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1




An Experimental Study of
Small-Sized Conical Spouted
Beds (CSBs)
11th ASME Early Career Technical Conference
Georgia Institute of Technology, November 4-5, 2011



Mandeep Sharma, Matthew Lousteau, Dr. Ingmar Schoegl
Department of Mechanical Engineering
Louisiana State University
2




Background

Mathur and Gishler introduced Spouted Bed
Reactors at NRC Canada in 1954
• Alternative for drying moist wheat grains (peas,
  lentils and flax)
• Combustion of solid and heavy liquid fuels

• Potential for gasification and pyrolysis of wastes:

   Biomass (rice husk, pine or hard wood saw dust
    etc.)
   Plastics

   Tires
3




Objective

  Major goal: develop a laboratory scale CSB
   gasifier facility for generating H2 from biomass

  Reactor design depends on hydrodynamic
   parameters

    Minimum Spouting Velocity
    Pressure drop across the bed
  Results from the Cold Flow CSB reactor model
   provides foundation for hot flow CSB reactor
4




Conical Spouting Bed

Contacting of solids with fluid by injecting a steady
axial jet of fluid
                                    Spouting behavior
Schematic of CSB reactor model
5




Unique Characteristics of CSBs

• Suitable for treatment of coarse, sticky, moist
  and irregular shaped material

• Short residence time

• Better heat and mass transfer inside the reactor

• Economical
6




Minimum Spouting Velocity (ums)o
 - minimum superficial fluid velocity at which inert
   particles bed remains in the spouted state
             Two ways to find it




      Experimental

                        Theoretical
7




Experiment
8




Cold Flow CSB model

• Fluidizing medium: Air

• Bed material: Aluminum oxide particles (dp = 483

  µm and 1092 µm, ρ = 3960 Kg/m3)

• Column: ID of 63.5 mm

• Fluid inlet diameters: 6.35 mm, 4.572 mm and
  3.302 mm

• The stagnated bed height: 10 mm to 50 mm- 60°

  conical contactor
9




CSB Cold Flow Setup




                                                                                  Air
Schematic of experimental set-up: (1) air manifold, (2) air filter (3), control valve, (4/5)
rotameters, (6) air inlet pipe, (7/8) pressure taps at bed inlet and outlet, (9) U-tube
manometer, (10) conical contactor, (11) bed material, and (12) cylindrical column.
10




Different Spouting Regimes
11




Effect of system parameters on (ums)o

       Effect of different Ho, Do and dp on (ums)o
12




Theoretical way
13




Existing Correlations for (ums)o
   Source               Correlation             Eqn.

Markowski
                                                (1)
(1983)

Choi (1992)                                     (2)

Gorshtein
                                                (3)
(1964)
Mukhlenov
                                                (4)
(1965)
Tsvik (1967)                                    (5)

Olazar (1992)                                   (6)

Olazar (1996)                                   (7)
Bi (1997) (for
                                                (8)
Db/Do ≥1.66)

 They used significantly larger CSBs than the model
 investigated in present study
14




 Summary of operating parameters used previously
            and in the present study
    Source         Particle     D0         Dc        Di      ϒ      Ho (mm)
                  size (mm)    (mm)       (mm)     (mm)    (deg)
Markowski et       3.41 ~                 300 ~    5.6 ~            3.36 ~
                              5.6 ~ 300                     37
al. (1983)         10.35                  1100      300              690
Choi et al.       2.1 ~ 2.8               240 ~                     240 ~
                              21 ~ 35               38      60
(1992)                                     450                       400
Olazar et al.     0.95 ~ 25                                28 ~      70 ~
                              30 ~ 60      360      60
(1992)                                                      45       300
Bi H. T. et al.     1.16       12.7 ~     65 ~             30 ~      80 ~
                                                   38.1
(1997)                          25.4      95.8              60       335
Present Study      0.483,      3.3 ~      63.5 ~   3.3~
                                                           30, 60   10 ~ 65
(2011)             1.092       9.525        70     9.52

      Evaluation of accuracy and applicability of
existing correlations for ums required small sized
CSBs
15




Evaluation of Correlations                 …cont’d

Correlations’ predictions comparison with
experimental results for a particular set of operating
parameters
16




Evaluation of Correlations                             …cont’d
For one particular data set      - e.g. 60°, 483 µm, 6.35 mm Do
         best performing correlations align with the
                       diagonal line
17




Evaluation of Correlations                      …cont’d
   Comparison of Gorshtein correlation for all data sets
18




Evaluation of Correlations                      …cont’d
  Comparison of Mukhlenov correlation for all data sets
19




Evaluation of Correlations                     …cont’d

     Comparison of Tsvik correlation for all data sets
20




Evaluation of Correlations                    …cont’d

      Comparison of Choi correlation for all data sets
21




Poor performance of correlations:
22




Proposed Correlation
23




Proposed correlation shows excellent agreement with experiments
                               75                       o
                                        Present Study, 60 cone angle
                               70                                      + 16.3 %
                                          0.483 mm dp, 6.350 mm Do
                               65         0.483 mm dp, 4.572 mm Do
                               60         0.483 mm dp, 3.302 mm Do
                               55         1.092 mm dp, 6.350 mm Do
       Predicted (ums)o, m/s




                               50         1.092 mm dp, 4.572 mm Do                - 17.15 %
                               45         1.092 mm dp, 3.302 mm Do
                               40
                               35
                               30
                               25
                               20
                               15
                               10
                                5
                                0
                                    0   5 10 15 20 25 30 35 40 45 50 55 60 65 70 75
                                                   Experimental (ums)o, m/s
24




Conclusions
• Available Correlations have shortcomings for
  small-sized laboratory scale CSB studies


• Developed Simple empirical correlation for (ums)o

  Showed excellent agreement with experimental
  findings


• Results provide platform for design and fabrication

  of hot flow facility
25




Work in Progress…

• Additional tests required for the development of a
  universally applicable correlation for ums
  predictions for small-sized laboratory scale CSBs.

• Data acquisition system installation

• design and development of a laboratory scale
  CSB biomass gasifier for H2 generation
26




Questions?
27




Thank You!




Acknowledgement: Louisiana State University Council on
Research Faculty Research Grant Program
28




Backup Slides
29




Pressure Drop Measurements

    Effects of Ho and Do on stable pressure drops and
                 maximum pressure drops

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Mandeep asme ectc_2011

  • 1. 1 An Experimental Study of Small-Sized Conical Spouted Beds (CSBs) 11th ASME Early Career Technical Conference Georgia Institute of Technology, November 4-5, 2011 Mandeep Sharma, Matthew Lousteau, Dr. Ingmar Schoegl Department of Mechanical Engineering Louisiana State University
  • 2. 2 Background Mathur and Gishler introduced Spouted Bed Reactors at NRC Canada in 1954 • Alternative for drying moist wheat grains (peas, lentils and flax) • Combustion of solid and heavy liquid fuels • Potential for gasification and pyrolysis of wastes:  Biomass (rice husk, pine or hard wood saw dust etc.)  Plastics  Tires
  • 3. 3 Objective  Major goal: develop a laboratory scale CSB gasifier facility for generating H2 from biomass  Reactor design depends on hydrodynamic parameters  Minimum Spouting Velocity  Pressure drop across the bed  Results from the Cold Flow CSB reactor model provides foundation for hot flow CSB reactor
  • 4. 4 Conical Spouting Bed Contacting of solids with fluid by injecting a steady axial jet of fluid Spouting behavior Schematic of CSB reactor model
  • 5. 5 Unique Characteristics of CSBs • Suitable for treatment of coarse, sticky, moist and irregular shaped material • Short residence time • Better heat and mass transfer inside the reactor • Economical
  • 6. 6 Minimum Spouting Velocity (ums)o - minimum superficial fluid velocity at which inert particles bed remains in the spouted state Two ways to find it Experimental Theoretical
  • 8. 8 Cold Flow CSB model • Fluidizing medium: Air • Bed material: Aluminum oxide particles (dp = 483 µm and 1092 µm, ρ = 3960 Kg/m3) • Column: ID of 63.5 mm • Fluid inlet diameters: 6.35 mm, 4.572 mm and 3.302 mm • The stagnated bed height: 10 mm to 50 mm- 60° conical contactor
  • 9. 9 CSB Cold Flow Setup Air Schematic of experimental set-up: (1) air manifold, (2) air filter (3), control valve, (4/5) rotameters, (6) air inlet pipe, (7/8) pressure taps at bed inlet and outlet, (9) U-tube manometer, (10) conical contactor, (11) bed material, and (12) cylindrical column.
  • 11. 11 Effect of system parameters on (ums)o Effect of different Ho, Do and dp on (ums)o
  • 13. 13 Existing Correlations for (ums)o Source Correlation Eqn. Markowski (1) (1983) Choi (1992) (2) Gorshtein (3) (1964) Mukhlenov (4) (1965) Tsvik (1967) (5) Olazar (1992) (6) Olazar (1996) (7) Bi (1997) (for (8) Db/Do ≥1.66) They used significantly larger CSBs than the model investigated in present study
  • 14. 14 Summary of operating parameters used previously and in the present study Source Particle D0 Dc Di ϒ Ho (mm) size (mm) (mm) (mm) (mm) (deg) Markowski et 3.41 ~ 300 ~ 5.6 ~ 3.36 ~ 5.6 ~ 300 37 al. (1983) 10.35 1100 300 690 Choi et al. 2.1 ~ 2.8 240 ~ 240 ~ 21 ~ 35 38 60 (1992) 450 400 Olazar et al. 0.95 ~ 25 28 ~ 70 ~ 30 ~ 60 360 60 (1992) 45 300 Bi H. T. et al. 1.16 12.7 ~ 65 ~ 30 ~ 80 ~ 38.1 (1997) 25.4 95.8 60 335 Present Study 0.483, 3.3 ~ 63.5 ~ 3.3~ 30, 60 10 ~ 65 (2011) 1.092 9.525 70 9.52 Evaluation of accuracy and applicability of existing correlations for ums required small sized CSBs
  • 15. 15 Evaluation of Correlations …cont’d Correlations’ predictions comparison with experimental results for a particular set of operating parameters
  • 16. 16 Evaluation of Correlations …cont’d For one particular data set - e.g. 60°, 483 µm, 6.35 mm Do best performing correlations align with the diagonal line
  • 17. 17 Evaluation of Correlations …cont’d Comparison of Gorshtein correlation for all data sets
  • 18. 18 Evaluation of Correlations …cont’d Comparison of Mukhlenov correlation for all data sets
  • 19. 19 Evaluation of Correlations …cont’d Comparison of Tsvik correlation for all data sets
  • 20. 20 Evaluation of Correlations …cont’d Comparison of Choi correlation for all data sets
  • 21. 21 Poor performance of correlations:
  • 23. 23 Proposed correlation shows excellent agreement with experiments 75 o Present Study, 60 cone angle 70 + 16.3 % 0.483 mm dp, 6.350 mm Do 65 0.483 mm dp, 4.572 mm Do 60 0.483 mm dp, 3.302 mm Do 55 1.092 mm dp, 6.350 mm Do Predicted (ums)o, m/s 50 1.092 mm dp, 4.572 mm Do - 17.15 % 45 1.092 mm dp, 3.302 mm Do 40 35 30 25 20 15 10 5 0 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 Experimental (ums)o, m/s
  • 24. 24 Conclusions • Available Correlations have shortcomings for small-sized laboratory scale CSB studies • Developed Simple empirical correlation for (ums)o Showed excellent agreement with experimental findings • Results provide platform for design and fabrication of hot flow facility
  • 25. 25 Work in Progress… • Additional tests required for the development of a universally applicable correlation for ums predictions for small-sized laboratory scale CSBs. • Data acquisition system installation • design and development of a laboratory scale CSB biomass gasifier for H2 generation
  • 27. 27 Thank You! Acknowledgement: Louisiana State University Council on Research Faculty Research Grant Program
  • 29. 29 Pressure Drop Measurements Effects of Ho and Do on stable pressure drops and maximum pressure drops