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CRYSTALLIZATION
INDUSTRIAL CHEMICAL PROCESS
1
CRYSTALLIZATION
 Crystallization is the (natural or artificial)
process by which a solid forms, where the
atoms or molecules are highly organized into
a structure known as a crystal.
 Some of the ways by which crystals form
are precipitating from a solution, freezing, or
more rarely deposition directly from a gas.
 Attributes of the resulting crystal depend
largely on factors such as temperature, air
pressure, and in the case of liquid crystals,
time of fluid evaporation.
2
Contd,..
 Crystallization is an operation in which solid
particles are formed from a liquid solution.
 It is a solid liquid operation used to seperates
solutes from solution in the form of crystals.
 In this operation mass tranferred from the
liquid phase to the solid phase/the crystal
surface
3
CLASSIFICATION OF
CRYSTALLIZER
It is based on the mode of operation
 Batch crystallizer: stir tank crystallizer
 Continuous crystallizer :swenson walker
crystallizer
4
Swenson-walker crystallizer
5
INTRODUCTION
 Swenson-walker crystallizer is a continuous
type crystallizer.
 This operation involves both heat and mass
transfer.
 Crystallization is the formation of solid
particles with in homogeneous phase.
 In the formation of crystals two steps are
required.
Nucleation(birth of new solute particle)
crystal growth(growth of the nucleus to
microscopic size )6
PRINCIPLE
 It works on the principle based on super
saturation by cooling.
7
CONSTRUCTION
8
OPERATION
9
ADVANTAGES AND
DISADVANTAGES
 Less floor space is required
 Saving labor cost
 Continuous process
 Crystal of uniform size, free from inclusions
 Scrapper may break crystal to the little extent
due to the agitation
10
Thank
you!!11

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Crstallization

  • 2. CRYSTALLIZATION  Crystallization is the (natural or artificial) process by which a solid forms, where the atoms or molecules are highly organized into a structure known as a crystal.  Some of the ways by which crystals form are precipitating from a solution, freezing, or more rarely deposition directly from a gas.  Attributes of the resulting crystal depend largely on factors such as temperature, air pressure, and in the case of liquid crystals, time of fluid evaporation. 2
  • 3. Contd,..  Crystallization is an operation in which solid particles are formed from a liquid solution.  It is a solid liquid operation used to seperates solutes from solution in the form of crystals.  In this operation mass tranferred from the liquid phase to the solid phase/the crystal surface 3
  • 4. CLASSIFICATION OF CRYSTALLIZER It is based on the mode of operation  Batch crystallizer: stir tank crystallizer  Continuous crystallizer :swenson walker crystallizer 4
  • 6. INTRODUCTION  Swenson-walker crystallizer is a continuous type crystallizer.  This operation involves both heat and mass transfer.  Crystallization is the formation of solid particles with in homogeneous phase.  In the formation of crystals two steps are required. Nucleation(birth of new solute particle) crystal growth(growth of the nucleus to microscopic size )6
  • 7. PRINCIPLE  It works on the principle based on super saturation by cooling. 7
  • 10. ADVANTAGES AND DISADVANTAGES  Less floor space is required  Saving labor cost  Continuous process  Crystal of uniform size, free from inclusions  Scrapper may break crystal to the little extent due to the agitation 10