - dry basis shall be determined at the end of the
test by evaporating the water in an oven maintained at 110±50c (230±90F) (Note 4).
Samples of clay soils containing their natural moisture content shall be dispersed in
distilled water before placing in the flask, using the dispersing equipment specified in
AASHTO T 88.
Oven - Dried Samples - When an oven - dried sample is t be used, the sample shall be
dried for at least 12h, or to constant mass Vo±50c (230±90F) (Note 4), transferred to
pycnometer and weighed. The sample shall then be soaked in distilled water for at least
12h.
NOTE 4 - Drying of certain soils at 1100c may bring about loss of moisture of
composition or hydration, and in such cases drying shall be done, if desired, in
reduced air pressure and at a lower temperature.
7. PROCEDURE
The sample containing natural moisture shall be placed in the pycnometer, care being
taken not to lose any of the soil in case the mass of the sample has been determined.
Distilled water shall be added to fill the volumetric flask about three - fourths full on
the stoppered bottle about half full.
Entrapped air shall be removed by either of the following methods:
86
1. By subjecting the contents to a partial vacuum (air pressure not exceeding 100mm
of mercury) or
2. By boiling gently for at least 10min. while occasionally rolling the pycnometer to
assist in the removal of the air. Subjection of the contents to reduced air pressure
may be done either by connecting the pycnometer directly to an aspiration or
vacuum pump, or by use of a bell jar. Some soils boil violently when subjected to
reduced air pressure. It will be necessary in those cases to reduce the air pressure
at a slower rate or to use a larger flask samples that are heated shall be cooled to
room temperature.
The pycnometer shall then be filled with distilled water and the outside cleaned and
dried with a clean dry cloth. The mass of the pycnometer and contents, Wb, and the
temperature in degrees Celsius, Tx, of the contents shall be determined, as described
in section 4. (Note 5)
NOTE 5 - The minimum volume of slurry that can be prepared by dispersing
equipment specified in AASHTO T88 is such that a 500ml flask is needed as
pycnometer.
8. CALCULATION AND REPORT
8.1 The specific gravity of the soil, based on water at a temperature Tx, shall be calculated
as follows:
Specific Gravity, Tx/TxC = Wo
Wo + (Wa + Wb)
Where Wa = mass of sample of oven - dry soil, in grams
Wa = mass of pycnometer filled with water at temperature Tx (Note 6), in grams
Wb = mass of pycnometer filled with water and soil at temperature Tz, in grams and
Tx = temperature of the contents of the pycnometer when weight Wb, was
determined, in degrees Celsius.
NOTE 6 - This value shall be taken from the table of values of Wa prepared in
accordance with 5.1 for the temperature prevailing when mass Wb was taken.
8.2 Unless otherwise required, specific gravity values reported shall be based on water at
200c. The value based on water at 200c shall be calculated from the value based on
water at the observed temperature Tx, as follows:
87
Specific gravity, Tx/200c = KX specific gravity, Tx/Tx0c, where:
K = a number found by dividing the relative density of water at temperature Tx by the
relative density of water at 200c. Values for a range of temperatures are given in Table
1.
8.3 When it is desired to report the specific gravity value based on water at 40c, such a
specific gravity value may be calculated by multiplying the specific gravity value at
temperature Tx by the relative density of water at temperature Tx.
8.4 When any portion of the original sample of soil is eliminated in the preparation of the
test sample, the portion of which the test has been made shall be reported.
Table 1 Relative Density of water and conversion factor K for various temperatures
Temperature,
0c
Relative Density of
Water
Correction Factor K
18 0.9986244 1.0004
19 0.9984347 1.0002
20 0.9982343 1.0000
21 0.9980233 0.9998
22 0.9978019 0.9996
23 0.9975702 0.9993
24 0.9973286 0.9991
25 0.9970770 0.9989
26 0.9968156 0.9986
27 0.9965451 0.9983
28 0.9962652 0.9980
29 0.9956761 0.9977
30 0.9956780 0.9974
88
Specific Gravity - Calculation of Soil
Bottle No. A B
W1 - Weight of Bottle 16 18
W2 - Weight of Sample 10 10
W3 - Weight of bottle + sample + water 40.2 40.3
W4 - Weight of Bottle full of Water 34 34.1
V - Volume of bottle (W4 + W2) - W3 3.8 3.8
GS - Specific Gravity W2
V
2.632 2.632
89
SECTION II
I. Moisture - Density Relationship
Theory
Compaction (degree of compaction)
Soil is the process where by soil particles are constrained to pack more closely together
through a reduction in air voids. The object in compacting soil is to improve its
properties and in particular to increase its strength and bearing capacity reduce its
compressibility and decrease its ability absorb water due to reduction in volume of voids.
Development of test procedures by R.R. proctor in 1993 in the USA in order to
determine a satisfactory state of compaction for soils being used in the construction of
roads air ports and dams. The test made use of a hand rammer and a cylindrical mold
with a volume of 1/30 cuff. At that time it was believed that the proctor test represented
in the laboratory the state of compaction which could be reasonably achieved in the field.
A laboratory test using increased energy of compaction was then necessary to reproduce
these higher compacted densities, so a test was introduced which used a heavier rammer
with the same mold. These procedures became known as the modified AASHTO T-180
test.
1. DEFINITIONS of the following
a. Compaction:- The process of packing soil particles more closely together, usually by
rolling, ramming or mechanical means, thus increasing the dry density of soil.
b. Moisture - Dry density relationship:- The relationship between dry density and
moisture content of a soil.
c. Optimum Moisture Content (OMC):- The moisture content of a soil at which a
specified amount of compaction will produce the max. dry density.
d. Max. dry density:- the dry density optioned using a specified amount of compaction
at eh Opt. M. C.
e. Percentage air void ( va):- the volume of air voids in a soil expressed as a
percentage.
f. Saturation line (zero air voids line):- the line on a graph showing the dry density-
moisture content relationship for a soil compacting no air voids.
g. Relative compaction (% (compaction):- the percentage ratio of the dry density of
the soils to its max compacted dry density determined by using a specified amount of
compaction (Lab max dry density and field dry density.
90
h. Standard proctor:- light compaction, for light traffic road compaction by using 5.5 lb
rammer and 3 layer compaction.
i. Modified proctor:- heavy compaction for heavy Load construction (axle load)
compaction by using 10 lb rammer and 5 layer compaction.
2. Compaction Process:- the solid soil particles are paced more closely together by
mechanical means. This process must not be confused with consolidation, in which
water is squeezed out under the action of a continuous static load. The air voids can not
be eliminated altogether by compaction, but with proper control they can be reduced for
a minimum. At low moisture content the soil grains are surrounded by a thin film of
water, which tends to keep the grins a part even when compacted. The finer soil grains
the more significant is this effect. If the moisture content is increased the additional
water enables the grains to be more easily compacted together, some of the air is
displaced and the dry density is increased. The addition of more water, up to a certain
point, enables more air to be expelled during compaction. At that point the soil grains
become as closely packed together as they can be (i.e. the dry density is at the
maximum) under the application of this compactive effort when the amount of water
exceeds that required to achieve this condition, the excess water begins to push the
particle apart or water takes more spaces, so that the dry density is reduced. At higher
moisture contents little or no more air is displaced by compaction, and the resulting dry
density continues to decrease.
3. Sample preparation:- the method of preparation of test samples from the original
(received from field) soil sample depends up on.
3.1 The largest size of stone (particles) present in the original sample.
3.2 Whether or not the soil particles are susceptible to crushing during compaction is
assessed by inspection, or by passing the soil through sieves in the gravel-size range
the amount of coarse materials determines the size of mold to be used i.e. whether
4" or 6" dia mold should be used.
If breakdown of particles results in a change in the soil characteristics, and it a single
batch of soil is compacted several times that change will be progressive during the
test. A separate - batch of susceptible soil is needed for each determination of
compacted dry density, consequently a much larger sample is required.
91
Cohesive soils should be broken down into small pieces before to be ready for
compaction.
4. Mass of sample for test:- the mass of sample to be prepared for the tests.
For each determination with 4"(102mm) diameter of mold about (2.5kg) for with
6"(152.4mm) diameter of mold about 6kg.
The amount of sample before riffling.
If gravel more than 75kg
If clay about 30-50kg
For subsequent determination, adjust the moisture condition of the samples as follows
To obtain a lower m/c allow the soil sample to partially air/dry do not allow the soil to
dry more than necessary.
Place the soil in an air tight container if it is not to be used immediately. For a cohesive
soil, leave it in the container for a maturing period of at least 24 hours to allow for a
uniform distribution of water in the sample.
5. For multiple sample batches:- subdivide the prepared sample to give 5 or more
representative specimens for test. Each specimen should be of about 2.5kg for 4" dia and
6kg for 6" diameter of mold.
6. Stone content sample:- particles larger than 19.5mm which are removed before test
may consist of gravel, fragments of rock and other hard material, and are collectively
referred to bellow as stone. The soil actually tested is called the matrix material (pass
19.5mm) four categories of soil are recognized, depending on the largest sizes of particles
remaining after initial preparation. These categories relate to the following test methods.
Method A and B material retained on 4.75mm sieve is removed and no correction is
made, if the amount of retained material is 7% or more by mass. Method "c" is
recommended instead.
Method "C" coarse grained material passing on a 19mm sieve and removed retained
material, and no correction is made. However if the amount of retained material is 10%
or more, Method "D" is recommended instead.
92
Method "D" the amount of material retained on the 19.5mm sieve is from 10% to 30%
the retained material on a 75mm sieve and discard the material retained on that 75mm
sieve. Replace the material between 75mm sieve by an equal mass of similar material
taken from an unused portion of the sample, passing 75mm sieve and retained on
4.75mm sieve mix in the replaced material thoroughly.
Choice.2 If the % retained material on 19mm sieve is 10-30%
Mass of sample for one batch = 6kg
6kg x 30% = 1. 8 of retained on 4.75mm sieve
And passing material on 19.5mm sieve is = 6 - 1. 8 = 4.2kg.
Mix the retained on 4.75mm sieve and passing on 19mm sieve (4.2+1. 8) = 6kg
If the amount of material retained in the 19mm is more than 30% the rest methods for
the determination of density or compaction is not applicable.
Mold for Compaction:- Method "A" and "C" the 4"(102mm) diameter of mold compaction
mold is used for method "D" the 6" (152.4mm) diameter compaction mold is used
Summary
Method "A" fine grained (102mm) diameter mold material passing 4.75mm sieve
Method B-6" (152mm) diameter mold material passing 4.75mm sieve fine grained
Method C-4" (102mm) diameter mold material passing 19mm sieve coarse grained
Method D-6" (152mm) diameter mold material passing 19mm sieve coarse grained
7. Compaction Effort:- the procedure used for various types of compaction are
summarized below.
A. Standard Proctor - Method "A" or "C"
Rammer weight 5.5lb (2.5kg)
Height (lift) of rammer 12" (30.8cm)
No. of blows 25
Layers 3 this test is knows as light compaction
Method "B" or "D"
Diameter of mold 6" (2.5)
Rammer weight 5.5lb (2.5kg)
Height (lift) of rammer 12"
No. of blows 56
93
Layer 3
B. Modified Proctor
Method "A" or "C" = Diameter of mould = 4"
Weight of rammer = 10lb (4.5kg)
Height (lift) of rammer = 18"
No of blows = 25
Layer = 5
Method "B" or "D" = Diameter of mould = 4"
Weight of rammer = 10lb (4.5kg)
Height (lift) of rammer = 18"
No of blows = 56
Layer = 5 this test is known as heavy
compaction
Summary
Methods Layer
No. of
blows
Wt of rammer
lb/kg
Height
Volume of
Mold cuft
A - C 3 25 5.5/2.5 12 1/30
A - C 5 25 10.0/4.5 18 1/30
B - D 3 56 5.5/2.5 12 1/13.13
B - D 5 56 10/4.5 18 1/13.13
The mechanical energy applied in each type of test in terms of the work done in
operating the rammer is derived and compared below.
A. Light compaction = rammer wt x lift of rammer x No of blows x layer
Volume of mold
Eg. (5.5 lb x (12") x 25x3 =
1/30 ft3.
Compared with:-
5.5 lb x (12") x 56x3 =
1/13.13 ft3.
94
B. Heavy compaction
10 lb x (18") x 25x5 =
1/30 ft3.
10 lb x (18") x 56x5 =
1/13.13 ft3.
8. Apparatus
1. Mold
2. Rammer
3. Measuring cylinder
4. 19 and 4.75mm sieves
5. Metal tray
6. Balance
7. Sample extruder (extracting)
8. Trimming knife (straightedge)
9. Drying oven
10.Moisture tine (can)
9. Test procedures
9.1 Check that mold, extension collar and base plate are clean and dry
9.2 Weigh the mold body to the nearest 1g sensitive balance
95
96
97
98
99
100
9.3 Measure its internal diameter and height of the mold and calculate internal volume
of the mold (v)
V = IID2H
4
9.4 Check that the lugs or clamps hold the extension and base plate securely to the
mold and assemble them together
9.5 Wipe with a slightly oily cloth on the internal surfaces
9.6 Check the rammer to ensure that it falls freely through the correct height of drop,
and that the lifting knob is secure.
9.7 Place the assembled mold on a solid base (concrete floor)
9.8 Prepare the sample as described in section 3 and weigh to provide the single sample
of about 2.5kg or 6kg and put in the mixing large tray and adjust the moisture
content to desired starting value (add that calculated or estimated water) and mix
thoroughly.
101
9.9 Add loose sample to the mold and compact the sample by applying 25 or 56 blows
of the rammer dropping from the controlled height and weight of 5.5lb/12"H or
10lb/18"H. Make sure that the end of the tube is resting on the soil surface, and
does not catch on the edge of the mold, before releasing the rammer. The guide
tube must be held vertically. Place the tube gently on the sample surface, the
rammer does the compaction not the tube. If the correct amount of sample has
been used, the compacted surface should be at about one-third of the height of the
mold body that is about 7.7cm for 4"(102mm) diameter and 9cm for 6" diameter
mold below the top of the mold body, or 127mm for the 4" diameter. mold and for 6"
mold 142mm diameter. Below the top of the mold extension collar. If the level
differs significantly from this remove the sample, break it up, mix it with the
remainder of the prepared material and start this stage again. After completed the
1st layer of compaction lightly scarify the surface of the compacted sample with the
spatula or point of a knife. Place a second, equal layer of soil in the mold, and
compact with 25 or 56 blows as before. Repeat with a third or up to 5th layer, which
should then bring the compacted surface in the extension collar to not more than
6mm above the level of the mold body. If the soil level is higher than this, the result
will be in accurate, so the sample should be removed, broken up and re-mixed, and
the test repeated with slightly less soil in each layer.
9.10 Carefully remove the extension collar. Cut away the excess sample and level (trim
off) to the top of the mold. Any sample cavity resulting from removal of small
fragments at the surface should be filled with fine material, well pressed in and
should be checked with the straight-edge.
9.11 Weigh sample and mold immediately
9.12 Remove the soil from mold by using sample extruder on jack. Break up the sample
on the tray.
102
103
9.13 Moisture Content Determination:- take representative sample in moisture tin or
containers from the middle of the molded specimen, weigh immediately and put in
the oven to dry.
Note: Amount of sample for moisture content determination
If it is clay or fine grained material not less than 100g and for coarse grained or
gravel not less than 500g.
9.14 Thoroughly break up the remaining portion (material) of the molded specimen and
the remainder of the prepared sample on the mixing tray, by rubbing until it will
pass through 19.5mm for coarse grained or 4.75mm for fine grained material as
judged by eye. Add an increment of sufficient water, to increase the moisture
content of the soil by 1 to 2% of water to 2.5kg for 4" dia mold or 6kg for 6" dia
mold of soil.
Note: For sandy and coarse grained soil about 1-%
For clay or silty clay 2-4% of water to 2.5kg or kg of soil.
Mix in the water thoroughly.
9.15 Repeat the above procedure (stages 8 to 9) for each increment of water added,
continue this series of determination until there is either a decrease or no change in
the wet (bulk) unit weight or mass of sample and mold (after compaction).
9.16 Calculation
9.16.1 Bulk density (wet), p = M2 - M1, g/cc
V
Where: m1 = weight of mold
m2 = weight of mold + sample
9.16.2 Moisture content
a. wt of wet sample + container
b. wet of dry sample + container
c. wt of container
moisture content, W0 = (a - b) * 100%, (W0,%)
b - c
9.16.3 Bulk Density (Wet), p = M2 - M1, g/cc
V
Where: m1 = weight of mold
m2 = weight of mold + sample
104
9.16.4 Dry Density, pd = p*100, g/cc
W0 + 100
9.17 Plot of Dry Density, Pd, against the corresponding Moisture Content
Draw a smooth curve through the points. The curves for "0" or some points air
voids may be plotted as well as certain the point of max dry density (MDD) on this
curve, and read off the maximum dry density value. The MDD value may lie
between tow plotted points, but the peak should not be exaggerated when drawing
the curve. Read off the corresponding moisture content, which is the optimum
moisture content (OMC).
Zero Air Void Line:- Va = wGs
1 + wGs
105
106
107
108
SECTION III
CALIFORNIA BEARING RATIO (CBR)
1. Definition:- CBR or bearing ration of the force required to penetrate a piston (plunger) of
3inch2 or 1936mm2 cross section in to soil in a mold at a rate of 1mm/min to that
required for similar penetration into a standard sample of compacted crushed rock or
lime.
The ration is determined at penetrations of 2.5 (0.1") and 5mm (0.2") value is used.
2. Historical Development and Principle California Bearing Ration (CBR): The basic
testing procedure employed in the determination of the California bearing ratio was
developed by the California division of highways around 1930, and has since been
adopted and modified by numerous states, the USA corps of engineers and many
countries of the world in 1961 the American society for testing and materials adopted the
modified as ASTM designation D 1883. Bearing ratio of laboratory competed soils.
The CBR is a comparative measure of the shearing resistance of a soil. This test consists
of measuring the load required the course a plunger of standard size to penetrate a soil
specimen at a specified ratio.
The CBR is the PSI or Mpa required to force a piston in to the soil, a certain depth
expressed as percentage of the load, PSI, required to force the piston the same depth in
to a standard sample of crushed rock, usually depths of 2.5mm or 5mm are used
penetration loads for bearing value is known as the California bearing ratio which is
generally abbreviated to CBR.
This test method is intended to provide the relative bearing value or CBR, of sub-grade
sub-base course materials procedures are gives for Laboratory compacted specimens of
swelling, non swelling and granular materials.
3. Tests on Laboratory- compacted specimens are performed usually to obtain
information, which will be used for design purposes.
109
The CBR value for a soil will depend upon its density, molding moisture content, and
moisture content after soaking since the procedure of laboratory compaction should
closely represent the results of field compaction. The first two of these variables must be
carefully controlled during the preparation of laboratory samples for testing, unless it
can be ascertained that the soil being tested be affected by it in the field after
construction. The CBR tests should be performed on soaked samples.
4. Sample preparation for CBR test
If the soils or material is damp (moist) when received from field, dry it until it becomes
friable under a trowel, drying may be in air or by oven dry not exceeding 600c.
Thoroughly break up aggregations, being carefully to avoid reducing the natural size of
the individual particles and passing the 19mm or 4.75mm sieve will be required.
5. Replacement
If the material is granular (method 'D'), and passing the 19.5mm sieve and retained on
the 4.75mm sieve. If all material passes a 19mm sieve, the entire gradation shall be used
for preparing specimens for compaction without replacement or modification. If its mass,
does not exceed 25% of the mass of the original sample, no correction is necessary for its
removal.
If the mass retained is greater than 25%, it should be replaced by a similar mass if
particles of between 4.75mm and 19mm sieve obtained from separate batch of similar
sample. If there is material retained on the 19mm sieve the material retained on the
19mm sieve shall be removed replaced by an equal amount of sample passing 19mm
sieve and retained on the 4.75mm sieve obtained by separation from portions of the
sample not other wise used for testing.
6. Examples
Amount of sample received from field 'M' sample
Quarter the M' sample.
If % Rt of the 19mm sieve is = 30%
Mass of sample retained on the 19mm sieve m1 mass of sample passed on the 19mm
sieve m2 mass of sample retained on the 4.75mm, equal amount of m1 sample = m3
amount of sample for one CBR mold.
= m2 + m3 = m4
110
OR the assumed amount of sample for one CBR 7kg
Amount of material Retained sieve
7 x 30% = 2.1kg
Amount of material passed on the 19mm sieve
7 - 2.1 = 4.9kg.
Total = 2.1 + 4.9 = 7.00kg
Quarter the replaced or non replaced sample weigh and keep the representative sample
at least 5.4kg 12lb for fine grained (silty clay) soil and 6.4 to 7.7kg (14 to 17lb) for
granular sample.
7. Type of sample for test
The sample may be compacted in to the mold under dynamically compacted in to it, at
the required moisture content, either to achieve a specified density or by using a
standard compactive effort.
Undisturbed sample:- may be taken on site in a CBR mold, either from natural ground
or from recompacted material, such as in an embankment or road sub-base
specimens may be tested in the mold either as prepared or after soaking in water
for required days.
Penetration resistance:- force or pressure required to maintain a constant rate of
penetration of CBR piston, in to the soil.
Sub soil:- soil bellow the sub-grade or fill
Subgrade:- Natural soil or embankment construction prepared and compacted to
support a pavement.
Sub-base:- layer of selected material of specified thickness in a pavement system
between sub-grade and base course.
Base course:- layer of high grade crushed gravel or rock material of specified thickness
constructed on the sub-base to spread the load from the pavement and provide
drainage.
111
8. Pavement:- constructed layer of material of specified thickness, usually of select, gravel,
asphalt and concrete materials, designed to carry wheeled vehicles. This covers roads
and airfield or airports.
9. Flexible pavement:- pavement constructed by using gravel, crushed gravel or rock and
Asphalt materials.
10. Rigid pavement:- pavement constructed of concrete.
11. Surfacing:- top most layer of the pavement construction, providing a durable surface
and smooth riding.
12. Basis of CBR test:- a constant rate of penetration shear test in which a standard
plunger (Pistons) is pushed in to the soil at a constant rate and the force required to
maintain that rate is measured at suitable intervals. The road penetration relationship is
drown as a graph from which the loads corresponding to standard penetrations are read
off and expressed as ratios of standard loads. The CBR value can be regarded as an
indirect measure of the shear strength of the soil, but it can not be related directly to
shear strength parameter. The only calculation necessary is to express the measured
force for a certain penetration as a percentage of the standard force for the same
penetration.
CBR = Measured force x 100%
Standard force
The standard force corresponding to penetrations reading from 0.64 to 12.7mm The
forces shown in corresponding to penetrations of 2.5mm (0.1") and 5mm (0.2) are those
used in the standard calculations of CBR value. These are rounded equivalents to the
original criteria for contact pressures under a piston (plunger) of 32inchcross-section of
1000 PSI at 2.5mm penetration and 1500 PSI at 5.00mm in penetration respectively.
These standard forces where based on tests on samples of compacted crashed rock or
lime and by definition relate to CBR of 100% standard force penetration.
Relationship for CBR test
Failure
Soil
Penetration
inch/mm
Force lbf/kgf
Pressure
PSI/kg/m2
0.1/2.5 3000/1361.2 1000/70.3
0.2/5 4500/041.74 1500/105.49
0.3/7.62 5700/2585.5 1900/133.6
0.4/10.16 6900/1769 2300/161.7
0.5/12.7 7800/3580.1 2600/182.8
112
The corresponding load-penetration relationship is shown bellow.
Standard lad/penetration curve for CBR of 100%
Load
LPF
7000
6000
4500
4000
3000
2000
1000
0 2 2.5 4 5 6 8 10 12 14
Penetration (mm)
12.1 Limitations:- CBR test should not be used to estimate the bearing capacity of
ground for foundations: the rest should be regarded as an index property. The
application of which is restricted to pavement.
113
12.2 Construction:-
Practical Aspects of the test (typical CBR value)
AASHTO Unified
CBR
Value
Condition
Can be
used as
Clay A-5, A-6, A-7 OH, CH, MK, OL 0-3 V. poor
Silty Clay A-4, A-5,
A-6, A-7,
OH, CH, MK, OL 3-7 Poor + fair
A-2, A-4, A-6, A-7 OL CL, MC, S M, SL 7-20 Fair Borrow
A-1-b, A-2-5, A-2-6 GM, GC, SW, SM, SP 20-50 Good Sub-base
A-1-a, A-2-4, A-3, GW, GM, >50 V. good Base course
12.3 Surcharge weight:- the surcharge weights, simulates the effect of the thickness
of road construction overlying the layer being tested. Each 5lb disc is equivalent
to about 70mm thickness of superimposed construction.
Surcharge weight should placed on the top of surface of the prepared specimen
before testing.
If the specimen is to be soaked before testing the surcharge rings should be
placed on the sample immediately before immersion so that their presence can be
control the amount of swelling.
The effect of surcharge is greater for granular soils than for cohesive soils, but
granular soils generally provide satisfactory sub-grades and pavement bases so
this difference is not critical.
12.4 Effect of soaking:- the American practice as a precaution to allow for moisture
content increase in the soil due to flooding or elevation of the water table,
however, soaking has been shown to give rise to conditions which are too severe
in many cases, resulting in unnecessarily conservative designs of pavement
thickness.
13. TESTS
Apparatus
114
Sample mixing tray
Compacting mold with base plate, and extension collar
Rammer
115
4.75 and 19mm sieves
116
Spacer disc
Balance
Dial gauge
Oven
Tripod
Load frame (machine)
Soaking tank
Moisture (container)
Filter paper
Trimming knife
Procedure
Determine natural moisture content of the CBR test sample
A. wt of sample (Air dry) + container
B. wt of oven dry sample + container
C. wt of container
N.M.C = (A - B) x 100%
(B - C)
Calculate the amount of water to be added in order to increase the moisture in
the amount of test sample.
Let mass of air dry sample = m
Optimum moisture content = Wo
Natural moisture content = w1
Amount of water to be added M (Wo - W1)
(100 + W1)
Weigh the required amount of sample
Place the weighed sample on the sample tray
Measure the required measured (calculated) water
Weigh the mold and record
Add that calculated water and mix thoroughly
Place the spacer disc on the bass plate.
Place filter paper on the top of the spacer disc
Place the 1st portion of sample in to the mold
Compact it with the required method, rammer and blows.
Repeat the process using the other required portions.
117
Remove the extension collar and carefully trim the compacted soil even with
the top of the mold by means of a straight edge patch with smaller size
material any holes and rough surface that may have developed in the
surface by the removal of coarse material.
Remove the perforated base plate and spacer disk.
Weigh and record the mass of the mold plus compacted soil
Place a disk of coarse filter paper on the perforated base plate.
Invert the mold and compacted soil, and clamp the perforated base plate to
the mold with compacted soil in contact with the filter paper.
Place the surcharge weights on the perforated late and adjustable stem
assembly and carefully lower on to the compacted soil specimen in the
mold
118
Apply a surcharge equal to the weight of the base material and pavement with
in 5 or 10lb.
Mount the dial gauge support on top the extension caller, fit the dial gauge
and adjust the level of the stem on the perforated plate so that the gauge
reads zero or some convenient value.
Swell
Immerses the assembled mold in water allowing free access of water to the top
and bottom of the specimen.
Take initial measurements for swell immediately and allow the specimen to
soak for 4 days (96 hours) maintain a constant water level during this
period. If water does not appear at the top surface after 3 days
immersion, pour water on to the top surface so that it remains covered
and leave to soak. Usually soaking period is 4 days and 6 hours but a
longer period may be necessary to allow swelling to reach completion.
Take final swell measurements and calculate the swell as a percentage of the
initial height of the specimen.
Calculation of swell
- Height of specimen = H
- Division of the swelling dial gauge = 0.0254mm
- Initial dial reading = H1
- Final dial reading = H2
% swell = (H2 - H1) x 0.0254 x 100%
H
119
120
121
Penetration Procedure
Remove the sample and mould from the tank. Place the mold and sample on
the rigid surface, to drain downward for 15min. Take care not to disturb
the surface of the specimen during the removal of the water.
After some water has drained away remove the surcharge disc, perforated
plate and extension collar and weigh the sample with mould.
Setting up loading frame:-
Place a surcharge of weights on the specimen sufficient to
produce an intensity of loading to the weight of the base
material or over burden of material.
Place the mold with base plate contains the sample centrally the
platen of the testing machine.
Contact the plunger with the top of the sample surface. Check
that the connections between plunger load ring and cross-
head are tight.
Mount the penetration dial gauge on the bracket attached to the
plunger.
Seat the penetration piston with the smallest possible load. The
value of which depends on the expected CBR values as
follows.
CBR Value PI Seat Load
Silty clay about 5% 20 - 30 10N
Silty 1 - 2% 0 10N
Sandy clay 4 - 7% 20 - 30 25N
Gravelly clay 5 - 30% 20 - 30 50N
Sandy Gravel Above 30% NP 250N
Winds up the machine platen slowly by hand until the load ring
indicates this reading. Then reset the load dial gauge to zero,
because the seating load is not taken into account in the
test.
Adjust the penetration dial gauge to read zero or same
convenient datum reading.
122
Switch on the motor and record the load ring dial and
penetration at 0.64mm (0.025") up to 12.7 (0.5")
0.64, 1.27, 1.95, 2.54, 3.18, 3.81, 4.45, 5.08, 10.16 and
12.7mm
123
124
125
126
127
Calculation
Penetration dial division = 0.0254
Load dial reading = C
Ring factor = R lb
Area of piston = A inch
Stress CxR = PSI
A
Load - Penetration Curve:- readings of the load ring dial gauge are converted
to force units by multiplying by the load ring factor (Rf) and plot the
128
stress-penetration curve. In some instances, the stress penetration curve
may be concave up ward initially, because of surface irregularities or
other courses, and in such cases the zero point shall be corrected or
adjusted.
Against penetration, and the force need be calculated only at penetration
of 2.5 and 5mm.
If the load PSI at 2.5mm = P
CBR = Px100 = CBR% and at 5mm P2x100 = CBR%
1000 1500
Or using corrected stress values taken from the stress penetration curve
for 0.1 inch and 0.2 inch penetrations. Calculate the bearing ratios for
each be dividing the corrected stress by the standard stress of 1000 PSI
= (6.9 MPa) and 1500 PSI (10.3 MPa) and multiplying by 100.
The bearing ratio normally reported for the soil is the one (0.1 inch) when
the ratio at 0.2 inch is greater rerun the test. If the check test gives a
similar result use the bearing ratio at 0.2.
Calculate the moisture content and unit weight or density, bulk and dry,
before soak and after soaked.
Three point CBR
If CBR value for soil at 95% of max. dry density is desired, samples
(specimen) should be compacted using 10, 30, and 65 blows per layer is
satisfactory penetration shall be performed on each of these specimen
load - penetration curve plot the CBR value versus dry density graph
determine the design CBR at the percentage of the max dry density. This
procedure is both for standard and modified compaction.
129
130
131
132
SECTION IV
IN-PLACE DENSITY (FIELD DENSITY)
This method of test is intended to (cover) determine the density (compaction) of soil
materials, in the natural state or after compaction in an embankment (fill) and road
pavement construction, by finding the weight and moisture content of a disturbed and
measuring the volume of density hole occupied by the sample prior to removal.
Three test methods are provided as follows.
I. Rubber Balloon Method
II. Sand Cone (Replace) Method
III. Nuclear Gauge Method
I. Rubber Balloon Method
1. This test method covers the determination of the in-place density of compacted or
firmly bonded soil using a rubber balloon apparatus.
This test method is suitable for undisturbed or natural in organic soil, deposits
soil or other similar firm materials and fill or embankments constructed of fine
grained soils.
This test method is not suitable for use in organic saturated, swampy or highly
plastic soil sand crashed rock fragments or sharp edge material. Because that
would deform under the pressure applied during this test. This test method may
require special core for use on.
1. Fill materials containing particles with sharp edges.
2. Soils consisting of unbounded granular materials that will not maintain
stable sides in a small hole.
3. Soils containing appreciable amount of coarse material in excess of specified
sieve size in mm.
4. Granular soils having high void ratios.
The volume of an excavated hole in a compacted soil is determined using a
liquid filled vessel for filling to fill the hole.
This test method may be used to determine the density of compacted soils used
in construction; backfill, earth embankments, road fill and structural backfill.
133
Soft soils are not recommended for this method because may deform easily.
Such soils may undergo a volume change during the application of pressure
during testing.
2. Apparatus calibrated vessel balloon apparatus
Calibrated vessel balloon apparatus
Base plate (a rigid metal)
Balance 1gm readable
Oven or drying apparatus
Sample container
Miscellaneous, chisels, spoon buckets, and plastic bags shovel etc.
3. Procedure
Verify procedure to be used and the accuracy of the volume indicator by using
the apparatus to measure containers or molds of known valium that
dimensionally simulate test trails that will be used in the field. The apparatus
and procedures shall be such that these containers will be measured to with in
1% of the actual volumes.
Determine the mass of water in cc or grams, required to fill the containers or
hole, molds using a glass plate and or thin film of grease, if needed for sealing
determine the mass of the container or mold and glass plate to the nearest
gram. Fill the container or mold with water, carefully sliding the glass plate over
the opening in such a manner as to ensure that no air bubbles are enter, that
the mold is filled completely with water.
Remove excess water and determine the mass of the glass plate, water and mold
or container to the nearest the gram. Determine the temperature of the water
calculate the volume of he mold or container. Repeat this procedure for each
container or mold until three consecutive volumes having or maximum variation
of 2.83 cm3 or 0.001 f3 is obtained. Record the average of the three trials.
Checking calibration:- place the rubber balloon apparatus and base plate on a
smooth horizontal surface. Applying on operating pressure take an initial
reading on the volume indicator. Before any measurements are taken it may be
necessary to distend the rubber balloon and by kneading remove the air
bubbles adhering to the inside of the membrane. If the calibration molds re air
tight, it may be necessary to provide an air escape to prevent erroneous results
134
caused by the trapping of air by the membrane. One means of providing air
escape is to place small diameter strings over the edge of and down the inside,
slightly beyond bottom enter of the mold. This will allow trapped air to scope
during the measurement of the calibrated mold or container.
Transfer the apparatus to one of the previously calibrated molds with a
horizontally leveled bearing surface. Apply the operating pressure as necessary
until there is no change indicated on the volume indicator. Depending on the
type of apparatus, the operating pressure maybe as high as 34.5kpa and may
be necessary to apply a downward load to the apparatus to keep it from rising.
It is recommended that the operating pressure of the apparatus be kept as low
as possible while maintaining the 1% volume accuracy. The use of higher
pressures than necessary may require the use of an additional load weight to
prevent up lift of the apparatus. The combined pressure and surcharge loads
may result in stressing the unsupported soil surrounding the test hole causing
it to deform.
Record the reading pressures, and surcharge roads used. The difference
between the initial and final readings is the indicated volumes determine the
volume of he other molds or containers. A satisfactory calibration check of an
apparatus has been achieved when the difference between the indicated
calibrated volume of the container or molds is 1% or less, for all volumes
measured. Select the optimum operating pressure and record it for use with the
apparatus during field testing operations.
Make this smooth surface at the test location so that it is plane and level. The
test area is not deformed compressed torn, or other wise disturbed.
Assemble the rubber balloons and bass plate apparatus on the smooth test
location
Take an initial reading on the volume indicator and record. The base plate shall
remain in-place through compilation of the test.
Dig a hole within the base plate. Care in digging the test hole so that soil around
the top edge of the hole is not disturbed. When material being tested contains a
small amount of over size and isolated large particles are encountered, the test
135
can be removed to a new location. If particles larger than 20 or 37.5mm are
prevalent, larger test apparatus and test volumes are required larger test-hole
volumes will provide improved accuracy and shall be used where particle.
Maximum Particle size Maximum Test hole
37.5mm 2840
20mm 1700
4.75mm 1130
The test hole shall be kept as free of pockets and sharp obtrusions as possible,
since they may affect accuracy or may puncture the rubber membrane
Place all soil removed from the test hole in an airtight container for later mass
and water content determination.
Place the apparatus after the test hole has been dug over the base plate in the
same position as used for the initial, reading.
Applying the same pressure and surcharge load as used in the calibration
check, take and record the reading on the volume indicator. The difference
between the initial and final readings is the volume of the test hole.
Determine the mass of all the wet soil removed from the test hole to the nearest 5gm
max all the soil thoroughly and select a representative water content sample
and determine the moisture content
Calculation
Volume of mold V = (W1-W2) x Vw
Where V = volume of mold
W1 = weight of mold and glass and water
W2 = weight of mold and glass
Vw = volume of water
In-place wet (bulk)t density, Pwet = Ay
Vh
Where Pwet = weight density
wA = weight of moist soil removed from the test hole
Vh = volume of the test hole
In-place dry density, d = Pwet .
1 + Wo
100
136
d = pwet x 100
100 + Wo
Where d = In place dry density
Wo = In place moisture content
% Compaction = d x 100
MDD
Where MDD standard testing lab
Report
Test location
Project
Test holes volume
In-place wet, dry density and moisture content
% compaction
Visual description of the soil
1. In-Place density by Nuclear methods:
This method of test covers a procedure for determining the density and moisture
content of soils, either in the natural state or after compaction by means of a nuclear
moisture density gauge.
The nuclear gauge can be used to make relative or percent compaction determination.
The density in mass per unit volume of the material under test is determined by
comparing the detected rate of gamma radiation with previously established calibration
data.
The test method described is useful as a rapid nondestructive technique for the in-
place determination of density of soil.
The test method is suitable for quality control and acceptance testing for construction
and for research and development applications.
The nondestructive nature of he test allows repetitive measurements to be made at a
single test location.
137
Over size material (Rock) poor or gap graded material (voids) in eth source detector
path may cause higher or lower density determination. Where lack of uniformity in the
soil due to layering rock or voids is suspected, the test volume site should be dug up
and visually examined to determine if he test material is representative of the full
material in general and if rock correction is required.
2. Apparatus
2.1 Nuclear gauges:- which contain a radio active source.
2.2 Reference standard
2.3 Site preparation device
2.4 Drive pine
2.5 Drive pin extractor
2.6 Slide hammer
3. Danger (Hazards) this equipment utilizes radioactive materials that may be hazardous
to the health of the users unless proper precautions are taken. Users of this equipment
must become familiar with applicable safety procedures and government regulations.
3.1 Effective user instructions together with leak tests, recording and evaluation of
film badge data, etc, are a recommended part of the operation and storage of this
instrument.
4. Procedure for field use
4.1 Standardize the gauge
4.2 Select a test location
4.3 Remove all disturbed and loose material
4.4 Remove additional material as necessary to reach the material.
4.5 That represents a valid sample of the zone or stratum to be tested. Surface drying
and spatial bias should be considered in determining the depth of material to be
removed.
4.6 Plane smooth horizontal surfaces so as to obtain maximum contact between the
gauge and the material being tested. To correct for surface irregularities, use of
fines or fine sand as filler may be necessary. The depth of the filler should not
exceed 3mm and the total area filled should not exceed 10% of the bottom area of
instrument several trial seating may be required to achieve these conditions.
4.7 Seat the gauge firmly on the prepared test site.
138
4.8 Keep all other radio active sources away from the gauge to avoid affecting the
measurement so as not to affect the readings.
4.9 Secure and record one or more readings for the normal measurement period in
the back scatter position.
4.10 Determine the ratio of the reading to the standard count or to the air gap count.
From this count ratio and the appropriate calibration and adjustment data,
determine the in-place bulk (wet) density.
4.11 Make a hole perpendicular to the prepared surface using the guide and the hole-
forming device or by drilling if necessary. The depth of the hole must be deeper
than the depth to which the probe will be placed. The guide shall be the same
sizes the base of the gauge with the hole in the same location on the guide as the
probe on the gauge. The corners of the guide are marked by scoring the surface of
the soil. The guide plate is than removed and any necessary repairs are made to
the prepared surface.
4.12 Set the gauge on the soil surface, carefully beginning it with the marks on the soil
so that the probe will be directly over the pre-formed hole.
4.13 Insert the probe in the hole
4.14 Seat the gauge firmly by rotating it about the probe with a back and forth motion.
4.15 Pull gently on the gauge in the direction that will bring the side of the probe
against the side of the hole that is closest to the detector (source) location in the
gauge housing.
4.16 Keep all other radioactive sources away from the gauge to avoid affecting the
measurement.
4.17 Record one or more readings for the normal measurement period.
4.18 Comparison need to be made to evaluate whether the presence of a single large
rock or void in the soil is producing unrepresentative values of density whenever
valves obtained are questionable, the test volume sit should be dug up and
visually examined.
4.19 If the material (sample) is containing oversize particles (rock) the test should be
corrected.
4.20 Calculation
4.20.1 The in-place wet density, moisture content and dry density are
determined as outlined in 4.6 - 4.18
4.20.2 Determine the max. dry density and OMC in Laboratory
4.20.3 Determine the % compaction c = Fdd x 100
MDD
139
Where C = % compaction
Fdd = field dry density
MDD = Max.dry density in Laboratory
5. In-Place density by the sand replacement method
5.1 This test method covers a procedure to determine of the In-place density of soils,
either in after compaction or in the natural state, using a pouring device and
calibrated sand material to determine. The weight and moisture content of a
disturbed sample and measuring the volume occupied by the sample prior to
removal.
5.2 The soil or material being tested should have sufficient cohesion or particle
attraction or particle interlocking to maintain stable sides during excavation of
the test pit on a small hole in excavation, and be firm enough to withstand the
minor pressure exerted in digging the hole and placing the apparatus over it or
pouring without deforming or sloughing.
5.3 This test method is not suitable for saturated condition highly plastic soils or
organic and are not recommended for materials that is soft or crumble easily or
compress (deform) during the excavation of the test hole. This test method may
not be suitable also for soils consisting of unbound gravel (coarse) materials that
will not maintain stable sides in eth test hole. The accuracy of the test methods
may be affected for materials that deform easily or that may undergo volume
change in the excavated hole during the test.
5.4 When materials to be tested contain appreciable amounts of particles larger than
50-37.5mm or where test hole volumes larger than 2830cm3 are required.
5.5 The construction subgrade, subbase, base course and surfacing after enoughly
compacted, at the test location is prepared and a metal frame is placed and fixed
into position. The volume of the space between the top of the metal frame and the
ground surface is determined by filling the space with calibrated sand using a
pouring device. The hole is filled with free flowing sand of a known unit weight
and the volume is determined. The wet density of the in-place material is
calculated from the mass of material removed and the measured volume of the
test pit. The water content of the material from the hole is determined and the dry
mass of the materials and the in-place dry density are calculated using the wet
mass of the soil, the water content, and the volume of the hole.
140
5.6 These test methods are used to determine placed during the construction of earth
embankments, structure backfill road backfill sub-base, base course and
surfacing. For construction control, these test methods are often used as the
141
bases for acceptance of material compacted to a specified density or to a
percentage of a maximum density determined by a standard laboratory test
method (by standard or modified proctor, max dry density)
5.7 Two In-place density test methods are provided
5.7.1 In-place density of total material is to be determined the maximum particle
size present in the in-place material bring tested does not exceed the max
particle size allowed in the lab. compaction test.
5.7.2 The In-place material contains particles larger than the max. particles size
allowed in the laboratory compaction test.
6. Apparatus
6.1 Sand cone density jar (apparatus) an attachable funnel or sand cone
6.2 Clean, dry and Calibrated sand
6.3 Balance
6.4 Drying equipment (oven)
6.5 Sieves 0.850, 0.60, 0.30 and 0.075mm
6.6 Metal plate with center hole
6.7 Straightedge
6.8 Miscellaneous equipment shovels chisel, brush etc.
7. Calibration and standardization of density sand
7.1 Wash the sand and shall be cleaned from dust and any fine particles
7.2 Dry and sieve the washed sand
7.3 Sieving
7.3.1 The dried sand is placed in the 0.850mm sieve shaken for long enough for
all fine particles smaller than 0.85mm sieve size to pass through. This can
be achieved most conveniently by using a mechanical sieve shaker. If a
shaker is not available, sieving can be done by hand.
7.3.2 Mechanical shaker:- the selected sieve with receiving pan is placed in the
shaker. The sand is placed in the top sieve, which is then fitted with the
lid, and the two or more sieves are securely fastened down in the machine
agitation in the shaker should be for a minimum period of 10 min.
7.3.3 Hand sieving:- place the dried sand sample on the largest sieve. The sieve
must be agitated by shaking so that the particles roll in an irregular
motion, and until no more particles pass through the openings.
142
Sieve Size Pass Retire
No. 20 (0.850)mm x
No. 30 (0.60)mm x
Or
No. 30 (0.6)mm x
No. 50 (0.30)mm x
Summary:-
Choice 1: Pass No 20(0.850mm) Retained No 30 (0.60mm)
Choice 2: Pass No 30(0.60mm) Retained No 50 (0.30mm)
7.4 Determination of the weight (mass) of the calibrated sand required to fill the
funnel (cone)
a. mass of Jar + Sand before pouring
b. mass of Far + Sand after filling (pouring)
Mass (weight) of sand in cone = a-b = c
7.5 Determination of Bulk unit weight of the clean and calibrated sand
V = volume of apparatus
S1 = mass of clean sand + container
S2 = mass of clean sand + container
S3 = mass of container sand + container
S4 = Average mass of clean sand = S1 + S2 + S3
3
S5 = mass of container
S6 = The Average mass of sand = S4 - S5
Bulk unit weight of sand = S6 g/cc
V
8. Determination of the density of the soil In-place (sand cone method)
8.1 Inspect all density apparatus
8.2 Assemble and Inspect the density jar apparatus cone for damage, free rotate of
the value, and properly matched base plate.
8.3 Inspect the compacted site visually compacted enough or not
8.4 Select a location that is representative of area to be tested the In-placed density
8.5 In-place density should be taken after compaction, about 24-78 hours.
8.6 Prepared the surface of the location to be tested
143
8.7 Remove all loose material from the surface of an area larger enough to receive the
metal plate make smooth surface in the soil to properly and firmly seat the plate
8.8 In soils where leveling is not successful or voids, remain, volume horizontally
bounded by test funnel, plate and ground surface must be determined by
preliminary test fill the space with sand from the apparatus determine the mass
of sand used to fill the space, refill apparatus, and determine a new initial mass of
apparatus and sand before proceeding with the test. After this measurement is
completed, carefully brush the sand from prepared surface.
8.9 Place the Metal plate centrally hole plate on the smooth (leveled) test size.
8.10 Nail on four position
8.11 Excavate the hole through the center hole in the plate, using chisel or knife, being
careful to avoid disturbing or deforming that will bound the hole, Do not permit
any movement of heavy equipment in the Area of the test pit PIS deformation of
the soil with in the test pit may occur.
8.12 Place all material removed from the test hole in a suitable container being
carefully to avoid losing any particle. Avoid moisture loss by keeping the container
covered while material is not being placed in it. Use sealable plastic bag, avoid
any heat before being weighed
8.13 Carefully trim the sides of the excavation
8.14 Continue the excavation to the required depth
8.15 The sides of the hole should slope in ward slightly. The sides of the test pit should
be smooth as possible and free of pockets to over hangs or anything that might
interfere with the free flow of the sand.
8.16 Clean the sides and bottom of the test pit of all loosened material.
8.17 If during excavation of material from with in the test pit, a particle larger than the
laboratory compaction material, go to method 2.
8.18 Carefully weigh the removed sample from hole and record
8.19 Put the weighed material in oven or drying apparatus to dry and determine the in-
place moisture content.
8.20 Fill or pour the calibrated sand in the density jar and weight initially.
8.21 Carefully put at the center of the test hole attached with metal plate.
8.22 Open carefully the density valve at the center of the test hole attached with metal
plate
8.23 While the sand is being poured, avoid any vibrations in the test area.
8.24 When it is being stop pouring in the test hole close the density valve.
8.25 Remove the remaining sand and jar.
144
8.26 Weigh the remaining sand and jar and record.
8.27 Removed the clean used sand was being in hole and place it n to container.
8.28 Remove the metal plate from test hole and calibrate
8.29 Reclean and calibrate the used sand, sieve by 0.850 and 0.600mm or 0.600 and
0.300mm sieve.
9. Calculation
9.1 Determine the volume of test hole.
P = W V = W
V 
Where V = Volume of density hole
W = Weight of sand in hole
 = Unit weigh of clean sand
9.2 Determine the in-place Bulk density
Bd = m1 - m2
V
Where m1 = mass of sample in hole + container
m2 = mass of container
V = Volume of test hole
or
9.3 Bulk density, Bd m1 - m2
msh
Where msh = mass of sand in hole
9.4 Determine the in-place moisture content
Wo = A - B x 100
B - C
Where Wo = moisture content
A = wt of wet sample + container in hole
B = wt of dry sample + container
145
9.5 Determine the in-place dry density
fdd = Bd .
1 + Wo
100
9.6 Determine the % compaction
C = Fdd x 100
Mdd
Where C = % compaction
Mdd = max. dry density in laboratory
Fdd = Field Dry Density
CLIENT :
PROJECT :
TEST ON :
TEST SPECIFIED BY :
SAMPLED BY :
KINDS OF TEST :
LAB. NO. :
DATE ISSUED :
IN-PLACE DENSITY DETERMINATION
SAMPLE NUMBER OR STATIONS 1 2 3 4
Weight of wet soil from hole, W(gm) 2348 2362 2344 2353
Weight of sand + jar before pouring, W1(gm) 6000 6000 6000 6000
Weight of sand + jar after pouring, W2(gm) 4400 4480 4510 4490
Weight of sand in cone, W3(gm) 480 480 480 480
Weight of sand in hole, W4=(W1-W2-W3) 1120 1040 1010 1030
Bulk Density Ww x Ps (g/cc)
Wsh
2.10 2.27 2.32 2.28
Wt. of Wet soil 2348 2362 2344 2352
Wt. of Dry soil 2150 2165 2138 2143
Wt. of Moisture, g 198 197 206 209
Moisture Content (m), % 9.2 9.1 9.6 9.8
146
Dry Density D = 100 x Wet Density, g/cc
100+m
1.92 2.1 2.12 2.08
M.D.D (g/cc) 2.21 2.21 2.21 2.21
Optimum Moisture Content (%) 2 12 12 12
% Compaction 87 95 96 94
% Moisture 77 76 80 82
Remark:
147
Summary
Bd = M1 x s
(m2 - m3 - m4)
Where Bd = bulk density
m1 = mass of sample in test ole
m2 = mass of sand + jar before pouring
m3 = mass of sand + jar after pouring
m4 = mass of sand in cone
s = density of sand
148
References
The American Association of State Highway and Transportation Officials
(AASHTO) part 2, 1986 T87-T274
ASTM Volume 04, 08 Rock and Soil (1) D420 - D4914
British Standard 1377 part 1 - 9 K H Head Part 1 and 2
Lambe
Soil Mech – M DAS
149
IN-PLACE DENSITY DETERMINATION-Form
AASHTO 191
ASTM D 1556
PROJECT: OPERATOR DATE
TEST TAKEN ON (A) ------------------------ (B) SUBBASE ----------------------------
STATION REP. FROM KM UNIT WEIGHT OF SAND (AS DETERMINED IN HE LAB.)
REPORTED TO: Lab. No
SAMPLE NUMBER OR STATIONS
Weight of wet soil from hole, W(gm)
Weight of sand + jar before pouring, W1(gm)
Weight of sand + jar after pouring, W2(gm)
Weight of sand in cone, W3(gm)
Weight of sand in hole, =(W1-W2-W3)(gm)
Bulk Density Ww x Ps (g/cc)
Wsh
Wt. of Wet soil
Wt. of Dry soil
Wt. of Moisture, g
Moisture Content (m), %
Dry Density D = 100 x Wet Density, g/cc
100+m
M.D.D (g/cc)
Optimum Moisture Content (%)
% Compaction
% Moisture
150
151
152
153

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Construction Material Testing Lab Manual Part I.doc

  • 1. Preface This manual describes the procedures for laboratory testing of road construction and building materials carried out at Central Materials Laboratory and at construction site Laboratory. The test procedures are in essence based on AASHTO, ASTM and British Standard methods of Sampling and Testing. To enhance the understanding of the testing principles and procedures, illustrative examples, standard test data sheets, diagrams, figures, and test result reports are included. The user is supposed to strictly follow the routine testing procedures described in the relevant sections of the manual. Besides, it is essential to use this manual in conjunction with the reference standards; i.e. AASHTO, ASTM and BS Standards. Manual part I presents details of the methods for Atterberg limits, Particle size analysis, AASHTO and unified soil classification, Moisture – Density Relationship (compaction), the California Bearing Ratio (CBR) , Specific Gravity and In-place Density of soil- aggregates. This testing manual has been prepared and compiled by SABA Engineering Plc, as part of the assignment for Consultancy Services for The Establishment of Regional Construction Materials Testing Laboratories for 11 towns in Ethiopia. Preparation of this soils and materials manual has been a component under the Contract Agreement signed between the MoWUD, the implementing body on behalf of the Ministry of Capacity Building, Public Sector Capacity Building (PSCAP) Support Project and SABA Engineering Plc. The project is financed by the World Bank.
  • 2. TABLE OF CONTENT Page Introduction --------------------------------------------------------------------------------------------1 Moisture Content --------------------------------------------------------------------------------------13 Atterberg Limits Casagrande - Liquid Limit Method ----------------------------------------------------------------15 Plastic Limit -------------------------------------------------------------------------- 25 Plasticity Index ---------------------------------------------------------------------- 28 Cone Penetrometer Liquid Limit ------------------------------------------------------------------28 Soil Classification AASHTO Soil Classification ----------------------------------------------------------------35 Unified Soil Classification ------------------------------------------------------------------44 Shrinkage Limits Volume Metric -------------------------------------------------------------------------------- 48 Linear ------------------------------------------------------------------------------------------ 54 Amount of Material Finer than No. 200 sieve ---------------------------------------------------- 59 Standard Method of Mechanical Analysis of Soil ------------------------------------------------ 62 Hydrometer Analysis --------------------------------------------------------------------------------- 65 Specific Gravity of Soil ------------------------------------------------------------------------------- 84 Moisture Density Relationship --------------------------------------------------------------------- 91 California Bearing Ratio (CBR) -------------------------------------------------------------------- 107 In-place Density ------------------------------------------------------------------------------------- 129
  • 3. 1 INTRODUCTION SOIL 1. Soil is derived from the Latin word solium. The upper layer of the earth that may be dug or plowed specifically, the loose surface material of the earth in which plants grow. The soil is used in the field of agronomy where the main concern is in the use of soil for raising crops. The term soil is used for the upper layer of mantle which can support plant. The material which is called soil by the agronomist or the geologist is known as top soil in geotechnical engineering or soil engineering. The top soil contains a large quantity of organic matter and is not suitable as a construction material or a foundation for structures. The top soil is removed from the earth's surface before the construction of structures. In soil engineering is defined as an unconsolidated material, composed of solid particles, produced by the disintegration of rocks. The void space between the particles may contain air, water or both. The solid particles may contain organic matter. The soil particles can be separated by such mechanical means as agitation in water. A natural aggregate of mineral particles bonded by strong and permanent cohesive forces is called rock. Soil is composed of loosely bound mineral grains of various size and shapes, organic material, water and gases. The bonds holding solid particles together in most soil are relatively weak in comparison to most sound rocks. In fact and air-dried sample of soil will crumble and break down within a relatively short period when placed in water and gently agitated. The solid particles of which soils are composed are usually the products of both physical and chemical action on weathering. Deposits of these weathered solid constituent may be found near or directly above the bed rock (residual soils) or organic deposits from which they were formed. Many soil deposits, however, have been transported from their point of origin to new locations by such agents as water, wind, ice or volcanic action water-transported soils are classed as alluvial (deposited by moving water on flood plains, deltos, and bars.
  • 4. 2 The Origin of Soil Soils are formed by weathering of rocks due to mechanical disintegration or chemical decomposition. when surface of a rock is exposed to atmosphere for an appreciable time, it disintegrates or decomposes into small particles and thus the soils are formed. Soil may be considered as an incidental material obtained from the geologic cycle which goes on continuously in nature. The geologic cycle consist of erosion, transportation, deposition and upheaval of soil. Exposed rocks are eroded and degraded by various physical and chemical processes. The products of erosion are picked p by agencies of transportation, such as water and wind and are carried to new locations where they are deposited. Based on the mode of origin, rocks can be divided into three basic types: igneous, sedimentary, and metamorphic. Igneous Rock:- are formed by solidification of molten magma ejected from the deeper part of the earth's mantle. Molten magma on the surface of the earth cools after being ejected by either fissure or volcanic eruption. Sedimentary Rock:- the deposits of gravel, sand, silt and clay formed by weathering may be come compacted by overburden pressure. Metamorphic Rock:- is the process of changing the composition and texture of rock (without melting) by heat and pressure. Marble:- is formed calcite and dolomite by re-crystallization. The mineral grains in marble are larger than those in the original rock. Quartzite a metamorphic rock formed from quartz-rich sand stones. Soil Structure Soil particles may vary over a wide range. Soils are generally called gravel, sand, silt, or clay, depending on the predominant silt of soil particles. To describe soils by their particle size, several organizations have developed soil-separate-size limits. For the coarse grained soils, primary structure can frequently be observed with the unaided
  • 5. 3 eye or a hand lens. Methods for observing the structure of fine grained soil (silts and clays) have been slower in developing. Water, Solids, and Air Relationships In the case of primary structures, however, visual observations usually are insufficient, and indirect means are employed to evaluate this factor roughly. To do this it has been found convenient to think of any soil as being composed of three states of matter solid, water and gas or air. Although it is impossible to make this separation into three separate states in the laboratory, it is convenient to represent soil as shown in figure 1. Va O Vv V Vw Ww W Vs Ws Fig. 1 2. Soil Type A geotechnical engineer should be well versed with the nomenclature and terminology of different types of soils. The following list gives the names and salient characteristics of different types of soils, arranged in alphabetical order. Black cotton Soil Brown clay Red clay Gray clay Pinkish clay Bentonite clay Boulders Tuff Desert soils Cobbles Gravel Lateritic Peat Sand Silt Top soil Expansive clays Organic clay Blue clay Yellow clay Green clay White clay etc. Air Water Solids
  • 6. 2 1. Desert Soil :- Loose fine deposit sand and silt and dust particles size of the particles is uniform in gradation. 2. Lateritic Soils :- formed by decomposition of rock, removal of base and silica, and accumulation of iron oxide and aluminum oxide. The presence of iron oxide gives these soils the characteristic red or pink color. These are residual soils formed from basalt. 3. Black Cotton soil :- is clay of high plasticity. Its contain essentially the clay mineral montmorillonite. The soil has high shrinkage and swelling characteristics. The shrinkage strength of the soil is extremely low. The soil is highly compressible and has very low bearing capacity. It is extremely difficult to work with such soil. 4. Betonite:- it is a type of clay with a very high percentage of clay mineral montmorillnite. It is highly plastic clay, resulting from the decomposition of volcanic ash. It is highly plastic clay, resulting from the decomposition of volcanic ash. It is highly water absorbent and has highly shrinkage and swelling characteristics. 5. Expansive Clay:- a large volume changes as the water content is changed. This soil contain the montmorillonite. 6. Clay:- it consists of microscopic and sub-microscopic particles derived from the chemical decomposition of rock. It contains a large quantity of clay minerals. It can be made plastic by adjusting the water content. It exhibits considerable strength when dry. Clay is a fine grained soil. It is a cohesive soil the particle size is less than 0.002mm. 7. Gravel:- gravel is a type of coarse-grained soil. The particles size ranges from 4.75mm to 75mm. 8. Cobbles:- cobbles are large size particles in the range of 75mm to 300mm. 9. Boulders:- boulders are rock fragments of large size, more than 300mm in size. 10. Peat:- it is an organic soil having fibrous aggregates of macroscopic and microscopic particles. It is formed from vegetal matter and different plants, animals wast water under conditions of excess moisture, such as in swamps. It is highly compressible and not suitable of foundation.
  • 7. 3 11. Sand:- it is a coarse-grained soil, having 0.075 to 4.75mm size. The particles are visible to naked eye. The sand is most of product from river. 12. Silt:- it is a fine grained soil, with particle size between 0.002 to 0.075mm the particle size is not visible to naked eye. It has non or little plasticity and no more swelling and cohesion less. 13. Tuff:- it is a fine-grained soil composed of very small particles ejected from volcanoes during its explosion and deposited by wind or water. 14. Top Soil:- top soil are surface souls that support and grow plants, they contain a large quantity of organic matter and are not suitable for foundation. 3. Soil Mechanics Soil mechanics is the application of the laws of mechanics and hydraulics to engineering problems dealing with sediments and other unconsolidated occultation of solid particles produced by the mechanical and chemical disintegration of rock regardless of whether or not they contain on admixture of organic constituents; soil mechanics is therefore, a branch of mechanics which deals with the action of forces on soil and with the flow of water in soil. 4. Geotechnical Engineering Soil In an applied science dealing with the applications of principles of soil mechanics to practical problems. It has a much wider scope than soil mechanics, as it deals with all engineering problems related with soils. It includes soil investigations, design and construction of foundations, earth-retaining structures and earth structures. 5. Soil Engineering Foundation:- every civil engineering structure, whether it is a building, a bridge, or a dam, is founded on or below the surface of the earth. Foundations are required to transmit the load of the structure to soil safely and efficiently.
  • 8. 4 a) Foundation is termed shallow foundation (light load) when it transmits the load to upper strata of earth. (A) Shallow Foundation (Footing) Load Column Natural Ground Level Soil
  • 9. 5
  • 10. 6
  • 11. 7 Purpose of Soil Testing The chemical and physical properties of materials are determined by carrying out different tests on samples of soil in a laboratory. Tests for the assessment of engineering properties, such as moisture content, Atterberg limits, gradation and hydrometer analysis, density, CBR, in-situ density etc. The parameters determined from laboratory tests, taken together with descriptive data relating to the soil, area required by soil engineers for many purposes. The more usual applications are follows. a) The findings of a site investigation can be supplemented by farther testing as construction proceed b) Criteria for the acceptance of a material used in construction c) Data acquired from classification tests are applied to the identification of soil of soil strata. d) Laboratory tests are needed as part of the control measures which are applied during construction of earth works on for ensuring that the design criteria are met. The advantages of laboratory testing are in a field investigation for different construction projects, the field operations, which includes of the geology and history of the site subsurface exploration and in place testing, are of prime importance. The determination of the ground characteristics by in place testing can take into account large scale effects. However the measurement of soil properties by mans of laboratory tests offers a number of advantages, as follows: 1. A test can be run under conditions which are similar to, or which different from those prevailing in situ, as may appropriate. 2. Test can be carried out on material (soils) which have been broken down and reconstituted. 3. Control of the test conditions, including boundary conditions can be exercised. 4. Control can be exercised over the choice of material which is too be tested. 5. Laboratory testing generally permits a greater degree of accuracy of measurements that does field tests.
  • 12. 8 The evaluation of soil properties from reliable test procedures has led to a closen understanding of the nature and probable behavior of soils as engineering materials. Some of the resulting advantages in the realm of civil engineering construction have been: a) Increasing economy in the use of soils as construction materials b) Reduction of uncertainties in the analysis of foundations and earthworks c) Exploitation of difficult sites d) Economies in design due to the use of lower factors of safety e) Erection of structures, and below-ground construction, which would not have been feasible without this knowledge. Scope of Manual This manual is concerned only with soil testing. Soil Laboratory Testing Test:- derived from Latin, testum treating or trying gold, metals and silver alloys. Examination or trial by which the quality of anything may be determined. The process or action of examining a substance under known conditions in order to determine its identify or that of one of its constituents. The physical properties of materials are tested in order to determine their ability to satisfy particular requirements. Laboratory:- experiments in natural science. Sample:- a relatively small quantity of material from which the quality of the mass which it represents may be inferred. Specimen:- a part of as representative of the whole sample. This manual deals with standard laboratory. - Moisture content - Atterberg limits (LL, PL, PI, SL, LS) - Compaction - Classification - California Bearing Ratio - In-place Density - Sieve analysis and hydrometer
  • 13. 9 Method of test for soil (for civil engineering purposes.) The procedure (tests) described here are based on Standard Practice Specified in the AASHTO, ASTM and BS (Standard). The main emphasis of the manual, however, is on the detailed procedures to be followed in preparing samples for and carrying out different tests in the laboratory. Appropriate to this test, details of the apparatus required, a procedural stages, and step by step detailed procedures are included. The typical examples, calculation and plotting of graphs and presentation of results are described. Finally:- it is essential material testing technician requires a knowledge of good testing techniques and an understanding of the correct procedures for the soil sample preparation and for testing. Terminology and units are used metric (SI).
  • 14. 10 Soil Survey (Investigation) and Sampling Purpose of the Soil Investigation (survey) is an essential part of a preliminary engineering soil survey for location and design purposes. Information on the distribution of soil material and ground-water table and conditions must be obtained before a reasonable and economic design can detailed soil survey (investigation) provides pertinent information on the following subject. 1. The selection of the type of surface and its design. 2. The design of the roadway section 3. The location of the road, both vertically and horizontally 4. The design and location of culvert ditches and drains. 5. The need for subgrade treatment and the type of treatment required. 6. The location and selection of borrow material for files and subgrade treatment. 7. The selection of local sources of construction materials for subbase, base course and surfacing or wearing course. The soil survey consists of the following: - The exploration of the site of the road location by test pit or auger borings and the preparation of soil profiles the significant soil layers. The critical depths to bed rock and water table and the extent of adverse ground conditions such as swaps or peat bogs. - The study of all existing information on soil, and ground-water conditions occurring in the vicinity of the proposed road location. - The identification of the various soil types from soil profile characteristics occurring on the proposed road project. - The taking of representative samples of soil and local construction materials (subbase, base course and surfacing materials) for laboratory testing. Road site Exploration:- the field work for this phase of the soil survey consists of making examinations of the soils by means of borings, test pits or road cuttings. Borings for foundation should be deep enough to determine if bed rock, adverse ground (peat) or water conditions are apt to be encountered during the construction of the proposed road. After the boundaries of each soil type are established, sampling sites are selected so that representative samples can be obtained for laboratory test purposes.
  • 15. 11 Equipment for Soil Survey The type of equipment required for making a soil survey. 1. Ouger 2. Rod 3. Tape 4. Sample bags 5. Shovel 6. Pick Soil sampling or selection:- sample of soil or gravel should be obtained from each soil layer (depth) and limited distance with pick and shovel from the proposed test pit selected on the basis of a study auger boring or test pit records. Each sample should be placed in a canvas bag, marked with adequate identification, tied securely and shipped to the laboratory. A sufficient amount and number of samples should be taken to establish the range in test results for what appears to be the same soil layer. Or soils survey should be conducted along the proposed route in order to asses the existing pavement condition including soil extension. Construction materials subbase material (select material source, base course material, surfacing and water should be sampled for laboratory test determination.
  • 16. 12 SECTION I 1. MOISTURE CONTENT AND INDEX TESTS 1.1 Moisture Content (BS1377: Part 2: 1990 and ASTM D2216) 1. Definition The mass of water which can be removed from the soil and aggregate by heating (oven drying) at 105 - 1100c expressed as a percentage of the dry mass. 2. Apparatus - Moisture can (container) - Balance - Oven - Spatula - Pan 3. Procedure Clean and dry the moisture can (container). Make sure that all are marked the same reference no. or letter. a. Weigh each container and record. b. Place the wet sample in the container, the mass of sample to be used as follows: Mass of soil sample 50-300 gm Mass of aggregate sample 300-500 gm c. Weigh wet of sample + container and record d. Place the wet sample + container in the over. Maintain the required temperature normally 105-1100c for 12 - 24 hours. e. Remove the sample from the oven and allow in the air to cool at least 10-15min. f. Weigh the dried sample + container and record.
  • 17. 13
  • 18. 14 4. Calculation:- The moisture content of a soil or aggregate is expressed as a percentage of its dry mass. Moisture content = A - B B - C Where A. Weight of wet sample + Container B. Weight of dry sample + Container C. Weight of Container 1.2 Atterberg Limits 1.2.1 Determining the Liquid Limit of Soil (AASHTO Designation T89-90) 1. Definition: The liquid limit of a soil is the moisture (water) content at which soil passes from the plastic to liquid state as determined by the liquid limit test. 2. Apparatus: a. Mixing (Evaporating dish) about 114mm diameter b. Spatula or peel knife having blade about 76 mm length and 19 mm width c. Motorized liquid limit device d. Grooving tool e. Moisture can (container) f. Balance sensitive to 0.01gm g. Pan (small) h. Drying oven i. Graduated measuring cylinder 10-50ml 3. Sample preparation The soil sample as received sufficient from field - A sample shall be taken from the thoroughly mixed portion of the material passing the No 40(0.425mm) sieve which has been obtained in accordance with the standard method of preparing disturbed soil sample or the standard method of wet preparation of disturbed soil sample for test. Dry preparation - Allow the sample in air to dry at room temperature or in an oven at a temperature not exceeding 600c. Break down aggregations of particles in a mortar
  • 19. 15 using a rubber pestle but avoid crushing individual particles. Place in the cup or dish a sample weighing about more than 100gm. 4. Procedure 4.1 Adjustment of Mechanical Device:- The liquid limit device shall be inspected to determine that the device is in good working order, that the pin connecting the cup is not worn sufficiently to permit side play that the screws connecting the cup to the hanger arm are tight and that a groove has not been worn in the cup through long usage. The grooving tool shall be inspected to determine that the critical dimensions are as shown Fig. 1.1. By means of the gauge on the handle of the grooving tool and the adjustment plat H, Fig 1.1, the height to which the cup is lifted shall be adjusted so that the point on the cup which comes in contact with the base is exactly 1cm (0.3937") above base. The adjustment plate H shall than be well secured by tightening the screws 1. With the gage still in place revolving the crank rapidly several times shall check the adjustment. If the adjustment is correct, a slight ringing sound will be heard when the cam strikes the cam follower. If the cup is raised off the gauge or no sound is heard further adjustment shall be made. The apparatus must be clean and the bowl must be dry and oil free. Check that the grooving tool is clean and dry, and conforms to the correct profile. The machine should be placed on a firm solid part of the bench so that it will not wobble. The position should also be convenient for turning the handle steadily and at the correct speed (two turns per second). Practice against a second's timer with the cup empty to get accustomed to the correct rhythm. 4.2 Mixing:- The soil sample shall be placed in the evaporating (mixing) dish and add sufficient distilled water and mix the soil sample in the mixing dish with the spatula for at least 10min. some soils especially heavy clay may need a longer mixing time up to 45min. When sufficient water has been thoroughly mixed with the soil to form a uniform mass of stiff consistency, a sufficient quantity of
  • 20. 16 this mixture shall be placed in the cap above the spot where the cap rests on the base and shall then be squeezed and spread into the position shown in Fig. 1.2 with as few strokes of the spatula as possible, care being taken to prevent the entrapping of air bubbles within the mass. With spatula the soil shall be leveled and at the same time trimmed to a depth of 10mm at the point of maximum thickness. The excess sample shall be returned to the mixing dish. The sample in the cup of the mechanical device shall be divided by a firm stroke of the grooving tool along the diameter through the centerline of the cum follower so that a clean sharp groove of the proper dimensions will be formed. To avoid tearing of the sides of the groove or slipping of the soil cake in the cup, upto six strokes from front to back or from back to front counting as one stroke shall be permitted. The depth of the groove should be increased with each stroke and only the last stroke should scrape the bottom of the cup. 4.3 Turn the crank handle of the machine at a steady rate of two revolutions per second, so that the bowl is lifted and dropped. Use a second's time if necessary to obtain the correct speed. If a revolution counter is not fitted, count the number of bumps counting aloud if necessary. Continue turning until the groove is closed along a distance of 13mm. The back end of the standard grooving tool serves as a length gauge. The groove is closed when the two parts of the soil come into contact at the bottom of the groove. Record the number of blows required to reach this condition. If there is a gap between two
  • 21. 17
  • 22. 18
  • 23. 19
  • 24. 20 Points of contact continue until there is a length of continuous contact of 13mm, and record the number of blows. 4.4 Remove a slice of soil approximately the width of the spatula extending from edge of the soil. Followed together shall be removed and placed in two suitable containers. The containers and samples shall be weighed and the weight recorded. 4.5 The soil remaining in the cup shall be transferred to the evaporating dish. The cup and grooving tool shall then be washed, clean and dried in preparation for the next trials. 4.6 The foregoing operation shall be repeated for at least two additional portions of the samples to which sufficient water has been added to bring the soil to a more fluid condition. The object of this procedure is to obtain samples of such consistency that at least one determination will be made in each of the following ranges of blows; 1st 25-35, 2nd 20-30, 3rd 15-25. 4.7 Place all the weighed and recorded sample and container in the oven to dry [see Section 1.1 (d-f)]. 4.8 Calculation:- The water content of the soil shall be expressed as the moisture content in percentage of the weight the oven dried mass and shall be calculated as follows. % Moisture content = (A-B) x 100 B-C Where A = weight of wet sample + container B = weight of dry sample + container C = weight of container 4.9 Preparation of flow curve Using a semi-logarithmic chart, plot the moisture content as ordinate (linear scale) against the corresponding number of blows as abscissa (logarithmic scale) and the number of blows as ordinates on the logarithmic scale. The flow curve shall be a straight line drown as. It may be used to determine the liquid limit for a soil with only one test; this procedure is generally called the "one point
  • 25. 21 method" this method has been adopted by ASTM under the designation D423- 66, Liquid limit = WN (N/25) n Where N = number of blows in liquid limit device for 0.5in, groove closure WN = corresponding moisture content n = 0.121 for all soils. The reason for obtaining fairly good results by the one point method is due to the small range of moisture involved for N between 20 and 30. The following table gives the values of (N)/25)0.121 for N=20 to N=30 N (N/25) 0.121 20 0.973 21 0.979 22 0.985 23 0.990 24 0.995 25 1.000 26 1.005 27 1.009 28 1.014 29 1.018 30 1.022
  • 26. 22
  • 27. 23 nearly as possible through the three or more plotted points. This is called the flow curve. 4.10 Liquid Limit Determination:- Draw the ordinate representing 25 blows and where it intersects the flow carve draw the horizontal line to the moisture content axis. Read off this value of moisture content and record it on the horizontal line to the nearest 0.1%. Fig. 1.2 Liquid limit (Casagrande test) Result and Graph 1.2.2 Determining the Plastic Limit and Plasticity Index of Soil (AASHTO Designation T 90-90) Definition:- The moisture content at which a mixture of soil passes from a liquid state to that of a semi-solid state.
  • 28. 24 1. Sample Preparation If the plastic limit analysis required take a quantity of soil weighing about 30- 50gm from the thoroughly mixed portion of the material passing the No 40 (0.425mm) sieve [see section 1.2.1 (3)]. 2. Apparatus 1. Glass plate reserved for rolling of threads. This should be smooth and free from scratches, soil and grease and about 300mm square and 10mm thick. 2. Palette knife or spatula 3. A short length 100mm length 3mm diameter of metal rod 4. Standard moisture content apparatus [section 1.2.1 (2)] 3. Procedure - Prepare chilled or a small portion of thoroughly or mixed sample from the first trial of LL test. - Roll into ball - Roll into thread until crumbling occurs. a. Rolling into a Ball Mould the ball between the fingers and roll between the palms of the hands so that the warmth of the hands slowly dries it. Squeeze an ellipsoidal shape mass. Roll this mass between the fingers and the ground glass plate with just sufficient pressure to roll the mass into a thread of uniform diameter through out its length. Equalize the distribution of moisture, and then form into a thread about 6mm diameter, using the first finger and thumb of each hand. The thread must be intact and homogenous. The pressure should reduce the diameter of the thread from 6mm to about 1/8in or 3mm after between five and ten back and front movements of the hand. Some heavy expansive clays may need more than this because this type of soil tends to become harder near the plastic limit. It is important to maintain a uniform rolling pressure throughout: do not reduce pressure as the thread approaches 3mm diameter. When the diameter of the thread becomes 1/8in (3mm) break the thread into six or eight pieces. Squeeze the pieces together between the thumbs and fingers of both hands into a uniform mass roughly ellipsoidal in shape and re- roll. Continue this alternate rolling to a thread 1/8in. (3mm) in diameter gathering together kneading and re-rolling, until the thread crumbles and
  • 29. 25 occurs surface cracks, under the pressure required for rolling and the soil can no longer be rolled into thread. The crumbling may occur when the thread has a diameter greater than 1/8in. (3mm). This shall be considered a satisfactory end point provided the soil has been previously rolled into a thread 1/8in. (3mm) in diameter. The crumbling will manifest itself differently with the various types of soil. Some soils such as dulotancy tuff, ash etc fall apart in numerous small aggregations of particles. Others may form an outside tubular layer that starts splitting at both ends. The splitting progress toward the middle and finally the thread falls apart in many small ploty particles. This type of samples should no longer be rolled.
  • 30. 26
  • 31. 27 a. Gather the pieces together after crumbling stage is reached. Divide into two parts and place in a suitable moisture can (container), weigh the container and wet soil, record the weight. Place the moisture can and wet sample in the over. Maintain the required temperature normally 105-1100c for 12-24 hours. Remove the sample from oven and allow in the air for about 5-10min. Weigh the dried sample and moisture can and record. b. Calculation Moisture content (A-B) x 100 (plastic limit) B-C Refer section 1.2.1 (4.8) 1.2.3 Plasticity Index The difference between the liquid limit and plastic limit is calculated to give the plasticity index (PI). Eg. Plasticity Index (PI) = Liquid Limit (LL, PL) Plastic Limit (PI). (If LL=40 and PL=21, then PI=40-21=19)
  • 32. 28 1.3 Liquid Limit - With Cone Penetrometer 1.3.1 General This method is used for determining the liquid limit of soil. It is based on the measurement of penetration into the soil of a standardized cone of specified mass. At the liquid limit the cone penetration is 20mm, it requires the same apparatus as is used for bituminous material testing but fitted with a special cone. 1.3.2 Apparatus 1. A flat glass plate, of convenient size, 10mm thick and about 500mm square. 2. Spatulas or palette knives. 3. Cone for the penetrometer, stainless steel or duralumin with smooth polished surface, length approximately 35mm, cone angle 300, sharp point mass of cone and sliding shaft 80g±0.1g. 4. Sharpness gauge for cone, consisting of a small steel plate 1.75mm ±0.1mm thick with a 1.5mm±0.02mm diameter hole accurately drilled and reamed. 5. Metal cups of brass or aluminum alloy 55mm thick and 40mm deep. 6. Metal straight edge about 100mm long. 7. Moisture content apparatus. 8. An evaporating dish (mixing dish), about 150mm diameter. 9. Wash bottle or beaker, containing distilled water. 1.3.3 Sample preparation a. Use of Natural Soil:- When the soil consists of clay and silt with little or no material retained on a No.40 (0.425mm) sieve, it can be prepared for testing from its natural state. Take a representative sample of about 500g of soil and chop into small pieces or shred with cheese grater. Mix with distilled water on a glass plate, using two palette knives. During this process remove any coarse particles by hand or with tweezers. Mix the water thoroughly into the soil until a thick homogeneous paste is formed and the paste has absorbed all the water with no surplus water visible. The mixing time should be at least 10min. with vigorous working of the palette knives. A longer mixing time period up to 45min may be needed for some soils, which do not readily absorb water.
  • 33. 29 Place the mixed soil in an airtight container, such as a sealed polythene bag, and leave to mature for 24 hours. A shorter maturing time may be acceptable for low plasticity clays, and very silty soils could be tested immediately after mixing. If in doubt, comparative trial tests should be performed. In a laboratory with a continuous workload it is good practice to be consistent and allow 24 hours maturing for all soils. The mixed and matured materials is then ready for the tests. b. Wet preparation :- Take a representative sample of the soil at its natural moisture content to give at least 350gm of material passing the No.40 (0.425mm) sieve. This quantity allows for a liquid limit and a plastic limit test. Chop into small pieces or shred with a cheese grater, and place in a weighed beaker, weigh and determine the mass of soil m(g) by difference. Take a similar representative sample and determine its moisture content w(%). The dry mass of soil in the test sample mD(g) can then be calculated from the equation:. mD = 100m 100+w Add enough distilled water to the beaker to just submerge the soil. Break down the soil pieces and stir until the mixture forms slurry. Nest a No. 40 (0.425mm) sieve on a receiver, under a guard sieve eg. No 10 (2mm) sieve if appropriate. Pour the slurry through the sieve or sieves, and wash with distilled water, collecting all the washings in the receiver. Use the minimum amount of water necessary, but continue washing until the water passing the No. 40 (0.425) sieve runs virtually clear. Transfer all the washings passing the sieve to a suitable beaker with out losing any soil particles. Collect the washed material retained on the sieves. Dry in the oven and determine the dry mass mR(g). Allow the soil particles in the beaker to settle for several hour, or overnight. If there is a layer of clear water above the suspension, this may be carefully poured or siphoned off, without losing any soil particles. However if the soil contains
  • 34. 30 water-soluble salts which might influence its properties, do not remove any water accept by evaporation. Stand the container in a warm place or in a current of warm air, so that it can partially dry. Protect from dust. Stir the soil water mixture frequently to prevent local over-drying. Alternatively, excess water may be removed by filtration. When the mixture forms a stiff paste such that the penetration of the cone penetrometr would not exceed 15mm the soil is ready for mixing on the glass plate as described above. No additional curing time is required and the material is ready for the tests. Calculate the percentage by dry mass of soil in the original sample passing the 0.425mm sieve (Pa) from the equation Pa = mD - mR x 100 mD c. Dry preparation:- Allow the soil sample to air dry at room temperature, or in one oven a temperature not exceeding 500c [see section 1.2.1(3)]. 1.3.4 Procedure a. Take a sample of about 300gms-soil paste and place the prepared soil paste on the glass plate. b. Mix the soil paste on the glass with the spatulas for at least 10-min. Some soil especially heavy clays may need a longer mixing time. If necessary add more distilled water so that the first cone penetration reading is about 15mm. c. Press the mixed soil paste into the cup with a palette knife (spatula) taking care not to trap air. Strike off excess soil with the straight edge to give a smooth level surface. d. Lock the cone shaft unit near the upper end of its travel and lower the supporting assembly carefully so that the tip of the cone is within a few mms of the surface of the soil in the cup. When the cone is in the correct position, a slight movement of the cup will just make the soil surface. Lower the stem of the dial gauge to contact the cone shaft and record the reading of the dial gauge to the nearest 0.1mm.
  • 35. 31
  • 36. 32 e. Release (Allow) the cone by pressing the button for a period of 5±1 second timed with a seconds timer or watch. If the apparatus is not fitted with an automatic release and locking device, take care not to jerk the apparatus during this operation. After 5 seconds release the button so as to lock the cone in place. Lower the dial gauge stem to make contact with the top of the core shaft without allowing the pointer sleeve to rotate relative to the stem adjustment knob. Record the reading of the dial gauge to the nearest 0.1mm Record the difference between the beginning and end of the drop as the cone penetration. See Fig. 1.3. f. Lift out the cone and clean it carefully to avoid scratching. g. Add a little distilled water and remix and add a little more wet soil to the cup, taking care not to trap air, make the surface smooth. Repeat section 1.3.3(d). If the second cone penetration differs from the first by less than 0.5mm, the average value is recorded, and proceed to the next h. h. If the second penetration is between 0.5 and 1mm different from the first, a third test is carried out provided that the overall range does not exceed 1mm, the average of the three penetrations is recorded and the content is measured stage (1). i. If the overall range exceeds 1mm, the soil is removed from the cup and re-mixed and the test is repeated from stage C. j. Take a moisture content sample of about not less than 10g, the area penetrated by the cone, using the tip of a small spatula. Place it in a suitable container and determine its moisture content. k. The soil remaining in the cup is re-mixed with the rest of the sample on the glass plate together with a little more distilled water, until a uniform softer consistency is obtained. The cup is scraped out with the square-ended spatula wiped clean and dried, and stages (C-J) are repeated at least three more times, with further increments of distilled water.
  • 37. 33
  • 38. 34 A range of penetration values from about 15mm to 25mm should be covered, fairly uniformly distributed. 1. Calculation The moisture content of the soil from each penetration reading is calculated from the wet and dry weightings as in the moisture content [see section 1.2.1 (4.8)]. Moisture content (%) = (A-B) x 100 B-C Where A = weight of wet sample + container B = weight of dry sample + container C = weight of container Test Results From the graph the moisture content corresponding to a standard cone penetration of 20mm is read off to the nearest 0% reported to the nearest whole number as the liquid limit. See Fig. 1.3 1.4 Choice I General Soil classification 1.4.1 General:- The American Association of State Highway and Transportation Official (AASHTO) system of soil classification is based upon the observed field performance of soil under highway pavements and is widely known and used among highway engineers. 1.4.2 Definition:- Soil classification is systematically grouping or categorizing of soil. It provides a common language to express briefly the general characteristics of soils. 1.4.3 Procedure:- The AASHTO soil classification system is classified into seven (7) major groups A-1 through A-7. Soils classified under groups A-1, A-3 and A-2 are granular (gravels, sand and gravelly clay). Materials with 35% or less passing through a No.200 (0.075mm) sieve. The silt and silty clay materials with more than 35% passing the No.200 (0.075mm) sieve are classified under groups A-4, A-5, A-6 and A-7. After the necessary laboratory tests have been preformed the proper classification for a given material can normally be made without great difficulty. The classification of a specific
  • 39. 35 soil is based upon the results of tests made in accordance with standard methods of soil testing. To classify a soil by Table 1.1 one must proceed form left to right with the required test data available by the process elimination. The first group from the left into which the test data will fit gives the correct classification. To evaluate the performance quality of a soil as a highway subgrade material under this system, a number called the group index is included with the groups and sub-groups of the soil. The group index of a soil may range from 0-20 and is expressed as a whole number. The approximate subgrade and base performance quality of a given soil is inversely proportional to its group index, and it can be expressed by the following empirical relation. Group index (GI) = (F-35%) [0.2+0.005 (LL-40)]+0.01(F-15)(PI-10) Where GI = group index F = percentage of soil passing a No 200 (0.075mm) sieve LL = liquid limit PI = plasticity index The group index is rounded off to the nearest whole number. The group index may also be evaluated with Fig. 1.4 by adding the vertical reading, the vertical reading is obtained from the two charts:  Chart one LL with No. 200 (0.075mm)passing sieve and  Chart two PI with a No. 200 (0.075mm) passing sieve. Add the two values. 1.4.4 Classification Parameters 1. Liquid Limit 2. Plasticity Index 3. Grain Size Analysis Note:- Detail Soil Classification General A-1, A-3, A-2, A-4, A-5, A6 and A-7 1. Granular Materials and Sand: 35% or less passing a No.200 (0.075mm) sieve are A-1, A-3 and A-2.
  • 40. 36 Soil Group A-1 material divided into two subgroups Sieve size % passing LL PI A-1 A-1-a No. 10 No. 40 No. 200 50max 30max 15max - 6 max A-1-b No. 40 No. 200 50max 25max - 6 max 2. Soil Group A-3 Material Sieve Size % Passing LL PI A-3 No. 40 51 min NP NP No. 200 10 max 3. Soil Group A-2 Material Soil Group A-2 material divided into four subgroups Sieve size % passing LL PI A-2 A-2-4 No.200 35 or less 40 max 10max A-2-5 No.200 35 or less 41 min 10max A-2-6 No.200 35 or less 40 max 11 min A-2-7 No.200 35 or less 41 min 11 min 2. Silt and Silty Clay or Heavy Clay Materials: 35% or more passing No. 200 (0.075mm) sieve are A-4, A-5, A-6, and A-7. 4. Soil Group A-4 Material Sieve Size % Passing LL PI A-4 No.200 36 min 40 max 10 min 5. Soil Group A-5 Material Sieve Size % Passing LL PI Soil Group A-5 No.200 36 min 41 max 10 min
  • 41. 37 6. Soil Group A-6 Material Sieve Size % Passing LL PI A-6 No.200 36 min 40 max 11 min 7. Soil Group A-7 Material Sieve Size % Passing LL PI A-7 A-7-5 No.200 36 min 41 min 11 min A-7-6 No.200 36 min 41 min 11 min Group of soil A-7-5 is plasticity Index result less or equal Liquid Limit – 30 (PI less or equal to LL-30) Group of soil A-7-6 is plasticity Index result greater than Liquid Limit result -30 (PI less than LL-30)
  • 42. 38
  • 43. 39 Example:- 1 Liquid Limit = 42 Plasticity Index = 12 Passing No 200 (0.075mm) sieve = 35 Soil classification is A-2-7 (1). Example:- 2 Liquid Limit = 60 Plasticity Index = 30 Passing No 200 (0.075mm) sieve = 36 Soil classification is A-7-5 (5). Example:- 3 Liquid Limit = 49 Plasticity Index = 22 Passing sieve No 200 (0.075mm) = 38 Soil classification is A-7-6 (4). Example:- 4 Liquid Limit or Plasticity Index is NP. Passing sieve No 200 (0.075mm) = 36 Soil classification is A-4 (0). 1.4.5 Soil Fractions 1. Over size (Boulders) - Material retained on 3 inch (75mm) sieve. They should be excluded from the portion of a sample to which the classification is applied but the percentage of such material should be recorded. 2. Gravel - Material passing sieve with 3inch (75mm) and retained on the No 10 (2mm) sieve. 3. Coarse Sand - Material passing the No. 10 (2mm) sieve and retained on No. 40 (0.425mm) sieve. 4. Fine Sand - Material passing the No. 40 (0.425mm) sieve and retained on the No 200 (0.075mm) sieve.
  • 44. 40 5. Silty Clay - Material passing the No. 200 (0.075mm) sieve. The word silt is applied to a fine material having a PI of 10 or less and the term clay is applied to fine material having a PI of more than 10. 1.4.6 Description of Classification Groups A. Granular Materials - Group A-1 - Well graded mixtures of stone fragments or gravel ranging from course to fine with non-plastic or slightly plastic silt binder. - Subgroup A-1-a - Stone fragments and sandy gravel some times with silt. - Subgroup A-1-b - Stone fragments and gravel with some times clayey silt. - Group A-3 - fine sands and non-plastic silt. - Group A-2 - sandy gravel with silt and gravelly clay. - Subgroup A-2-4- and A-2-5- include various granular materials and sandy clayey silt. - Subgroup A-2-6 and A-2-7 include materials similar to those described under subgroups A-2-4 and A-2-5 except that the fine portion contains plastic clay having a higher PI.
  • 45. 41 3. choice II-Soil Classification Definition:- soil classification is systematically grouping or categorizing of soil. It provides a common language to express briefly the general characteristics of soils A. AASHTO Soil Classification System: is classified into 7 major groups A-1 through A-7 classified and under groups A-1, A-3, A-2, A-4, A-5, A-6, A-7 soils. Under groups A-1, A- 2 and A-3 are granular or gravelly clay and sand materials with 35% or less passing through a No. 200 (075mm) sieve. The silt and clay materials with more than 35% passing the No 200 (075mm) sieve are classified under groups A-4, A-5, A-6 and A-7. AASHTO Classification Parameters 1. Liquid Limit 2. Plasticity index 3. Grain size analysis Group A-1 A-2 and A-7 material divided into 4 and 2 sub groups. A-1 A-1-a A-1-b A-2 materials are divided into 4 sub groups. A-2 A-2-4 A-2-5 A-2-6 A-2-7  A-1 material can be used for surfacing, base course and subbase.  A-2 material for subbase and subgrade.  A-4,5,6 and 7 subgrade only. A-7 material is divided into two sub groups A-7 A-7-5 A-7-6
  • 46. 42 A-7-5 Group of Soil Material:- PI is equal to or less than LL-30 A-7-6Group of Material:- PI is greater than LL-30 Examples LL PI Passing Sieve (mm) Soil Classification 2 0.425 0.075 1 42 12 - - 36 A-7-5 (1) 2 70 30 - - 39 A-7-5 (5) 3 30 10 - - 10 A-2-4 (0) 4 41 20 - - 45 A-7-6 (5) 5 NP 20 15 3 A-1-a (1) A-1 Material:- Stone fragments, gravelly and coarse sand with binder of low plasticity or NP. A-2 Materials:- gravelly silt, clay and sand with low and little high plastic material A-3 Material:- Sand A-4,5,6 & 7 Materials:- Silty clay and Same fines with few gravel B. Silty Clay Soil Materials - Group A-4 - The typical material of this group is fine sandy and silty clay sometimes non-plastic material, liquid limit not exceeding 40 and PI not exceeding 10. - Group A-5 - The typical material of this group is similar to that described under group A-4, except that it is usually of diatomaceous or micaceous character and may be highly elastic as indicated by the high liquid limit. - Group A-6 - This typical material is a plastic clay soil. The group includes also mixture of fine clayey soil and the Plasticity Index may be high. - Group A-7 - The typical materials and problems of this group are similar to those described under group A-6 except that they have the liquid limit and the range of group index values is 1 to 20 with increasing values indicating the combined effect of increasing liquid limits and plasticity indexes and decreasing percentages of coarse material. - Subgroup of A-7-5 - includes those materials with moderate plasticity index in relation to liquid limit and which may be highly elastic as well as subject to considerable volume change.
  • 47. 43 - Subgroup of A-7-6 - includes those materials with high plasticity indexes in relation to liquid limit and which are subject to extremely high volume change.  Highly organic soils such as peat and muck are not included in this classification. 1.5 Unified Soil Classification System General Unified classification system is widely used. This system is an out growth of the Airfield classification developed by casagrande and is utilized by the corps of engineers. In this system, soils fall within one of three major categories: curse grained, fine grained and highly organic soils. These categories are further subdivided into 15 basic soil groups. The following group symbols are used in the unified system. G - gravel O - organic S - sand W - well graded M - silt P - poorly graded C - clay U - uniformly graded Pt - peat L - low liquid limit H - high liquid limit Combinations of above letters are used to identify the soils. For expamle, SP is a sand that is poorly graded and CL and CH indicate clays with low and high liquid limits respectively. The essentials of unified classification system are given in Table 1.5.1 and characteristics pertinent of roads and air fields are sown in Table 1.5.2. A. Soil components in the unified classification system are as follows: - Cobbles - above 75mm (3 inch) - Gravel - 75mm to 4.75mm (3inch - No.4) sieve - Coarse sand - 4.75mm to 2mm (No 4 - No. 10) sieve - Medium sand -2mm to 0.425 mm (No 10 to No 40) sieve - Fine sand - 0.425 mm to 0.075mm (No 40 to No 200) sieve - Fine silt and clay - passing 0.075mm (0.075) sieve.
  • 48. 44 B. Laboratory test specified for silts and clays are the determination of the liquid limit and the plastic limit and plasticity index. C. Laboratory test for coarse-grained soils is based on the grain size analysis. Coarse- grained materials are those containing 50% or less passing 0.075 mm (No.200) sieve. Fine grained are those with more than 50% passing 0.075mm (No.200) sieve. After determining its grain size distribution, liquid limit and plasticity index, the soil can be classified using table 1.2 and Fig 1.4. The minus 0.075mm (No. 200) sieve material is "silt" if non-plastic and the liquid limit and plasticity index plot below the "A" line on the plasticity chart (Fig. 1.4) and "clay" if plastic and the liquid limit and plasticity index plot above the "A" line. This holds true for inorganic silts and clays and organic silts, but not for organic clays since they plot below the "A" line. The "A" line is an arbitrarily drawn line on the plasticity chart of Fig. 1.4. The letters in parentheses stand for symbols by which each group is known. A. Coarse Grained Symbols GW-GM, GP-GM,_GW-GC, GP-GC, SW-SM, SW-SC, SP-SM B. Fine Grained Soil Classification with Symbols ML, MI, MH, MV, ME, CL, CI, CH, CV, CE In Ethiopian practice this chart is divided into five zones, giving the following categories for clays and silts. 1. Clays of low plasticity (CL) less than 35, liquid limit or silts of low plasticity (ML) less than 35 liquid limit. 2. Clays or silts of medium plasticity (CI) or (MI), liquid limit from 35 to 50. 3. Clays or silts of high plasticity (CH) or (MH), liquid limit from 50 to 70 4. Clays or silts of very high plasticity (CV) or (MV), liquid limit from 70 to 90 5. Clays or silts or extremely high plasticity (CE) or (ME), liquid limit exceeding 90.
  • 49. 45 Example Liquid Limit = 72 Plasticity Index = 36 Passing No. 200 sieve = 98 Classification is according to the chart (Fig. 1.5.2) = MV. The soil is MV group.
  • 50. 46
  • 51. 47
  • 52. 48 1.6 Determining the Shrinkage Factors and Limit of Soils 1. Scope This procedure furnishes data from which the following soil characteristics may by calculated: (a) Shrinkage Limit (b) Shrinkage Ratio (c) Volumetric change (d) Linear shrinkage A. Determination of Volumetric Shrinkage 2. Apparatus 2.1 Evaporating (mixing) dish about 150mm diameter. 2.2 Spatula or peel knife having a blade above 76mm long and 20mm wide. 2.3 Glass cup about 57mm diameter and 38mm deep with rim ground flat. 2.4 Prong plate, glass or clear acrylic, fitted with three non-corrodible prongs. 2.5 Glass plate, large enough to cover the shrinkage dish. 2.6 Measuring cylinder 25 to 100ml. 2.7 Mercury, rather more than that will fill the glass cup. 2.8 Straight edge, spatula, small tools.
  • 53. 49 2.9 Balance 3000g capacity reading to 0.01g. 2.10 Moisture content can (container). 2.11 Large tray containing a small amount of water to retain any spilled mercury. 2.12 Vaseline 3. Sample preparation Receive sufficient sample from field prepare. About 50g of soil sample passing the 0.425 (No. 40) sieve from natural soil and place the prepared sample in the mixing dish or cup.
  • 54. 50
  • 55. 51 4. Procedure 4.1 Place the prepared soil sample in an evaporating dish and thoroughly mix with distilled water to make into a readily workable plate. Air bubbles must not be included. The moisture content should be somewhat greater than the liquid limit. The consistency should be such as to require about 10 blows of the Casagrande liquid limit apparatus to close the groove or to give about 25-28mm penetration of the cone penetrometer. Add the mixed soil paste to the shrinkage dish so as to fill it about one-third. Avoid trapping of air. Tap the dish on the smooth surface bench surface to cause the soil to flow to the edges of the dish. This should also release any small air bubbles present. The bench should be padded with a few layers of blotting paper or similar material. Add a second amount of soil, about the same as the first and repeat the tapping operation until all entrapped air has been released. Add more soil and continue tapping, so that the dish is completely filled with excess standing out. Strike off the excess with a straight edge and clean off adhering soil from the outside. Immediately after the above, weigh the sample (soil) and dish to 0.01g. Record as m1. 4.2 Drying Allow the sample in the dish to dry in the air for at least 12 hours or 24 hours until its color changes from dark to light. Place it in oven at 600c for 6 hours and continue at 105 - 1100c and dry to constant mass. If the shrinkage curve during drying is required, make a series of volume measurement at suitable intervals before drying in the oven. Leave the soil in the shrinkage dish exposed to warm air, and when it has shrunk away from the dish and can be safely handled, determine its volume and mass. Place the soil- pat on a flat surface to dry further and repeat the measurements until the color changes from dark to light. Then dry in the oven.
  • 56. 52 4.3 Weighing Dry Mass Cool in a dessicatoor or in air and weigh the dry soil and dish or container to 0.01g. Record ad md. 4.4 Measurement of Volume Remove the dried soil-pat carefully from the shrinkage dish. It should be intact and be kept long enough to dry in air before transferring to the oven. Place the glass cup in a clean evaporating dish standing on the large tray. Fill the cup to overflowing with mercury, and remove the excess by pressing the glass prong plate firmly on top of the cup. Avoid trapping air under the glass plate. Carefully remove the prong plate, and brush off any mercury drops adhering to the glass cup. Place the cup into another lean evaporating dish without spilling any mercury. Place the soil-pat on the surface of the mercury press the three prongs of the prong plate carefully on the sample so as to force it under the mercury Fig… Avoid trapping any air; press the plate firmly on to the dish. Displaced mercury will be filled in the evaporating dish. Brush off any droplets of mercury adhering to the cup into the dish. Transfer all the displaced mercury to the measuring cylinder and record its volume (Vd). This is equal to the volume of the dry soil-pat. 4.5 Measure the dish volume and weight. Clean and dry the shrinkage dish and weigh it to 0.01g (m2). Its internal volume is determined by measuring the volume of mercury held. Place the dish in on evaporating dish and fill it to overflowing with mercury. The evaporating dish will catch the overflow. Place the small glass plate firmly over the top of the shrinkage dish so that excess mercury is displaced, but avoid trapping any air. Remove the glass plat carefully and transfer the mercury to the 25ml-measuring cylinder. Record the volume of mercury in ml, which is the volume of the shrinkage dish (V1).
  • 57. 53 4.6 Calculations Calculate the moisture content of the initial wet soil-pat, w1 from the equation. Moisture content (w1) = (M1-Md) x 100 Md Dish No. A B C Wt of dish + wet soil (m1) Wt of dish + dry soil (m2) Wt of dish (m1) Wt of water (m1-m2) (m4) Wt of wet soil (m1-m3) (m6) Volume of dish (V1) Volume of dry soil (V2) Volume Change (V1-V2) (V3) Shrinkage limit (Ws) can then be calculated from the equation, Moisture content (Wo) = (m1-m2) x 100 m5(m2-m3) Where V1 = volume of wet soil (dish) V2 = volume of dry soil-pat m5 = mass (wt) of dry soil The shrinkage ratio, Rs, can be calculated from Rs = ms V2
  • 58. SABA Engineering Plc. P.O.Box 62668 Addis Ababa, Ethiopia. Tel. 34 10 65/34 16 17/34 30 04 Fax.. 34 12 30/34 16 17 E-mail sava.eng@telecom.net.et 54 SHRINKAGE LIMIT TEST (VOLUMETRIC) Lab No. Dish No. A B C A. Wt. of dish and wet soil 48 47.5 48.2 B. Wt. of dish and dry soil 36 35.8 36 C. Wt. of dish 10 9 10 D. Wt. of water (A-B) 12 11.7 12.2 E. Wt. of dry soil (B-C) 26 25 26 F. Volume of dish 13 10.8 13 G. Volume of displaced mercury 8 6.4 8 H. Volume of change cc (F-G) 5 5 5 I. D – H 7 6.7 7.2 Shrinkage Limit (I/E) x 100 26.9 26.8 27.7 Shrinkage Ration (E/G) 3.25 3.91 3.25
  • 59. 55 b. Linear Shrinkage Definition:- This test gives the percentage linear shrinkage of a soil. It can be used for soils of low plasticity, including silts, as well as for clays. 1. Apparatus 1.1 Non-corrodible metal mould (Brass), 140mm long and 25mm in diameter 1.2 Flat glass plate as for the liquid limit test 1.3 Palette knives 1.4 Petroleum jelly 1.5 Vernier calipers 1.6 Moisture content apparatus 2. Procedure 2.1 Preparation of mould:- Clean and dry the mould. Apply a thin film of Vaseline or petroleum jelly to the inner surfaces to prevent soil from sticking. 2.2 Preparation of sample About 200g of soil sample passing 0.425mm (No.40) sieve is prepared from soil. This proportion of the original sample passing the 0.425mm (No.40) sieve is recorded. Place the soil in the mixing dish and mix thoroughly with distilled water, as the liquid limit test. Continue mixing until it becomes a smooth homogenous paste at about the liquid limit. This is not critical, but it may be checked by using the cone penetrometer, which should give a penetration of about 20mm.
  • 60. 56 2.3 Place the paste in the mould, avoiding the trapping of air as far as possible, so that the mould is slightly over filled. Tap it gently on the bench to remove any air pockets. Level (trim) off along the top edge of the mould with a spatula or straight edge. Wipe off any soil adhering to the rim of the mould. 2.4 Leave the mould and soil exposed to the air but in a draught-free position so that the soil can dry slowly. When the soil has shrunk away from the walls of the mould, it can be transferred to an oven set at 600c. When shrinkage has virtually ceased, increase the drying temperature to 105 - 1100c to complete the drying. 2.5 Allow the mould and soil to cool in a dessicator, measure the length of the bar of soil with the caliper, making two or three readings and taking the average (LD). If the specimen is curved during drying, remove it carefully from the mould and measure the lengths of the top and bottom surfaces. Take the mean of these two lengths as the dry length as (LD).
  • 61. 57 If the specimen has fractured in one place, two portions can be fitted together before measuring the length. If it has cracked badly, and the length is difficult to measure, repeat the test using a very slower drying rate leaving the sample and mould longer in air (about more than 24 hours) before transferring to the oven. 2.6 Calculation Calculate the linear shrinkage (LS) as a percentage of the original length of the specimen from the equation, LS = (1-LD) x 100 LO Where: LO = original length of the mould LD = length of dry specimen Linear Shrinkage Limit Inician Length (Lo) - wet Final Length (Ld) - dry SL = Lo - Ld x 100 LD Results The Linear Shrinkage of the soil is reported to the nearest whole Number
  • 62. 58 . AMOUNT OF MATERIAL FINER THAN NO.200(0.075mm) SIEVE IN AGGREGATE AASHTO DESIGNATION T-11 1. Scope This method of test covers a procedure for the determination of the quantity of aggregate finer than a standard No. 200 (0.075mm) sieve by washing. This procedure may not determine the total amount of material finer than the No. 200 (0.075mm) sieve. Such a determination may be made by combining washing and dry sieving as required in the sieve analysis of fine and coarse aggregate. 2. Apparatus 1.1 Sieves - No. 16 and No. 200 (0.075) sieves. The sieves shall be of woven wire-cloth construction, conforming to the requirements of AASHTO Designation M-92. 1.2 Container - a pan or vessel of a size sufficient to contain the sample, when covered with water, and to permit vigorous agitation without an advertent loss of any art of the sample or water. 1.3 Balance - A balance with a capacity of 2000gm and sensitive to 0.1gm. 1.4 Scale - A heavy duty scale with a capacity of at least 50 lb and sensitive to 0.1 lb. 1.5 Drying Oven - an oven capable of maintaining a uniform temperature of 230 ± 90F. 2. Test Sample The test sample shall be selected from material which has been thoroughly mixed and which contains sufficient moisture to prevent segregation. Representative samples shall weigh, after drying, not less than the amount indicated in the following table.
  • 63. 59 Maximum Sieve Size Minimum Sample (Mass)Weight No. 4 500gm 3/8 inch 1000gm ¾ inch 2500gm 1 ½ inch or over 5000gm
  • 64. 60 3. Test Procedures Dry the test sample to constant weight (± 16 hours) at a temperature of 230±90F, and weigh the sample to the nearest 0.1 percent. Place the sample in a suitable container, and cover the sample with water. Agitate the contents of the container by vigorous stirring with a large spoon or rod, and pour the wash water over the nested sieves, arranged with the No. 200 sieve on the bottom. The agitation should be sufficiently vigorous so that all particles finer than the No. 200 sieve are brought into suspension and are subsequently washed through the nested sieve. Be careful to avoid loss of the coarser particles. Repeat this washing operation until the wash water is clear. If the material consists of clay, it may be advantageous to let is soak 16 to 20 hours and to add a detergent to assist deflocculation. In the case of soil samples, it is often advantageous to separate the sample on the No. 4 sieve. The material passing the No.4 sieve may be washed as outlined above. The material passing the No. 4 sieve may be washed as outlined above or by means of a suitable mechanical washing device. Return all material retained on the nested sieves to the washed sample. Dry the sample to constant weight (± 16 hours) at a temperature of 230±90F, and weight the sample to the nearest 0.1 percent. Pan - drying shall be permissible when oven - drying is impracticable or impossible. However, in no case shall a sample be heated in excess of 2390F. 4. Calculation The percentage of material finer than the No. 200 sieve shall be calculated as follows: F = W - W1 x 100 W Where F = the percent of material finer than the No. 200 sieve. W = the original dry weight of the sample W1 = the dry weight of the sample after washing. 5. Precautions The No. 200 (0.075) sieve is extremely delicate, and should be handled accordingly. In no event should wire brushes be used on this sieve. Take care to avoid loss of sample material during washing and during transfer of material from the nested sieves to the washed sample.
  • 65. 61 Standard Method of Mechanical Analysis of Soils AASHTO DESIGNATION T88 - 57 1. Scope This method describes a procedure for the quantitative determination of the distribution of particles size in soils. 2. Apparatus The apparatus shall consist of the following: Balance - A balance sensitive to 0.1gm for weighing small samples; for large samples, the balance is to be sensitive to within 0.1 percent of the weight of the sample to be tested. Stirring apparatus - a mechanically operated stirring apparatus consisting of an electric motor suitability mounted to turn a vertical shaft at a speed not less than 10,000 revolutions per minute without load, a replaceable stirring paddle made of metal, plastic or hard rubber similar to the design shown in Figure 1, and a dispersion scup conforming to either of the designs shown in Figure 2. (Alternate b) Dispersing Device - An air - jet type dispersing device similar to either of the designs shown in Figure 3. Hydrometer - A hydrometer of the exact size and shape shown in Figure 4, the body of which has been blown in a mold to assure duplication of all dimensions, and equipped with either scale a or scale B. Scale A shall be graduated form -5 to +60 gm of soil per liter, and hydrometers equipped with this scale shall be identified as 152H. It shall be calibrated on the assumption that distilled water has a specific gravity of 1.000 at 680F and that the soil in suspension has a specific gravity of 2.65. Scale B shall be graduated from 0.995 to 1.038 specific gravity and calibrated to read 1.000 in distilled water at 680F (200c). Hydrometers equipped with this scale shall be identified as 151H. A glass graduate 18 inches in height, 2 ½ inches in diameter, and graduated for a volume 1000ml. Thermometer - A Fahrenheit thermometer accurate to 10F (0.50c). Sieve - A series of sieves of square mesh woven wire cloth, conforming to the requirements of standard specifications for sieves for Testing purposes (AASHTO Designation: M92). The sieves required are as follows:
  • 66. 62 2 inch sieve (50mm) 1 ½ inch sieve (37.5mm) 1 inch sieve (25mm) ¾ inch sieve (20mm) 3/8 inch sieve (10mm) No. 4 sieve (4.75) No. 10 sieve (2mm) No. 40 sieve (0.425) No. 200 sieve (0.075mm) Water Bath or Constant Temperature Room A water bath or constant temperature room for maintaining the soil suspension at a constant temperature during the hydrometer analysis. A satisfactory water bath is an insulated than which maintains the suspension at a convenient constant temperature as near 680F (20.00c) as the room and faucet water temperature will permit. Such a device is illustrated in Figure 5. In cases where the work is performed in a room at an automatically controlled constant temperature, the water bath is not necessary and subsequent reference to a constant temperature bat shall be interpreted as meaning either a water bath or a constant temperature room. Beaker - A beaker of 250 ml Capacity 3. Sample The sample required for this test shall include all of the material on the No. 10 (2,000 micron) sieve, plus a 60 or 110gm representative portion of the fraction passing the No. 10 sieve, the larger quantity being required only when this fraction is very sandy. These samples shall be obtained in accordance with the Standard method of Dry Preparation of Disturbed Soil Samples Test (AASHTO DESIGNATION: T87), or the Standard Method of Wet Preparation of Disturbed Soil Samples for test (AASHTO DESIGNATION: T146). 4. Sieve Analysis of Fraction Retained on No. 10 sieve The portion of the sample retained on the No. 10 sieve shall be separated into a series of sizes by the use of the 2 inch, 1 ½, 1 ½ - inch, 1 - inch, ¾ - inch, 3/8 - inch, and the No. 4 sieve.
  • 67. 63 The sieving operation shall be conducted by means of a lateral and vertical, accompanied by jarring action so as to keep the sample moving continuously over the surface of the sieve. In no case shall fragments in the sample be turned or manipulated through the sieve by hand. Sieving shall be continued until not more than 1 percent by weight of the residue passes any sieve during 1 minute when sieving machines are used, their thoroughness of sieving shall be tested by comparison with hand methods of sieving as above described. The portion of the sample retained on each sieve shall be weighed and the weight recorded although it shall be permissible to record the accumulated weights as the contents of each successive sieve is added to the fractions previously deposited on the scales pan.
  • 68. 64 HYDROMETER AND SIEVE ANALYSIS OF FRACTION PASSING THE NO.10 SIEVE 5. Hygroscopic Moisture A 10gm portion of the fraction of the sample passing the No.10 sieve shall be used for the determination of the hygroscopic moisture. The portion of the sample shall be weighed, dried to constant weight in an oven at 1100c (2300F), weighed, and the results recorded. 6. Dispersion of Soil Sample Approximately 50 grams of most soil or 100 grams of very sandy soils shall be taken from the fraction passing the No. 10 sieve by use of a riffle sampler, weighed, placed in a 250ml, breaker, covered wit 125ml of stock solution of the selected dispersing agent, stirred thoroughly with a glass rod, and allowed to soak for a minimum of 12 hours. Any of the four dispersing agents listed in Table 1 may be used. The stock solution shall be prepared by dissolving the quantity of the salt given in the table in sufficient distilled water to make a liter of solution. After soaking, the contents of the beaker shall be washed into one of the dispersion cups shown in Figure 2, distilled water added until the cup is more than half full, and the contents dispersed for a period of 1 minute in the mechanical stirring apparatus. 7. Alternate Method for Dispersion The representative soil sample shall be weighed and placed in a 250ml beaker, covered with 125ml of the stock solution of the selected dispersing agent specified in section 6, and allowed to soak for a minimum of 12 hours. The air jet dispersion apparatus shall be assembled as shown in fig 3 without the cover cap in place. The needle value controlling the fine pressure shall be opened until the pressure gauge indicates one pound per square inch air pressure. The initial air pressure is required to prevent the soil water mixture from entering the air - jet chamber when the mixture is transferred to the dispersion cup. After the apparatus is adjusted, the soil water mixture shall be transferred from the beaker to the dispersion cup, using a wash bottle to assist in the transfer operation.
  • 69. 65 The volume of the soil - water mixture in the dispersion cup shall not exceed 250ml. The cover containing the baffle late shall be placed upon the dispersion cup and the needle value opened until the pressure gauge reads 20 pounds per square inch. The soil - water mixture shall be dispersed for 5, 10 or 15 minutes depending upon the plasticity index of the soil. Soils with a PI of 5 or less shall be dispersed from 5 minutes; soils with a PI between 6 and 20 for 10 minutes; and soils with a PI greater than 20 for 15 minutes. Soils containing large percentages of mica need be dispersed for 1 minute only. After the dispersion period is completed, the needle value shall be closed until the pressures gauge indicates one pound per square inch. The cover shall be removed and all adhering soil particles washed back into the dispersion cup. The soil-water suspension shall then the washed into the 1000ml glass graduate and the needle value closed.
  • 70. 66 8. Hydrometer Test After dispersion, the mixture shall be transferred to the glass graduate and distilled water having the same temperature as the constant temperature bath added until the mixture attains a volume of 1000ml. The graduate containing the soil suspension shall then be placed in the constant temperature bat. When the soil suspension attains the temperature of the bath, the graduate shall be removed and its contents thoroughly shaken for 1 minute, the palm of the hand being used as a stopper over the mouth of the graduate. At the conclusion of this shaking, the time shall be recorded, the graduate placed in the bat, and readings taken with the hydrometer at the end of 2 minutes. The hydrometer shall be read at the top of the meniscus formed by the suspension around its stem. If hydrometer with scale A is used, it shall be read to the nearest 0.5gm/liter. Scale B shall be read to the nearest 0.0005 specific gravity. Subsequent readings shall be taken at intervals of 5, 15, 30, 60, 250, and 1440 minutes after the beginning of sedimentation. Readings of the thermometer placed in the soil suspension shall be made immediately following each hydrometer reading and recorded.
  • 71. 67
  • 72. 68
  • 73. 69 After each reading the hydrometer shall be very carefully removed from the soil suspension and placed with a spinning motion in a graduate of clean water. About 25 or 30 seconds before the time for a reading, it shall be taken for a clean water, and slowly immersed in the soil suspension to assure that it comes to rest before the appointed reading time. 9. Sieve Analysis At the conclusion of the final reading of the hydrometer, the suspension shall be washed on a No.200 (74 micron) sieve. That fraction retained on the No.200 sieve shall be dried and a sieve analysis made, using the following sieves: No.40, No.60 and No. 200. CALCULATIONS 10.Percentage of Hygroscopic Moisture The hygroscopic moisture shall be expressed as a percentage of the weight of the oven-dried soil and shall be determined as follows: Percentage of hygroscopic moisture = W - W1 x 100 W1 Where W = weight of air - dried soil, and W1 = weight of oven - dried soil To correct the weight of the air - dried sample for hygroscopic moisture, the given value shall be multiplied by the expression. 100 __ 100 + percentage of hygroscopic moisture 11.Coarse Material The percentage of coarse material shall be calculated from the weight of the fractions recorded during the sieving of the material retained on the No.10 sieve, in accordance with section 4, and the total weights recorded during the preparation of the sample, in accordance with the Standard Method of Dry Preparation of Disturbed Samples for Tests (AASHTO DESIGNATION: 87). The percentage of coarse material retained on the No.10 sieve shall be calculated as follows: From the weight of the air - dried total sample, subtract the weight of the air -
  • 74. 70 dried total sample, subtract the weight of the oven - dried fraction retained on the No.10 sieve. The difference is assumed to equal the weight of the air dried fraction passing the No.10 sieve (Note 1). NOTE 1: According to this assumption no hygroscopic moisture is contained in the air - dried particles retained on the No.10 sieve, when as a matter of fact a small percentage of moisture may be present in this fraction. This amount of moisture, compared with that held in the pores of the fraction passing the No.10 sieve is relatively small. Therefore, any error produced by the assumption as stated may be considered negligible in amount. The weight of the fraction passing the No.10 sieve shall be corrected for hygroscopic moisture as indicated in section 10. To this value shall be added the weight of the oven - dried fraction retained on the No.10 sieve to obtain the weight of the total test sample corrected for hygroscopic moisture. The fractions retained on the No.10 and coarser sieves shall be expressed as percentages of this corrected weight. 12.Percentage of Soil in Suspension Hydrometer readings made at temperatures other than 680F shall be corrected by applying the appropriate composite correction from one of the following tables. Tables 151H and 152H list composite correction for hydrometer 151H and 152H to account for the different dispersing agents, temperature variations from 680F, (20.00c), and height of meniscus on the stem of hydrometer. The percentage of the dispersed soil is suspension represented by different corrected hydrometer readings depends upon both the amount and the specific gravity of the soil dispersed. The percentage of dispersed soil remaining in suspension shall be calculated as follows: For hydrometer 152H, P = Ra x 100 W Where : p = Finer R = Corrected hydrometer reading W = Mass of dry soil a = Constant depending on the density of the suspension
  • 75. 71
  • 76. 72
  • 77. 73 For hydrometer 151H, P = 1606 (R - 1)a x 100 W Where, P = Percentage of originally dispersed soil remaining in suspension R = Corrected hydrometer reading W = Weight in grams of soil originally dispersed minus the hygroscopic moisture and a = Constant depending on the density of the suspension. For an assumed value of G for the specific gravity of the soil, and water density of 1.000 at 680F (20.00c), the value "a" may be obtained by the formula. A = 2.6500 - 1.000 x G 2.6500 G-1.0 The value of "a", given to two decimal places are shown in table 2. TABLE 2 - Values of a, for different specific gravities Specific Gravity, G Constant, a 2.95 0.94 2.85 0.96 2.75 0.98 2.65 1.00 2.55 1.02 2.45 1.05 2.35 1.08 Table 151H and 152H It is sufficiently accurate for ordinary tests to select the constant for the specific gravity nearest to that of the particular soil tested. To convert the percentages of the soil in suspension to percentages of the total test sample including the fraction retained on the No.10 sieve, the percentage of originally dispersed soil remaining in suspension shall be multiplied by the expression. 100 - Percentage retained on No.10 sieve 100
  • 78. 74 13.Diameter of soil particles in suspension The maximum diameter, d, of the particles in suspension, corresponding to the percentage indicated by a given hydrometer reading, shall be calculated by the use of stocks' law. According to stocks law: d = √ 30nL 980(G - G1)T Where d = maximum grain diameter in millimeters N = Coefficient of viscosity of the suspending medium (in the case water) in poises varies with changes in temperature of the suspending medium. L = distance in cm through which soil particles settle in a given period of time. T = time in minutes, period of sedimentation G = specific gravity of soil particles and G1 = specific gravity of the suspending medium (approximately 1.0 for water) The maximum grain diameter in suspension for assumed conditions and corresponding to the periods of sedimentation specified in this procedure are given in Table 3. These grain diameters shall be corrected for the conditions of test applying the proper correction factors as described and explained below. Table 3: Maximum Grain Diameter in Suspension under Assumed Conditions Time (Min.) Max Grain Diameter (Mm) 2 0.040 5 0.026 15 0.015 30 0.010 60 0.0074 250 0.0036 1440 100015
  • 79. 75 The grain diameters given in Table 3 are calculated according to the following assumptions: L, the distance through which the particles fall is constant and equal to 17.5cm n, the coefficient of viscosity equals 0.01005 poise, that of water at 680F. G, the specific gravity of the soil is constant and equal to 2.65. Figure 6 The grain diameter corrected for other than the assumed conditions shall be obtained by the formula. D = d' X KL XDGXDa Where in d = corrected grain diameter in mm d' = grain diameter obtained from table 2 KL = correction factor obtained from figure 6. When the hydrometer reading not adjusted for composite correction is used for the ordinate reading Kg = correction factor obtained from figure 7A. Kn = correction factor obtained from figure 7B. The coefficient Kg and Ka are independent of the shape and position of the hydrometer and are as shown in Figures 7A and 7B. Figure 7A and 7B 14.Fine Sieve Analysis The percentage of the dispersed soil sample retained on each of the sieves in the sieve analysis of the material washed on the No.200 shall be obtained by dividing the weight of fraction retained on each sieve by the over-dry weight of the dispersed soil and multiplying by 100. The percentage of the total test sample, including the fraction retained on the No.10 (2000 microns) sieve, shall be obtained by multiplying these values by the expression.
  • 80. 76 100 minus the percentage retained on No.10 sieve 100
  • 81. 77
  • 82. 78 15. Plotting The accumulated percentages of grains of different diameters shall be plotted on semi logarithmic paper to obtain a "grain size accumulation curve," such as that shown in figure 8. Figure 8 16. Report 16.1 The results, read from the accumulation curve, shall be reported as follows: a) Particles larger than 2mm Percent b) Coarse sand, 2.0 to 0.42mm Percent c) Fine sand, 0.42 to 0.074mm Percent d) Silt, 0.074 to 0.005mm Percent e) Clay, smaller than 0.005mm Percent f) Colloids, smaller than 0.001mm Percent 16.2 The results complete mechanical analysis furnished by the combined sieve and hydrometer analysis shall be reported as follows. SIEVE ANALYSIS Sieve Size Percent Passing 2inch (50mm) 1 ½ inch (37.5mm) 1 inch (25mm) ¾ inch(20mm) 3/8 inch (10mm) No.4 (4.75mm) No.10 (2mm) No.40 (0.425mm) No.200 (0.075mm)
  • 83. 79 HYDROMETER ANALYSIS Smaller than Percent 0.02mm 0.005mm 0.001mm For materials examined for any particular type of work or purpose, only such fractions shall be reported as are included in the specification or other requirements for the work or purpose.
  • 84. SABA Engineering Plc. P.O.Box 62668 Addis Ababa, Ethiopia. Tel. 34 10 65/34 16 17/34 30 04 Fax.. 34 12 30/34 16 17 E-mail sava.eng@telecom.net.et 80 Mechanical Analysis 1. Sieve Analysis Sieve Site (mm) Weight retained gm % Retained % Passing 75 - 63.5 - 50 - 37.5 - 25 600 23.83 76 20 480 19.06 57 12.5 360 14.3 43 9.5 278 11.04 32 4.7 260 10.33 21 2 60 2.38 19 Pan 480 19.06 Total 2518 100 2. Specific gravity = 2.67 3. Hygroscopic Moisture a) Wt. of wet sample = 50 b) Wt. of dry sample = 48 c) % dry sample b/a x 100 = 96 Coputed dry Wt. cxa = 48gm 100 4. Sample Pass 2mm Sieve Weight Retain % Retained % Passing 0.425 10 20.83 15.0 0.250 8 16.7 12 0.075 6 12.5 9.5
  • 85. 81 2. Hydrometer (152H) Observed time Sedimentation Min (Elapsed time) Hydrometer Reading Temp. 0F/0c Diameter mm Corrected Reading 680F % finer P=Ra/w*100 Diameter mm 0 70 2 27 70 0.0395 20.5 42.52 5 25 70 0.0256 18.5 38.37 0.02 15 23 70 0.0148 16.5 34.22 30 20 71 0.0101 13.7 28.41 60 17 71 0.00692 10.7 22.19 0.005 250 15 71 0.00354 8.7 18.04 0.002 1440 12 70 0.00144 5.5 11.41 0.001 3. Report A B 1. Particles larger than 4.75mm 76% b. Smaller than % passing 2. Coarse sand 4.75-0.425mm 10% 0.02mm 7.2 3. Fine sand 0.425-0.075mm 5% 0.005mm 4.2 4. Silt 0.075-0.002mm 6.50% 0.001mm 2.2 5. Clay smaller than 0.002mm 2.50%
  • 86. 82
  • 87. 83 SPECIFIC GRAVITY OF SOILS AASHTO DESIGNATION: T 100 - 75 (1982) (ASTEM DESIGNATION: d 854 - 58 (1972)) 1. SCOPE 1.1This method of test is intended for determining the specific gravity of soils by means of a pycnometer. When the soils is composed of particles larger than the 4.75mm (No.4) sieve, the method outlined in the Standard Method of Test for Specific Gravity and Absorption of Coarse Aggregate (AASHTO T 85) shall be followed. When the soil is composed of particles both large and smaller than the 4.75mm sieve, the sample shall be separated on the 4.75mm sieve and the appropriate method of test used on each portion. The specific gravity value for the soil shall be the weighted average of the two values. When the specific gravity value is to be used in calculations in connection with the hydrometer portion of the Standard Method of Mechanical Analysis of Soils (AASHTO 88) it is intended that the specific gravity test be made on that portion of the soil which passes the 2.00mm (No.10) or 0.425mm (No.40) sieve, as appropriate. 2. DEFINITION 2.1Specific Gravity - Specific gravity is the ration of the mass in air of a given volume of a material at a stated temperature to the mass in air of an equal volume of distilled water at a stated temperature. 3. APPARATUS The apparatus shall consist of the following: Pycnometer - Either a volumetric flask having a capacity of at least 100ml or a stoppered bottle having a capacity of at least 50ml (Note 1). The stopper shall be of the same material as the bottle, and of such size and shape that it can be easily inserted to a fixed depth in the neck of the bottle, and shall have a small hole through its center to permit the emission of air and surplus water. Note 1 - The use of either the volumetric flask or the stoppered bottle is a matter of individual preference, but in general, the flask should be used when a larger sample that can be used in the stoppered bottle is needed due to maximum grain size of the sample.
  • 88. 84 Balance - Either a balance sensitive to 0.01g for use with the volumetric flask, or a balance sensitive to 0.001g for use with the stoppered bottle. Desiccator - A desiccator, about 8 in. (approximately 200mm) in diameter containing anhydrous sillca gel or other suitable desiccant. Oven - A thermostatically controlled drying over capable of maintaining a temperature of 110±5c (230±90F). Thermometer - A thermometer covering the range of 0-500c (32 - 1220F), readable and accurate to 10c (20F). 4. GENERAL REQUIREMENTS FOR WEIGHING 4.1When the volumetric flask is used in the specific gravity determination all masses shall be determined to the nearest 0.01g. When the stoppered bottle is used in the specific gravity determination all masses shall be determined to the nearest 0.001g. 5. CALIBRATION OF PYCNOMETER The pycnometer shall be cleaned, dried, weighed, and the mass recorded. The pycnometer shall be filled with distilled water (Note 2) essentially at room temperature. The mass of the pycnometer and water, Wa, shall be determined and recorded. A thermometer shall be inserted in the water and its temperature Ti determined to the nearest whole degree. NOTE 2 - Kerosene is a better wetting agent than water for most soils and may be used in place of distilled water for oven - dried samples. From the mass W1 determined at the observed temperature Ti a table of vales of masses Wa shall be prepared for a series of temperatures that are likely to prevail when masses Wb are determined later (Note 3). These values of Wa shall be calculated as follows: Wa (at Tx) = density of water at Tx X (Wa (at Ti) - Wf) + Wf Density of water at Ti Wa = mass of the pycnometer and water, in grams Wf = mass of pycnometer, in grams Ti = observed temperature of water, in degrees Celsius, and Tx = any other desired temperature, in degrees Celsius.
  • 89. 85 NOTE 3 - The method provides a procedure that is most convenient for laboratories making many determinations with the same pycnometer. If no equally applicable to a single determination, bringing the pycnometer and contents to some designated temperature when masses Wa and Wb are taken, requires considerable time. It is much more convenient to prepare a table of masses Wa for various temperatures likely to prevail when masses Wb are taken. It is important that masses Wa and Wb be based on water at the same temperature. Values for the relative density of water at temperatures form 18 to 300c are given in table 1. 6. SAMPLE The soil to be used in the specific gravity test may contain its natural moisture or be oven - dried. The mass of the test sample on an oven - dry basis shall be at least 25g when the volumetric flask is to be used, and at least 10g when the stoppered bottle is to be used. Samples containing natural moisture - When the sample contains its natural moisture, the mass of the soil, Wo, on an oven - dry basis shall be determined at the end of the test by evaporating the water in an oven maintained at 110±50c (230±90F) (Note 4). Samples of clay soils containing their natural moisture content shall be dispersed in distilled water before placing in the flask, using the dispersing equipment specified in AASHTO T 88. Oven - Dried Samples - When an oven - dried sample is t be used, the sample shall be dried for at least 12h, or to constant mass Vo±50c (230±90F) (Note 4), transferred to pycnometer and weighed. The sample shall then be soaked in distilled water for at least 12h. NOTE 4 - Drying of certain soils at 1100c may bring about loss of moisture of composition or hydration, and in such cases drying shall be done, if desired, in reduced air pressure and at a lower temperature. 7. PROCEDURE The sample containing natural moisture shall be placed in the pycnometer, care being taken not to lose any of the soil in case the mass of the sample has been determined. Distilled water shall be added to fill the volumetric flask about three - fourths full on the stoppered bottle about half full. Entrapped air shall be removed by either of the following methods:
  • 90. 86 1. By subjecting the contents to a partial vacuum (air pressure not exceeding 100mm of mercury) or 2. By boiling gently for at least 10min. while occasionally rolling the pycnometer to assist in the removal of the air. Subjection of the contents to reduced air pressure may be done either by connecting the pycnometer directly to an aspiration or vacuum pump, or by use of a bell jar. Some soils boil violently when subjected to reduced air pressure. It will be necessary in those cases to reduce the air pressure at a slower rate or to use a larger flask samples that are heated shall be cooled to room temperature. The pycnometer shall then be filled with distilled water and the outside cleaned and dried with a clean dry cloth. The mass of the pycnometer and contents, Wb, and the temperature in degrees Celsius, Tx, of the contents shall be determined, as described in section 4. (Note 5) NOTE 5 - The minimum volume of slurry that can be prepared by dispersing equipment specified in AASHTO T88 is such that a 500ml flask is needed as pycnometer. 8. CALCULATION AND REPORT 8.1 The specific gravity of the soil, based on water at a temperature Tx, shall be calculated as follows: Specific Gravity, Tx/TxC = Wo Wo + (Wa + Wb) Where Wa = mass of sample of oven - dry soil, in grams Wa = mass of pycnometer filled with water at temperature Tx (Note 6), in grams Wb = mass of pycnometer filled with water and soil at temperature Tz, in grams and Tx = temperature of the contents of the pycnometer when weight Wb, was determined, in degrees Celsius. NOTE 6 - This value shall be taken from the table of values of Wa prepared in accordance with 5.1 for the temperature prevailing when mass Wb was taken. 8.2 Unless otherwise required, specific gravity values reported shall be based on water at 200c. The value based on water at 200c shall be calculated from the value based on water at the observed temperature Tx, as follows:
  • 91. 87 Specific gravity, Tx/200c = KX specific gravity, Tx/Tx0c, where: K = a number found by dividing the relative density of water at temperature Tx by the relative density of water at 200c. Values for a range of temperatures are given in Table 1. 8.3 When it is desired to report the specific gravity value based on water at 40c, such a specific gravity value may be calculated by multiplying the specific gravity value at temperature Tx by the relative density of water at temperature Tx. 8.4 When any portion of the original sample of soil is eliminated in the preparation of the test sample, the portion of which the test has been made shall be reported. Table 1 Relative Density of water and conversion factor K for various temperatures Temperature, 0c Relative Density of Water Correction Factor K 18 0.9986244 1.0004 19 0.9984347 1.0002 20 0.9982343 1.0000 21 0.9980233 0.9998 22 0.9978019 0.9996 23 0.9975702 0.9993 24 0.9973286 0.9991 25 0.9970770 0.9989 26 0.9968156 0.9986 27 0.9965451 0.9983 28 0.9962652 0.9980 29 0.9956761 0.9977 30 0.9956780 0.9974
  • 92. 88 Specific Gravity - Calculation of Soil Bottle No. A B W1 - Weight of Bottle 16 18 W2 - Weight of Sample 10 10 W3 - Weight of bottle + sample + water 40.2 40.3 W4 - Weight of Bottle full of Water 34 34.1 V - Volume of bottle (W4 + W2) - W3 3.8 3.8 GS - Specific Gravity W2 V 2.632 2.632
  • 93. 89 SECTION II I. Moisture - Density Relationship Theory Compaction (degree of compaction) Soil is the process where by soil particles are constrained to pack more closely together through a reduction in air voids. The object in compacting soil is to improve its properties and in particular to increase its strength and bearing capacity reduce its compressibility and decrease its ability absorb water due to reduction in volume of voids. Development of test procedures by R.R. proctor in 1993 in the USA in order to determine a satisfactory state of compaction for soils being used in the construction of roads air ports and dams. The test made use of a hand rammer and a cylindrical mold with a volume of 1/30 cuff. At that time it was believed that the proctor test represented in the laboratory the state of compaction which could be reasonably achieved in the field. A laboratory test using increased energy of compaction was then necessary to reproduce these higher compacted densities, so a test was introduced which used a heavier rammer with the same mold. These procedures became known as the modified AASHTO T-180 test. 1. DEFINITIONS of the following a. Compaction:- The process of packing soil particles more closely together, usually by rolling, ramming or mechanical means, thus increasing the dry density of soil. b. Moisture - Dry density relationship:- The relationship between dry density and moisture content of a soil. c. Optimum Moisture Content (OMC):- The moisture content of a soil at which a specified amount of compaction will produce the max. dry density. d. Max. dry density:- the dry density optioned using a specified amount of compaction at eh Opt. M. C. e. Percentage air void ( va):- the volume of air voids in a soil expressed as a percentage. f. Saturation line (zero air voids line):- the line on a graph showing the dry density- moisture content relationship for a soil compacting no air voids. g. Relative compaction (% (compaction):- the percentage ratio of the dry density of the soils to its max compacted dry density determined by using a specified amount of compaction (Lab max dry density and field dry density.
  • 94. 90 h. Standard proctor:- light compaction, for light traffic road compaction by using 5.5 lb rammer and 3 layer compaction. i. Modified proctor:- heavy compaction for heavy Load construction (axle load) compaction by using 10 lb rammer and 5 layer compaction. 2. Compaction Process:- the solid soil particles are paced more closely together by mechanical means. This process must not be confused with consolidation, in which water is squeezed out under the action of a continuous static load. The air voids can not be eliminated altogether by compaction, but with proper control they can be reduced for a minimum. At low moisture content the soil grains are surrounded by a thin film of water, which tends to keep the grins a part even when compacted. The finer soil grains the more significant is this effect. If the moisture content is increased the additional water enables the grains to be more easily compacted together, some of the air is displaced and the dry density is increased. The addition of more water, up to a certain point, enables more air to be expelled during compaction. At that point the soil grains become as closely packed together as they can be (i.e. the dry density is at the maximum) under the application of this compactive effort when the amount of water exceeds that required to achieve this condition, the excess water begins to push the particle apart or water takes more spaces, so that the dry density is reduced. At higher moisture contents little or no more air is displaced by compaction, and the resulting dry density continues to decrease. 3. Sample preparation:- the method of preparation of test samples from the original (received from field) soil sample depends up on. 3.1 The largest size of stone (particles) present in the original sample. 3.2 Whether or not the soil particles are susceptible to crushing during compaction is assessed by inspection, or by passing the soil through sieves in the gravel-size range the amount of coarse materials determines the size of mold to be used i.e. whether 4" or 6" dia mold should be used. If breakdown of particles results in a change in the soil characteristics, and it a single batch of soil is compacted several times that change will be progressive during the test. A separate - batch of susceptible soil is needed for each determination of compacted dry density, consequently a much larger sample is required.
  • 95. 91 Cohesive soils should be broken down into small pieces before to be ready for compaction. 4. Mass of sample for test:- the mass of sample to be prepared for the tests. For each determination with 4"(102mm) diameter of mold about (2.5kg) for with 6"(152.4mm) diameter of mold about 6kg. The amount of sample before riffling. If gravel more than 75kg If clay about 30-50kg For subsequent determination, adjust the moisture condition of the samples as follows To obtain a lower m/c allow the soil sample to partially air/dry do not allow the soil to dry more than necessary. Place the soil in an air tight container if it is not to be used immediately. For a cohesive soil, leave it in the container for a maturing period of at least 24 hours to allow for a uniform distribution of water in the sample. 5. For multiple sample batches:- subdivide the prepared sample to give 5 or more representative specimens for test. Each specimen should be of about 2.5kg for 4" dia and 6kg for 6" diameter of mold. 6. Stone content sample:- particles larger than 19.5mm which are removed before test may consist of gravel, fragments of rock and other hard material, and are collectively referred to bellow as stone. The soil actually tested is called the matrix material (pass 19.5mm) four categories of soil are recognized, depending on the largest sizes of particles remaining after initial preparation. These categories relate to the following test methods. Method A and B material retained on 4.75mm sieve is removed and no correction is made, if the amount of retained material is 7% or more by mass. Method "c" is recommended instead. Method "C" coarse grained material passing on a 19mm sieve and removed retained material, and no correction is made. However if the amount of retained material is 10% or more, Method "D" is recommended instead.
  • 96. 92 Method "D" the amount of material retained on the 19.5mm sieve is from 10% to 30% the retained material on a 75mm sieve and discard the material retained on that 75mm sieve. Replace the material between 75mm sieve by an equal mass of similar material taken from an unused portion of the sample, passing 75mm sieve and retained on 4.75mm sieve mix in the replaced material thoroughly. Choice.2 If the % retained material on 19mm sieve is 10-30% Mass of sample for one batch = 6kg 6kg x 30% = 1. 8 of retained on 4.75mm sieve And passing material on 19.5mm sieve is = 6 - 1. 8 = 4.2kg. Mix the retained on 4.75mm sieve and passing on 19mm sieve (4.2+1. 8) = 6kg If the amount of material retained in the 19mm is more than 30% the rest methods for the determination of density or compaction is not applicable. Mold for Compaction:- Method "A" and "C" the 4"(102mm) diameter of mold compaction mold is used for method "D" the 6" (152.4mm) diameter compaction mold is used Summary Method "A" fine grained (102mm) diameter mold material passing 4.75mm sieve Method B-6" (152mm) diameter mold material passing 4.75mm sieve fine grained Method C-4" (102mm) diameter mold material passing 19mm sieve coarse grained Method D-6" (152mm) diameter mold material passing 19mm sieve coarse grained 7. Compaction Effort:- the procedure used for various types of compaction are summarized below. A. Standard Proctor - Method "A" or "C" Rammer weight 5.5lb (2.5kg) Height (lift) of rammer 12" (30.8cm) No. of blows 25 Layers 3 this test is knows as light compaction Method "B" or "D" Diameter of mold 6" (2.5) Rammer weight 5.5lb (2.5kg) Height (lift) of rammer 12" No. of blows 56
  • 97. 93 Layer 3 B. Modified Proctor Method "A" or "C" = Diameter of mould = 4" Weight of rammer = 10lb (4.5kg) Height (lift) of rammer = 18" No of blows = 25 Layer = 5 Method "B" or "D" = Diameter of mould = 4" Weight of rammer = 10lb (4.5kg) Height (lift) of rammer = 18" No of blows = 56 Layer = 5 this test is known as heavy compaction Summary Methods Layer No. of blows Wt of rammer lb/kg Height Volume of Mold cuft A - C 3 25 5.5/2.5 12 1/30 A - C 5 25 10.0/4.5 18 1/30 B - D 3 56 5.5/2.5 12 1/13.13 B - D 5 56 10/4.5 18 1/13.13 The mechanical energy applied in each type of test in terms of the work done in operating the rammer is derived and compared below. A. Light compaction = rammer wt x lift of rammer x No of blows x layer Volume of mold Eg. (5.5 lb x (12") x 25x3 = 1/30 ft3. Compared with:- 5.5 lb x (12") x 56x3 = 1/13.13 ft3.
  • 98. 94 B. Heavy compaction 10 lb x (18") x 25x5 = 1/30 ft3. 10 lb x (18") x 56x5 = 1/13.13 ft3. 8. Apparatus 1. Mold 2. Rammer 3. Measuring cylinder 4. 19 and 4.75mm sieves 5. Metal tray 6. Balance 7. Sample extruder (extracting) 8. Trimming knife (straightedge) 9. Drying oven 10.Moisture tine (can) 9. Test procedures 9.1 Check that mold, extension collar and base plate are clean and dry 9.2 Weigh the mold body to the nearest 1g sensitive balance
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  • 104. 100 9.3 Measure its internal diameter and height of the mold and calculate internal volume of the mold (v) V = IID2H 4 9.4 Check that the lugs or clamps hold the extension and base plate securely to the mold and assemble them together 9.5 Wipe with a slightly oily cloth on the internal surfaces 9.6 Check the rammer to ensure that it falls freely through the correct height of drop, and that the lifting knob is secure. 9.7 Place the assembled mold on a solid base (concrete floor) 9.8 Prepare the sample as described in section 3 and weigh to provide the single sample of about 2.5kg or 6kg and put in the mixing large tray and adjust the moisture content to desired starting value (add that calculated or estimated water) and mix thoroughly.
  • 105. 101 9.9 Add loose sample to the mold and compact the sample by applying 25 or 56 blows of the rammer dropping from the controlled height and weight of 5.5lb/12"H or 10lb/18"H. Make sure that the end of the tube is resting on the soil surface, and does not catch on the edge of the mold, before releasing the rammer. The guide tube must be held vertically. Place the tube gently on the sample surface, the rammer does the compaction not the tube. If the correct amount of sample has been used, the compacted surface should be at about one-third of the height of the mold body that is about 7.7cm for 4"(102mm) diameter and 9cm for 6" diameter mold below the top of the mold body, or 127mm for the 4" diameter. mold and for 6" mold 142mm diameter. Below the top of the mold extension collar. If the level differs significantly from this remove the sample, break it up, mix it with the remainder of the prepared material and start this stage again. After completed the 1st layer of compaction lightly scarify the surface of the compacted sample with the spatula or point of a knife. Place a second, equal layer of soil in the mold, and compact with 25 or 56 blows as before. Repeat with a third or up to 5th layer, which should then bring the compacted surface in the extension collar to not more than 6mm above the level of the mold body. If the soil level is higher than this, the result will be in accurate, so the sample should be removed, broken up and re-mixed, and the test repeated with slightly less soil in each layer. 9.10 Carefully remove the extension collar. Cut away the excess sample and level (trim off) to the top of the mold. Any sample cavity resulting from removal of small fragments at the surface should be filled with fine material, well pressed in and should be checked with the straight-edge. 9.11 Weigh sample and mold immediately 9.12 Remove the soil from mold by using sample extruder on jack. Break up the sample on the tray.
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  • 107. 103 9.13 Moisture Content Determination:- take representative sample in moisture tin or containers from the middle of the molded specimen, weigh immediately and put in the oven to dry. Note: Amount of sample for moisture content determination If it is clay or fine grained material not less than 100g and for coarse grained or gravel not less than 500g. 9.14 Thoroughly break up the remaining portion (material) of the molded specimen and the remainder of the prepared sample on the mixing tray, by rubbing until it will pass through 19.5mm for coarse grained or 4.75mm for fine grained material as judged by eye. Add an increment of sufficient water, to increase the moisture content of the soil by 1 to 2% of water to 2.5kg for 4" dia mold or 6kg for 6" dia mold of soil. Note: For sandy and coarse grained soil about 1-% For clay or silty clay 2-4% of water to 2.5kg or kg of soil. Mix in the water thoroughly. 9.15 Repeat the above procedure (stages 8 to 9) for each increment of water added, continue this series of determination until there is either a decrease or no change in the wet (bulk) unit weight or mass of sample and mold (after compaction). 9.16 Calculation 9.16.1 Bulk density (wet), p = M2 - M1, g/cc V Where: m1 = weight of mold m2 = weight of mold + sample 9.16.2 Moisture content a. wt of wet sample + container b. wet of dry sample + container c. wt of container moisture content, W0 = (a - b) * 100%, (W0,%) b - c 9.16.3 Bulk Density (Wet), p = M2 - M1, g/cc V Where: m1 = weight of mold m2 = weight of mold + sample
  • 108. 104 9.16.4 Dry Density, pd = p*100, g/cc W0 + 100 9.17 Plot of Dry Density, Pd, against the corresponding Moisture Content Draw a smooth curve through the points. The curves for "0" or some points air voids may be plotted as well as certain the point of max dry density (MDD) on this curve, and read off the maximum dry density value. The MDD value may lie between tow plotted points, but the peak should not be exaggerated when drawing the curve. Read off the corresponding moisture content, which is the optimum moisture content (OMC). Zero Air Void Line:- Va = wGs 1 + wGs
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  • 112. 108 SECTION III CALIFORNIA BEARING RATIO (CBR) 1. Definition:- CBR or bearing ration of the force required to penetrate a piston (plunger) of 3inch2 or 1936mm2 cross section in to soil in a mold at a rate of 1mm/min to that required for similar penetration into a standard sample of compacted crushed rock or lime. The ration is determined at penetrations of 2.5 (0.1") and 5mm (0.2") value is used. 2. Historical Development and Principle California Bearing Ration (CBR): The basic testing procedure employed in the determination of the California bearing ratio was developed by the California division of highways around 1930, and has since been adopted and modified by numerous states, the USA corps of engineers and many countries of the world in 1961 the American society for testing and materials adopted the modified as ASTM designation D 1883. Bearing ratio of laboratory competed soils. The CBR is a comparative measure of the shearing resistance of a soil. This test consists of measuring the load required the course a plunger of standard size to penetrate a soil specimen at a specified ratio. The CBR is the PSI or Mpa required to force a piston in to the soil, a certain depth expressed as percentage of the load, PSI, required to force the piston the same depth in to a standard sample of crushed rock, usually depths of 2.5mm or 5mm are used penetration loads for bearing value is known as the California bearing ratio which is generally abbreviated to CBR. This test method is intended to provide the relative bearing value or CBR, of sub-grade sub-base course materials procedures are gives for Laboratory compacted specimens of swelling, non swelling and granular materials. 3. Tests on Laboratory- compacted specimens are performed usually to obtain information, which will be used for design purposes.
  • 113. 109 The CBR value for a soil will depend upon its density, molding moisture content, and moisture content after soaking since the procedure of laboratory compaction should closely represent the results of field compaction. The first two of these variables must be carefully controlled during the preparation of laboratory samples for testing, unless it can be ascertained that the soil being tested be affected by it in the field after construction. The CBR tests should be performed on soaked samples. 4. Sample preparation for CBR test If the soils or material is damp (moist) when received from field, dry it until it becomes friable under a trowel, drying may be in air or by oven dry not exceeding 600c. Thoroughly break up aggregations, being carefully to avoid reducing the natural size of the individual particles and passing the 19mm or 4.75mm sieve will be required. 5. Replacement If the material is granular (method 'D'), and passing the 19.5mm sieve and retained on the 4.75mm sieve. If all material passes a 19mm sieve, the entire gradation shall be used for preparing specimens for compaction without replacement or modification. If its mass, does not exceed 25% of the mass of the original sample, no correction is necessary for its removal. If the mass retained is greater than 25%, it should be replaced by a similar mass if particles of between 4.75mm and 19mm sieve obtained from separate batch of similar sample. If there is material retained on the 19mm sieve the material retained on the 19mm sieve shall be removed replaced by an equal amount of sample passing 19mm sieve and retained on the 4.75mm sieve obtained by separation from portions of the sample not other wise used for testing. 6. Examples Amount of sample received from field 'M' sample Quarter the M' sample. If % Rt of the 19mm sieve is = 30% Mass of sample retained on the 19mm sieve m1 mass of sample passed on the 19mm sieve m2 mass of sample retained on the 4.75mm, equal amount of m1 sample = m3 amount of sample for one CBR mold. = m2 + m3 = m4
  • 114. 110 OR the assumed amount of sample for one CBR 7kg Amount of material Retained sieve 7 x 30% = 2.1kg Amount of material passed on the 19mm sieve 7 - 2.1 = 4.9kg. Total = 2.1 + 4.9 = 7.00kg Quarter the replaced or non replaced sample weigh and keep the representative sample at least 5.4kg 12lb for fine grained (silty clay) soil and 6.4 to 7.7kg (14 to 17lb) for granular sample. 7. Type of sample for test The sample may be compacted in to the mold under dynamically compacted in to it, at the required moisture content, either to achieve a specified density or by using a standard compactive effort. Undisturbed sample:- may be taken on site in a CBR mold, either from natural ground or from recompacted material, such as in an embankment or road sub-base specimens may be tested in the mold either as prepared or after soaking in water for required days. Penetration resistance:- force or pressure required to maintain a constant rate of penetration of CBR piston, in to the soil. Sub soil:- soil bellow the sub-grade or fill Subgrade:- Natural soil or embankment construction prepared and compacted to support a pavement. Sub-base:- layer of selected material of specified thickness in a pavement system between sub-grade and base course. Base course:- layer of high grade crushed gravel or rock material of specified thickness constructed on the sub-base to spread the load from the pavement and provide drainage.
  • 115. 111 8. Pavement:- constructed layer of material of specified thickness, usually of select, gravel, asphalt and concrete materials, designed to carry wheeled vehicles. This covers roads and airfield or airports. 9. Flexible pavement:- pavement constructed by using gravel, crushed gravel or rock and Asphalt materials. 10. Rigid pavement:- pavement constructed of concrete. 11. Surfacing:- top most layer of the pavement construction, providing a durable surface and smooth riding. 12. Basis of CBR test:- a constant rate of penetration shear test in which a standard plunger (Pistons) is pushed in to the soil at a constant rate and the force required to maintain that rate is measured at suitable intervals. The road penetration relationship is drown as a graph from which the loads corresponding to standard penetrations are read off and expressed as ratios of standard loads. The CBR value can be regarded as an indirect measure of the shear strength of the soil, but it can not be related directly to shear strength parameter. The only calculation necessary is to express the measured force for a certain penetration as a percentage of the standard force for the same penetration. CBR = Measured force x 100% Standard force The standard force corresponding to penetrations reading from 0.64 to 12.7mm The forces shown in corresponding to penetrations of 2.5mm (0.1") and 5mm (0.2) are those used in the standard calculations of CBR value. These are rounded equivalents to the original criteria for contact pressures under a piston (plunger) of 32inchcross-section of 1000 PSI at 2.5mm penetration and 1500 PSI at 5.00mm in penetration respectively. These standard forces where based on tests on samples of compacted crashed rock or lime and by definition relate to CBR of 100% standard force penetration. Relationship for CBR test Failure Soil Penetration inch/mm Force lbf/kgf Pressure PSI/kg/m2 0.1/2.5 3000/1361.2 1000/70.3 0.2/5 4500/041.74 1500/105.49 0.3/7.62 5700/2585.5 1900/133.6 0.4/10.16 6900/1769 2300/161.7 0.5/12.7 7800/3580.1 2600/182.8
  • 116. 112 The corresponding load-penetration relationship is shown bellow. Standard lad/penetration curve for CBR of 100% Load LPF 7000 6000 4500 4000 3000 2000 1000 0 2 2.5 4 5 6 8 10 12 14 Penetration (mm) 12.1 Limitations:- CBR test should not be used to estimate the bearing capacity of ground for foundations: the rest should be regarded as an index property. The application of which is restricted to pavement.
  • 117. 113 12.2 Construction:- Practical Aspects of the test (typical CBR value) AASHTO Unified CBR Value Condition Can be used as Clay A-5, A-6, A-7 OH, CH, MK, OL 0-3 V. poor Silty Clay A-4, A-5, A-6, A-7, OH, CH, MK, OL 3-7 Poor + fair A-2, A-4, A-6, A-7 OL CL, MC, S M, SL 7-20 Fair Borrow A-1-b, A-2-5, A-2-6 GM, GC, SW, SM, SP 20-50 Good Sub-base A-1-a, A-2-4, A-3, GW, GM, >50 V. good Base course 12.3 Surcharge weight:- the surcharge weights, simulates the effect of the thickness of road construction overlying the layer being tested. Each 5lb disc is equivalent to about 70mm thickness of superimposed construction. Surcharge weight should placed on the top of surface of the prepared specimen before testing. If the specimen is to be soaked before testing the surcharge rings should be placed on the sample immediately before immersion so that their presence can be control the amount of swelling. The effect of surcharge is greater for granular soils than for cohesive soils, but granular soils generally provide satisfactory sub-grades and pavement bases so this difference is not critical. 12.4 Effect of soaking:- the American practice as a precaution to allow for moisture content increase in the soil due to flooding or elevation of the water table, however, soaking has been shown to give rise to conditions which are too severe in many cases, resulting in unnecessarily conservative designs of pavement thickness. 13. TESTS Apparatus
  • 118. 114 Sample mixing tray Compacting mold with base plate, and extension collar Rammer
  • 119. 115 4.75 and 19mm sieves
  • 120. 116 Spacer disc Balance Dial gauge Oven Tripod Load frame (machine) Soaking tank Moisture (container) Filter paper Trimming knife Procedure Determine natural moisture content of the CBR test sample A. wt of sample (Air dry) + container B. wt of oven dry sample + container C. wt of container N.M.C = (A - B) x 100% (B - C) Calculate the amount of water to be added in order to increase the moisture in the amount of test sample. Let mass of air dry sample = m Optimum moisture content = Wo Natural moisture content = w1 Amount of water to be added M (Wo - W1) (100 + W1) Weigh the required amount of sample Place the weighed sample on the sample tray Measure the required measured (calculated) water Weigh the mold and record Add that calculated water and mix thoroughly Place the spacer disc on the bass plate. Place filter paper on the top of the spacer disc Place the 1st portion of sample in to the mold Compact it with the required method, rammer and blows. Repeat the process using the other required portions.
  • 121. 117 Remove the extension collar and carefully trim the compacted soil even with the top of the mold by means of a straight edge patch with smaller size material any holes and rough surface that may have developed in the surface by the removal of coarse material. Remove the perforated base plate and spacer disk. Weigh and record the mass of the mold plus compacted soil Place a disk of coarse filter paper on the perforated base plate. Invert the mold and compacted soil, and clamp the perforated base plate to the mold with compacted soil in contact with the filter paper. Place the surcharge weights on the perforated late and adjustable stem assembly and carefully lower on to the compacted soil specimen in the mold
  • 122. 118 Apply a surcharge equal to the weight of the base material and pavement with in 5 or 10lb. Mount the dial gauge support on top the extension caller, fit the dial gauge and adjust the level of the stem on the perforated plate so that the gauge reads zero or some convenient value. Swell Immerses the assembled mold in water allowing free access of water to the top and bottom of the specimen. Take initial measurements for swell immediately and allow the specimen to soak for 4 days (96 hours) maintain a constant water level during this period. If water does not appear at the top surface after 3 days immersion, pour water on to the top surface so that it remains covered and leave to soak. Usually soaking period is 4 days and 6 hours but a longer period may be necessary to allow swelling to reach completion. Take final swell measurements and calculate the swell as a percentage of the initial height of the specimen. Calculation of swell - Height of specimen = H - Division of the swelling dial gauge = 0.0254mm - Initial dial reading = H1 - Final dial reading = H2 % swell = (H2 - H1) x 0.0254 x 100% H
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  • 125. 121 Penetration Procedure Remove the sample and mould from the tank. Place the mold and sample on the rigid surface, to drain downward for 15min. Take care not to disturb the surface of the specimen during the removal of the water. After some water has drained away remove the surcharge disc, perforated plate and extension collar and weigh the sample with mould. Setting up loading frame:- Place a surcharge of weights on the specimen sufficient to produce an intensity of loading to the weight of the base material or over burden of material. Place the mold with base plate contains the sample centrally the platen of the testing machine. Contact the plunger with the top of the sample surface. Check that the connections between plunger load ring and cross- head are tight. Mount the penetration dial gauge on the bracket attached to the plunger. Seat the penetration piston with the smallest possible load. The value of which depends on the expected CBR values as follows. CBR Value PI Seat Load Silty clay about 5% 20 - 30 10N Silty 1 - 2% 0 10N Sandy clay 4 - 7% 20 - 30 25N Gravelly clay 5 - 30% 20 - 30 50N Sandy Gravel Above 30% NP 250N Winds up the machine platen slowly by hand until the load ring indicates this reading. Then reset the load dial gauge to zero, because the seating load is not taken into account in the test. Adjust the penetration dial gauge to read zero or same convenient datum reading.
  • 126. 122 Switch on the motor and record the load ring dial and penetration at 0.64mm (0.025") up to 12.7 (0.5") 0.64, 1.27, 1.95, 2.54, 3.18, 3.81, 4.45, 5.08, 10.16 and 12.7mm
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  • 131. 127 Calculation Penetration dial division = 0.0254 Load dial reading = C Ring factor = R lb Area of piston = A inch Stress CxR = PSI A Load - Penetration Curve:- readings of the load ring dial gauge are converted to force units by multiplying by the load ring factor (Rf) and plot the
  • 132. 128 stress-penetration curve. In some instances, the stress penetration curve may be concave up ward initially, because of surface irregularities or other courses, and in such cases the zero point shall be corrected or adjusted. Against penetration, and the force need be calculated only at penetration of 2.5 and 5mm. If the load PSI at 2.5mm = P CBR = Px100 = CBR% and at 5mm P2x100 = CBR% 1000 1500 Or using corrected stress values taken from the stress penetration curve for 0.1 inch and 0.2 inch penetrations. Calculate the bearing ratios for each be dividing the corrected stress by the standard stress of 1000 PSI = (6.9 MPa) and 1500 PSI (10.3 MPa) and multiplying by 100. The bearing ratio normally reported for the soil is the one (0.1 inch) when the ratio at 0.2 inch is greater rerun the test. If the check test gives a similar result use the bearing ratio at 0.2. Calculate the moisture content and unit weight or density, bulk and dry, before soak and after soaked. Three point CBR If CBR value for soil at 95% of max. dry density is desired, samples (specimen) should be compacted using 10, 30, and 65 blows per layer is satisfactory penetration shall be performed on each of these specimen load - penetration curve plot the CBR value versus dry density graph determine the design CBR at the percentage of the max dry density. This procedure is both for standard and modified compaction.
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  • 136. 132 SECTION IV IN-PLACE DENSITY (FIELD DENSITY) This method of test is intended to (cover) determine the density (compaction) of soil materials, in the natural state or after compaction in an embankment (fill) and road pavement construction, by finding the weight and moisture content of a disturbed and measuring the volume of density hole occupied by the sample prior to removal. Three test methods are provided as follows. I. Rubber Balloon Method II. Sand Cone (Replace) Method III. Nuclear Gauge Method I. Rubber Balloon Method 1. This test method covers the determination of the in-place density of compacted or firmly bonded soil using a rubber balloon apparatus. This test method is suitable for undisturbed or natural in organic soil, deposits soil or other similar firm materials and fill or embankments constructed of fine grained soils. This test method is not suitable for use in organic saturated, swampy or highly plastic soil sand crashed rock fragments or sharp edge material. Because that would deform under the pressure applied during this test. This test method may require special core for use on. 1. Fill materials containing particles with sharp edges. 2. Soils consisting of unbounded granular materials that will not maintain stable sides in a small hole. 3. Soils containing appreciable amount of coarse material in excess of specified sieve size in mm. 4. Granular soils having high void ratios. The volume of an excavated hole in a compacted soil is determined using a liquid filled vessel for filling to fill the hole. This test method may be used to determine the density of compacted soils used in construction; backfill, earth embankments, road fill and structural backfill.
  • 137. 133 Soft soils are not recommended for this method because may deform easily. Such soils may undergo a volume change during the application of pressure during testing. 2. Apparatus calibrated vessel balloon apparatus Calibrated vessel balloon apparatus Base plate (a rigid metal) Balance 1gm readable Oven or drying apparatus Sample container Miscellaneous, chisels, spoon buckets, and plastic bags shovel etc. 3. Procedure Verify procedure to be used and the accuracy of the volume indicator by using the apparatus to measure containers or molds of known valium that dimensionally simulate test trails that will be used in the field. The apparatus and procedures shall be such that these containers will be measured to with in 1% of the actual volumes. Determine the mass of water in cc or grams, required to fill the containers or hole, molds using a glass plate and or thin film of grease, if needed for sealing determine the mass of the container or mold and glass plate to the nearest gram. Fill the container or mold with water, carefully sliding the glass plate over the opening in such a manner as to ensure that no air bubbles are enter, that the mold is filled completely with water. Remove excess water and determine the mass of the glass plate, water and mold or container to the nearest the gram. Determine the temperature of the water calculate the volume of he mold or container. Repeat this procedure for each container or mold until three consecutive volumes having or maximum variation of 2.83 cm3 or 0.001 f3 is obtained. Record the average of the three trials. Checking calibration:- place the rubber balloon apparatus and base plate on a smooth horizontal surface. Applying on operating pressure take an initial reading on the volume indicator. Before any measurements are taken it may be necessary to distend the rubber balloon and by kneading remove the air bubbles adhering to the inside of the membrane. If the calibration molds re air tight, it may be necessary to provide an air escape to prevent erroneous results
  • 138. 134 caused by the trapping of air by the membrane. One means of providing air escape is to place small diameter strings over the edge of and down the inside, slightly beyond bottom enter of the mold. This will allow trapped air to scope during the measurement of the calibrated mold or container. Transfer the apparatus to one of the previously calibrated molds with a horizontally leveled bearing surface. Apply the operating pressure as necessary until there is no change indicated on the volume indicator. Depending on the type of apparatus, the operating pressure maybe as high as 34.5kpa and may be necessary to apply a downward load to the apparatus to keep it from rising. It is recommended that the operating pressure of the apparatus be kept as low as possible while maintaining the 1% volume accuracy. The use of higher pressures than necessary may require the use of an additional load weight to prevent up lift of the apparatus. The combined pressure and surcharge loads may result in stressing the unsupported soil surrounding the test hole causing it to deform. Record the reading pressures, and surcharge roads used. The difference between the initial and final readings is the indicated volumes determine the volume of he other molds or containers. A satisfactory calibration check of an apparatus has been achieved when the difference between the indicated calibrated volume of the container or molds is 1% or less, for all volumes measured. Select the optimum operating pressure and record it for use with the apparatus during field testing operations. Make this smooth surface at the test location so that it is plane and level. The test area is not deformed compressed torn, or other wise disturbed. Assemble the rubber balloons and bass plate apparatus on the smooth test location Take an initial reading on the volume indicator and record. The base plate shall remain in-place through compilation of the test. Dig a hole within the base plate. Care in digging the test hole so that soil around the top edge of the hole is not disturbed. When material being tested contains a small amount of over size and isolated large particles are encountered, the test
  • 139. 135 can be removed to a new location. If particles larger than 20 or 37.5mm are prevalent, larger test apparatus and test volumes are required larger test-hole volumes will provide improved accuracy and shall be used where particle. Maximum Particle size Maximum Test hole 37.5mm 2840 20mm 1700 4.75mm 1130 The test hole shall be kept as free of pockets and sharp obtrusions as possible, since they may affect accuracy or may puncture the rubber membrane Place all soil removed from the test hole in an airtight container for later mass and water content determination. Place the apparatus after the test hole has been dug over the base plate in the same position as used for the initial, reading. Applying the same pressure and surcharge load as used in the calibration check, take and record the reading on the volume indicator. The difference between the initial and final readings is the volume of the test hole. Determine the mass of all the wet soil removed from the test hole to the nearest 5gm max all the soil thoroughly and select a representative water content sample and determine the moisture content Calculation Volume of mold V = (W1-W2) x Vw Where V = volume of mold W1 = weight of mold and glass and water W2 = weight of mold and glass Vw = volume of water In-place wet (bulk)t density, Pwet = Ay Vh Where Pwet = weight density wA = weight of moist soil removed from the test hole Vh = volume of the test hole In-place dry density, d = Pwet . 1 + Wo 100
  • 140. 136 d = pwet x 100 100 + Wo Where d = In place dry density Wo = In place moisture content % Compaction = d x 100 MDD Where MDD standard testing lab Report Test location Project Test holes volume In-place wet, dry density and moisture content % compaction Visual description of the soil 1. In-Place density by Nuclear methods: This method of test covers a procedure for determining the density and moisture content of soils, either in the natural state or after compaction by means of a nuclear moisture density gauge. The nuclear gauge can be used to make relative or percent compaction determination. The density in mass per unit volume of the material under test is determined by comparing the detected rate of gamma radiation with previously established calibration data. The test method described is useful as a rapid nondestructive technique for the in- place determination of density of soil. The test method is suitable for quality control and acceptance testing for construction and for research and development applications. The nondestructive nature of he test allows repetitive measurements to be made at a single test location.
  • 141. 137 Over size material (Rock) poor or gap graded material (voids) in eth source detector path may cause higher or lower density determination. Where lack of uniformity in the soil due to layering rock or voids is suspected, the test volume site should be dug up and visually examined to determine if he test material is representative of the full material in general and if rock correction is required. 2. Apparatus 2.1 Nuclear gauges:- which contain a radio active source. 2.2 Reference standard 2.3 Site preparation device 2.4 Drive pine 2.5 Drive pin extractor 2.6 Slide hammer 3. Danger (Hazards) this equipment utilizes radioactive materials that may be hazardous to the health of the users unless proper precautions are taken. Users of this equipment must become familiar with applicable safety procedures and government regulations. 3.1 Effective user instructions together with leak tests, recording and evaluation of film badge data, etc, are a recommended part of the operation and storage of this instrument. 4. Procedure for field use 4.1 Standardize the gauge 4.2 Select a test location 4.3 Remove all disturbed and loose material 4.4 Remove additional material as necessary to reach the material. 4.5 That represents a valid sample of the zone or stratum to be tested. Surface drying and spatial bias should be considered in determining the depth of material to be removed. 4.6 Plane smooth horizontal surfaces so as to obtain maximum contact between the gauge and the material being tested. To correct for surface irregularities, use of fines or fine sand as filler may be necessary. The depth of the filler should not exceed 3mm and the total area filled should not exceed 10% of the bottom area of instrument several trial seating may be required to achieve these conditions. 4.7 Seat the gauge firmly on the prepared test site.
  • 142. 138 4.8 Keep all other radio active sources away from the gauge to avoid affecting the measurement so as not to affect the readings. 4.9 Secure and record one or more readings for the normal measurement period in the back scatter position. 4.10 Determine the ratio of the reading to the standard count or to the air gap count. From this count ratio and the appropriate calibration and adjustment data, determine the in-place bulk (wet) density. 4.11 Make a hole perpendicular to the prepared surface using the guide and the hole- forming device or by drilling if necessary. The depth of the hole must be deeper than the depth to which the probe will be placed. The guide shall be the same sizes the base of the gauge with the hole in the same location on the guide as the probe on the gauge. The corners of the guide are marked by scoring the surface of the soil. The guide plate is than removed and any necessary repairs are made to the prepared surface. 4.12 Set the gauge on the soil surface, carefully beginning it with the marks on the soil so that the probe will be directly over the pre-formed hole. 4.13 Insert the probe in the hole 4.14 Seat the gauge firmly by rotating it about the probe with a back and forth motion. 4.15 Pull gently on the gauge in the direction that will bring the side of the probe against the side of the hole that is closest to the detector (source) location in the gauge housing. 4.16 Keep all other radioactive sources away from the gauge to avoid affecting the measurement. 4.17 Record one or more readings for the normal measurement period. 4.18 Comparison need to be made to evaluate whether the presence of a single large rock or void in the soil is producing unrepresentative values of density whenever valves obtained are questionable, the test volume sit should be dug up and visually examined. 4.19 If the material (sample) is containing oversize particles (rock) the test should be corrected. 4.20 Calculation 4.20.1 The in-place wet density, moisture content and dry density are determined as outlined in 4.6 - 4.18 4.20.2 Determine the max. dry density and OMC in Laboratory 4.20.3 Determine the % compaction c = Fdd x 100 MDD
  • 143. 139 Where C = % compaction Fdd = field dry density MDD = Max.dry density in Laboratory 5. In-Place density by the sand replacement method 5.1 This test method covers a procedure to determine of the In-place density of soils, either in after compaction or in the natural state, using a pouring device and calibrated sand material to determine. The weight and moisture content of a disturbed sample and measuring the volume occupied by the sample prior to removal. 5.2 The soil or material being tested should have sufficient cohesion or particle attraction or particle interlocking to maintain stable sides during excavation of the test pit on a small hole in excavation, and be firm enough to withstand the minor pressure exerted in digging the hole and placing the apparatus over it or pouring without deforming or sloughing. 5.3 This test method is not suitable for saturated condition highly plastic soils or organic and are not recommended for materials that is soft or crumble easily or compress (deform) during the excavation of the test hole. This test method may not be suitable also for soils consisting of unbound gravel (coarse) materials that will not maintain stable sides in eth test hole. The accuracy of the test methods may be affected for materials that deform easily or that may undergo volume change in the excavated hole during the test. 5.4 When materials to be tested contain appreciable amounts of particles larger than 50-37.5mm or where test hole volumes larger than 2830cm3 are required. 5.5 The construction subgrade, subbase, base course and surfacing after enoughly compacted, at the test location is prepared and a metal frame is placed and fixed into position. The volume of the space between the top of the metal frame and the ground surface is determined by filling the space with calibrated sand using a pouring device. The hole is filled with free flowing sand of a known unit weight and the volume is determined. The wet density of the in-place material is calculated from the mass of material removed and the measured volume of the test pit. The water content of the material from the hole is determined and the dry mass of the materials and the in-place dry density are calculated using the wet mass of the soil, the water content, and the volume of the hole.
  • 144. 140 5.6 These test methods are used to determine placed during the construction of earth embankments, structure backfill road backfill sub-base, base course and surfacing. For construction control, these test methods are often used as the
  • 145. 141 bases for acceptance of material compacted to a specified density or to a percentage of a maximum density determined by a standard laboratory test method (by standard or modified proctor, max dry density) 5.7 Two In-place density test methods are provided 5.7.1 In-place density of total material is to be determined the maximum particle size present in the in-place material bring tested does not exceed the max particle size allowed in the lab. compaction test. 5.7.2 The In-place material contains particles larger than the max. particles size allowed in the laboratory compaction test. 6. Apparatus 6.1 Sand cone density jar (apparatus) an attachable funnel or sand cone 6.2 Clean, dry and Calibrated sand 6.3 Balance 6.4 Drying equipment (oven) 6.5 Sieves 0.850, 0.60, 0.30 and 0.075mm 6.6 Metal plate with center hole 6.7 Straightedge 6.8 Miscellaneous equipment shovels chisel, brush etc. 7. Calibration and standardization of density sand 7.1 Wash the sand and shall be cleaned from dust and any fine particles 7.2 Dry and sieve the washed sand 7.3 Sieving 7.3.1 The dried sand is placed in the 0.850mm sieve shaken for long enough for all fine particles smaller than 0.85mm sieve size to pass through. This can be achieved most conveniently by using a mechanical sieve shaker. If a shaker is not available, sieving can be done by hand. 7.3.2 Mechanical shaker:- the selected sieve with receiving pan is placed in the shaker. The sand is placed in the top sieve, which is then fitted with the lid, and the two or more sieves are securely fastened down in the machine agitation in the shaker should be for a minimum period of 10 min. 7.3.3 Hand sieving:- place the dried sand sample on the largest sieve. The sieve must be agitated by shaking so that the particles roll in an irregular motion, and until no more particles pass through the openings.
  • 146. 142 Sieve Size Pass Retire No. 20 (0.850)mm x No. 30 (0.60)mm x Or No. 30 (0.6)mm x No. 50 (0.30)mm x Summary:- Choice 1: Pass No 20(0.850mm) Retained No 30 (0.60mm) Choice 2: Pass No 30(0.60mm) Retained No 50 (0.30mm) 7.4 Determination of the weight (mass) of the calibrated sand required to fill the funnel (cone) a. mass of Jar + Sand before pouring b. mass of Far + Sand after filling (pouring) Mass (weight) of sand in cone = a-b = c 7.5 Determination of Bulk unit weight of the clean and calibrated sand V = volume of apparatus S1 = mass of clean sand + container S2 = mass of clean sand + container S3 = mass of container sand + container S4 = Average mass of clean sand = S1 + S2 + S3 3 S5 = mass of container S6 = The Average mass of sand = S4 - S5 Bulk unit weight of sand = S6 g/cc V 8. Determination of the density of the soil In-place (sand cone method) 8.1 Inspect all density apparatus 8.2 Assemble and Inspect the density jar apparatus cone for damage, free rotate of the value, and properly matched base plate. 8.3 Inspect the compacted site visually compacted enough or not 8.4 Select a location that is representative of area to be tested the In-placed density 8.5 In-place density should be taken after compaction, about 24-78 hours. 8.6 Prepared the surface of the location to be tested
  • 147. 143 8.7 Remove all loose material from the surface of an area larger enough to receive the metal plate make smooth surface in the soil to properly and firmly seat the plate 8.8 In soils where leveling is not successful or voids, remain, volume horizontally bounded by test funnel, plate and ground surface must be determined by preliminary test fill the space with sand from the apparatus determine the mass of sand used to fill the space, refill apparatus, and determine a new initial mass of apparatus and sand before proceeding with the test. After this measurement is completed, carefully brush the sand from prepared surface. 8.9 Place the Metal plate centrally hole plate on the smooth (leveled) test size. 8.10 Nail on four position 8.11 Excavate the hole through the center hole in the plate, using chisel or knife, being careful to avoid disturbing or deforming that will bound the hole, Do not permit any movement of heavy equipment in the Area of the test pit PIS deformation of the soil with in the test pit may occur. 8.12 Place all material removed from the test hole in a suitable container being carefully to avoid losing any particle. Avoid moisture loss by keeping the container covered while material is not being placed in it. Use sealable plastic bag, avoid any heat before being weighed 8.13 Carefully trim the sides of the excavation 8.14 Continue the excavation to the required depth 8.15 The sides of the hole should slope in ward slightly. The sides of the test pit should be smooth as possible and free of pockets to over hangs or anything that might interfere with the free flow of the sand. 8.16 Clean the sides and bottom of the test pit of all loosened material. 8.17 If during excavation of material from with in the test pit, a particle larger than the laboratory compaction material, go to method 2. 8.18 Carefully weigh the removed sample from hole and record 8.19 Put the weighed material in oven or drying apparatus to dry and determine the in- place moisture content. 8.20 Fill or pour the calibrated sand in the density jar and weight initially. 8.21 Carefully put at the center of the test hole attached with metal plate. 8.22 Open carefully the density valve at the center of the test hole attached with metal plate 8.23 While the sand is being poured, avoid any vibrations in the test area. 8.24 When it is being stop pouring in the test hole close the density valve. 8.25 Remove the remaining sand and jar.
  • 148. 144 8.26 Weigh the remaining sand and jar and record. 8.27 Removed the clean used sand was being in hole and place it n to container. 8.28 Remove the metal plate from test hole and calibrate 8.29 Reclean and calibrate the used sand, sieve by 0.850 and 0.600mm or 0.600 and 0.300mm sieve. 9. Calculation 9.1 Determine the volume of test hole. P = W V = W V  Where V = Volume of density hole W = Weight of sand in hole  = Unit weigh of clean sand 9.2 Determine the in-place Bulk density Bd = m1 - m2 V Where m1 = mass of sample in hole + container m2 = mass of container V = Volume of test hole or 9.3 Bulk density, Bd m1 - m2 msh Where msh = mass of sand in hole 9.4 Determine the in-place moisture content Wo = A - B x 100 B - C Where Wo = moisture content A = wt of wet sample + container in hole B = wt of dry sample + container
  • 149. 145 9.5 Determine the in-place dry density fdd = Bd . 1 + Wo 100 9.6 Determine the % compaction C = Fdd x 100 Mdd Where C = % compaction Mdd = max. dry density in laboratory Fdd = Field Dry Density CLIENT : PROJECT : TEST ON : TEST SPECIFIED BY : SAMPLED BY : KINDS OF TEST : LAB. NO. : DATE ISSUED : IN-PLACE DENSITY DETERMINATION SAMPLE NUMBER OR STATIONS 1 2 3 4 Weight of wet soil from hole, W(gm) 2348 2362 2344 2353 Weight of sand + jar before pouring, W1(gm) 6000 6000 6000 6000 Weight of sand + jar after pouring, W2(gm) 4400 4480 4510 4490 Weight of sand in cone, W3(gm) 480 480 480 480 Weight of sand in hole, W4=(W1-W2-W3) 1120 1040 1010 1030 Bulk Density Ww x Ps (g/cc) Wsh 2.10 2.27 2.32 2.28 Wt. of Wet soil 2348 2362 2344 2352 Wt. of Dry soil 2150 2165 2138 2143 Wt. of Moisture, g 198 197 206 209 Moisture Content (m), % 9.2 9.1 9.6 9.8
  • 150. 146 Dry Density D = 100 x Wet Density, g/cc 100+m 1.92 2.1 2.12 2.08 M.D.D (g/cc) 2.21 2.21 2.21 2.21 Optimum Moisture Content (%) 2 12 12 12 % Compaction 87 95 96 94 % Moisture 77 76 80 82 Remark:
  • 151. 147 Summary Bd = M1 x s (m2 - m3 - m4) Where Bd = bulk density m1 = mass of sample in test ole m2 = mass of sand + jar before pouring m3 = mass of sand + jar after pouring m4 = mass of sand in cone s = density of sand
  • 152. 148 References The American Association of State Highway and Transportation Officials (AASHTO) part 2, 1986 T87-T274 ASTM Volume 04, 08 Rock and Soil (1) D420 - D4914 British Standard 1377 part 1 - 9 K H Head Part 1 and 2 Lambe Soil Mech – M DAS
  • 153. 149 IN-PLACE DENSITY DETERMINATION-Form AASHTO 191 ASTM D 1556 PROJECT: OPERATOR DATE TEST TAKEN ON (A) ------------------------ (B) SUBBASE ---------------------------- STATION REP. FROM KM UNIT WEIGHT OF SAND (AS DETERMINED IN HE LAB.) REPORTED TO: Lab. No SAMPLE NUMBER OR STATIONS Weight of wet soil from hole, W(gm) Weight of sand + jar before pouring, W1(gm) Weight of sand + jar after pouring, W2(gm) Weight of sand in cone, W3(gm) Weight of sand in hole, =(W1-W2-W3)(gm) Bulk Density Ww x Ps (g/cc) Wsh Wt. of Wet soil Wt. of Dry soil Wt. of Moisture, g Moisture Content (m), % Dry Density D = 100 x Wet Density, g/cc 100+m M.D.D (g/cc) Optimum Moisture Content (%) % Compaction % Moisture
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